System and method for continuously preparing furfural from acid-containing pentose solution
A technology of furfural and solution, which is applied in the direction of organic chemistry, can solve the problems of many reaction by-products, low unit energy consumption, and low production efficiency, and achieve the effects of low unit energy consumption, strong catalytic ability, and simplified production process
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[0061] use as figure 2 The system shown is for the continuous production of furfural from an acid-containing pentose sugar solution.
[0062]Wherein, a pentose solution with a pentose concentration of 5 g / l is used as a pentose raw material solution, and sulfuric acid is added thereto as a catalyst so that the sulfuric acid concentration in the pentose solution is 4 wt%. The acid-containing pentose solution is heated to 150° C. through the heat exchange unit 40 and then enters the stripping reaction tower 10 from the first raw material inlet 12 . At the same time, the stripping steam with a temperature of 180° C. is input into the stripping reaction tower 10 from the stripping steam inlet 13 . The rising stripping steam is in countercurrent contact with the pentose solution, the pentose solution is heated to about 170° C., and the dehydration and cyclization reaction is carried out in the reaction tower 10 . The furfural produced enters the stripping steam, and is extracted...
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