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Rolling and heat treatment method of high performance aln/az91d magnesium matrix composite

A heat treatment method and composite material technology, which is applied in the field of rolling and heat treatment of high-performance AlN/AZ91D magnesium-based composite materials, can solve the problems of restricting the development and application of traditional magnesium alloy materials, high processing environment requirements, and complicated processes, etc., to achieve The raw material preparation device is safe and reliable, the process parameters are easy to control, and the effect of simple process parameters

Active Publication Date: 2019-05-10
NORTHWESTERN POLYTECHNICAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Since magnesium has a hexagonal close-packed structure (HCP), non-basal slip is difficult to start at room temperature, which leads to low strength and plasticity of magnesium alloys and magnesium-based composites at room temperature.
Low strength and plasticity have always restricted the development and application of plastic deformation of magnesium alloys and magnesium-based composites at room temperature, especially for AZ series cast magnesium alloys, whose poor plasticity makes it difficult to improve mechanical properties and Expand the scope of application by preparing products such as plates and profiles
Therefore, only deformed magnesium alloys such as AZ31 with low strength and good plasticity can be used to prepare plates and profiles, while cast magnesium alloys such as AZ91 with higher room temperature strength do not improve their mechanical properties significantly even after limited thermoplastic deformation, and In the deformation process, there are problems such as complex process, high processing environment requirements, complex equipment, and high preparation cost, which seriously affect and restrict the development and application of traditional magnesium alloy materials.

Method used

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  • Rolling and heat treatment method of high performance aln/az91d magnesium matrix composite
  • Rolling and heat treatment method of high performance aln/az91d magnesium matrix composite
  • Rolling and heat treatment method of high performance aln/az91d magnesium matrix composite

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] 1. The AlN / AZ91 magnesium-based composite ingot of Ф100×130 is used as the original billet, and its preparation method refers to patent ZL201510882938.5;

[0027] 2. Put the AlN / AZ91D magnesium-based composite billet into a muffle furnace, and perform solution treatment at 415°C, and the solution time is 24 hours.

[0028] 3. After the solid solution treatment, take the material out of the muffle furnace and put it into tap water for quenching.

[0029] 4. Cut the quenched composite material ingot into the shape of rolling plate, and the surface is polished smooth, such as figure 2 shown.

[0030] 5. Put the prepared rolled plate into a muffle furnace and preheat it at 350°C for 5-15 minutes, then put it into a two-roll rolling mill for rolling (the rolls do not need to be heated). The rolling speed is 0.25m / s, the initial and final pass reductions are not more than 5%, and the intermediate pass reduction is 10%, annealing at 350°C for 5-10min between each pass. When...

Embodiment 2

[0034] 1. The AlN / AZ91 magnesium-based composite ingot of Ф100×130 is used as the original billet, and its preparation method refers to patent ZL201510882938.5;

[0035] 2. Put the AlN / AZ91D magnesium-based composite billet into a muffle furnace, and perform solution treatment at 420°C, and the solution time is 17 hours.

[0036] 3. After the solid solution treatment, take the material out of the muffle furnace and put it into tap water for quenching.

[0037] 4. Cut the quenched composite material ingot into the shape of rolling plate, and the surface is polished smooth, such as figure 2 shown.

[0038] 5. Put the prepared rolled plate into a muffle furnace and preheat it at 320° C. for 5-15 minutes, then put it into a two-roll mill for rolling (the rolls do not need to be heated). The rolling speed is 0.15m / s, the initial and final pass reductions are not more than 5%, the intermediate pass reduction is 15%, and annealing is performed at 320°C for 5-10min between each pass...

Embodiment 3

[0041]1. The AlN / AZ91 magnesium-based composite ingot of Ф100×130 is used as the original billet, and its preparation method refers to patent ZL201510882938.5;

[0042] 2. Put the AlN / AZ91D magnesium-based composite billet into a muffle furnace, and perform solution treatment at 400°C, and the solution time is 24 hours.

[0043] 3. After the solid solution treatment, take the material out of the muffle furnace and put it into tap water for quenching.

[0044] 4. Cut the quenched composite material ingot into the shape of rolling plate, and the surface is polished smooth, such as figure 2 shown.

[0045] 5. Put the prepared rolled plate into a muffle furnace and preheat it at 320° C. for 12 minutes, then put it into a two-roll rolling mill for rolling (the rolls do not need to be heated). The rolling speed is 0.15m / s, the initial and final pass reductions are not more than 5%, the middle pass reduction is 15%, and each pass is annealed at 350°C for 5 minutes. When the total ...

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Abstract

The invention relates to a rolling and thermal treatment method of high-performance AlN / AZ91D Mg-based composite. Traditional rolling deformation and thermal treatment technology is carried out on thematerial, and the technological parameters are optimized by combining the specific texture structure and strengthening mechanism of the particle reinforced Mg-based composite to prepare a AlN / AZ91D Mg-based composite plate with higher performance. The rolling and thermal treatment technology dedicated to the composite is disclosed, so that rolling deformation of AZ91 alloy as matrix alloy is realized, the mechanical performance of the AlN / AZ91D Mg-based composite is further improved remarkably, and the tensile strength and plasticity of the high-performance AlN / AZ91D Mg-based composite far exceed those of AZ91 alloy as the matrix alloy and most of traditional deformation Mg alloy. In addition, due to the characteristics that the technology is simple, a roller does not need to be heated during rolling deformation and a raw material preparation device is safe and reliable, the rolling and thermal treatment method of high-performance AlN / AZ91D Mg-based composite can be widely applied toindustrial production.

Description

technical field [0001] The invention relates to a rolling and heat treatment method of a high-performance AlN / AZ91D magnesium-based composite material. The in-situ particle-strengthened AlN / AZ91D magnesium-based composite material (patent number: 201510882938.5) is used as a deformed casting slab, and rolling deformation and subsequent The AlN / AZ91D magnesium-based composite sheet with significantly improved mechanical properties was prepared by the heat treatment process, thereby improving the mechanical properties of the widely used AZ91D magnesium alloy in industry. Background technique [0002] Wrought magnesium alloys are widely used due to their superior mechanical properties and formability compared to cast magnesium alloys. However, the inherent low strength and low plasticity of magnesium alloys limit their application as high-performance metal structural materials. Therefore, the development of low-cost high-strength New magnesium-based composite materials with hig...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22F1/06
CPCC22F1/002C22F1/06
Inventor 杨长林赵东辰张斌孙云霞王晓波刘峰
Owner NORTHWESTERN POLYTECHNICAL UNIV