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775results about How to "Optimizing Process Parameters" patented technology

Method for directly producing high-purity oxygen-free copper by pyrogenic process continuous refining of scrap copper

The invention relates to a method for directly producing high-purity oxygen-free copper by pyrogenic process continuous refining of scrap copper, and belongs to the technical field of non-ferrous metallurgy. The method comprises the following steps: by taking scrap copper as a raw material; analyzing the component characteristics of each batch of raw material, and then preparing into a mixture, wherein the mass percent of a copper element in the mixture is greater than or equal to 93%; adding metaphosphate or phosphorus pentoxide and flux to the mixture; refining by oxidation; stewing and drossing after oxidation is finished, and then orderly carrying out reduction refining and refining agent refining under an agitation state, so as to obtain the high-purity oxygen-free copper of which the copper content is greater than or equal to 99.95% and the oxygen content is smaller than 0.003%, wherein the electrical resistivity of the obtained copper wire after drawing is below 0.017241omega/(mm), and the relative electrical conductivity is over 100% of International annealed copper standard (IACS). The method is strong in flexibility, significant in refining effect, and applicable to different components of scrap copper materials; the scrap copper can be used for directly making a rod after being refined. Compared with the traditional pyrogenic process smelting-electrolytic refining-copper cathode purification process, the method disclosed by the invention has the beneficial effects that the flow is shortened, the cost is reduced, the energy is saved, and continuous operation is achieved.
Owner:CENT SOUTH UNIV

Silicon-slag microcrystalline glass and preparation method thereof

The invention relates to silicon-slag microcrystalline glass and a preparation method thereof. Silicon smelting waste slag is taken as a major raw material, and silicon dioxide or silica sand (SiO2), fluorite (CaF2), limestone or calcite (CaCO3), industrial sodium carbonate (Na2CO3), zinc oxide (ZnO) and potassium carbonate (K2CO3) are taken as auxiliary raw materials, wherein the dosage of the silicon smelting waste slag in the raw materials of the microcrystalline glass is 26.0-75.0wt%. The preparation method specifically comprises the following steps of: evenly mixing cold-state silicon slag with other auxiliary raw materials in a blender mixer to obtain a basic mixed batch, melting the basic mixed batch into qualified glass liquid in a melting furnace, and then performing calendering, casting or water quenching on the glass liquid to form a basic glass plate or granules; finally, subjecting the basic glass plate to crystallization heat treatment to obtain the microcrystalline glass. The density of the microcrystalline glass is 2.5-2.8 g/cm<3>, the rupture strength of the microcrystalline glass is 30.0-103.5 MPa, the compressive strength of the microcrystalline glass is 70.0-903.0 MPa, the Moh's hardness of the microcrystalline glass is 5-8 and the abrasive resistance of the microcrystalline glass is 0.063-0.15 g/cm<2>; the silicon-slag microcrystalline glass can be widely applied to the fields such as chemical engineering, metallurgy, architectural ornament, petroleum, mine and machinery.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Preparation process of palladium electrode ion polymer and metal composite

The invention discloses a preparation process of a palladium electrode ion polymer and metal composite, which is used for preparing a palladium metal electrode IPMC (Ion Polymer Metal Composite) by using immersion reduction plating and chemical plating methods in which an ion exchange membrane is used as a matrix material and [Pd (NH3)4] C12 is used as a main salt. The preparation process comprises the following four main steps of: (1) pretreatment of the matrix membrane: carrying out roughening, surface cleaning, foreign ion removal and full swelling on the matrix membrane; (2) immersion reduction plating including two processes, i.e., ion exchange and ion reduction: subjecting a pretreated Nafion membrane to repeated palladium ion immersion and exchange, and reducing the pretreated Nafion membrane with NaBH4 by adopting ultrasonic waves to form palladium metals on the surface and the internal surface of the ion exchange membrane; (3) chemical plating: wherein the thickening electrodes on the outer surface of a core material to compact internal surface electrodes by using an improved chemical plating method; and (4) postprocessing of the composite. The preparation process has a higher popularization value due to relatively improved efficiency, relatively lower cost and excellent actuation response.
Owner:XI AN JIAOTONG UNIV

Laser-reinforced jet-electrodeposition rapid-prototyping processing apparatus and method

The invention discloses a laser-reinforced jet-electrodeposition rapid-prototyping processing apparatus and method. An anode is connected with a laser generation mechanism, an eye shield is located between the laser generation mechanism and the anode, a cathode is a deposition substrate which is arranged in a deposition groove, and a power supply is connected with the cathode and the anode; a Z-axis mobile platform is connected with the anode and the laser generation mechanism, and an X-axis mobile platform and a Y-axis mobile platform are successively arranged below the deposition groove; the liquid inlet end of a constant temperature liquid storage mechanism is connected with the anode, the liquid returning end of the constant temperature liquid storage mechanism is connected with the deposition groove, and a controller is connected with the laser generation mechanism, the power supply, the X-axis mobile platform, the Y-axis mobile platform, the Z-axis mobile platform and the constant temperature liquid storage mechanism. According to the invention, a high-energy density laser beam and a high-speed electrodeposition solution are synchronously jetted to the surface of the cathode through a tubular passive anode centre bore, combination of laser reinforced electrodeposition technology and electrodeposition solution injection is realized, and a high deposition speed is obtained.
Owner:TONGLING UNIV

Method for simultaneously recovering water and latent heat in high-humidity flue gas and heat pump device

The invention discloses a method for simultaneously recovering water and latent heat in high-humidity flue gas and a heat pump device, relating to the technique of energy-saving equipment. A heat exchanger is arranged in an absorber of the heat pump device, the top of the absorber is provided with a flue gas discharging pipe, the bottom of the absorber is provided with a dilute solution outlet, the side surface of the bottom is provided with a gas inlet pipe, the side surface of the top is provided with a concentrated solution inlet, and a concentrated solution pipeline is communicated with a spray head at the inner upper part of a cavity; the top of a regenerator is provided with a dilute solution inlet, the bottom of the regenerator is provided with a concentrated solution pipeline outlet, a gas-liquid heat exchanger is arranged in the regenerator, and an inlet and an outlet of the gas-liquid heat exchanger are communicated with a flue gas pipe; the flue gas pipe is communicated with the gas inlet pipe at the bottom of the absorber after passing through the regenerator; the bottom of the absorber is communicated with the regenerator through a dilute solution pipeline, in which a regulating valve is arranged; and the regenerator runs under negative pressure, and the bottom of the regenerator is communicated with the absorber through the concentrated solution pipeline, in which a solution pump is arranged. The method and the device directly recover the water and the latent heat in the flue gas and have the advantages of equipment simplification, better energy saving, environmental protection and economic benefit.
Owner:INST OF ENGINEERING THERMOPHYSICS - CHINESE ACAD OF SCI

Preparation of non-magnetic high corrosion resistant amorphous steel coating

The invention relates to a ferrous alloy with strong performance of glass formation and a technique method for preparing the coating of the amorphous alloy, in particular to a preparation method of non-magnetic amorphous steel coating with the performance of high anticorrosion and wearing resistance. The method of the invention solves the problem that large brittleness is existed in Fe-based large bulk of amorphous alloy and is a restriction as the structural material to go to engineering application, while the invention causes the application of bulk amorphous alloy to surface engineering field (especially amorphous alloy coating) to be possible. By adopting the Fe-based bulk amorphous alloy to prepare Fe-based amorphous alloy coating, firstly, mater alloy is produced by a method of vacuum induction melting according to needed components; then gas atomization technology is adopted to prepare amorphous alloy powder; supersonic thermal spray technology is adopted to prepare Fe-based amorphous alloy coating. The non-magnetic amorphous steel coating with high anticorrosion performance and wearing resistance produced by the invention is uniform, has low void ratio (less than 0.1 percent), is non-magnetic and has the performance of high anticorrosion and wearing resistance as well as vast application prospect to shell material of ships.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Method for setting process parameters of stainless steel strip steel withdrawal and straightening machine unit

The invention relates to a method for setting process parameters of a stainless steel strip steel withdrawal and straightening machine unit. The method is characterized in that a set of systemic method for setting the process parameters of a stainless steel withdrawal and straightening machine is established by utilizing finite element software to establish a simulation model and applying the stepwise regression principle to set the process parameters such as insertion depths and tension values of a 1# roller, a 2# roller and a 3# roller of a withdrawal and straightening machine, and optimization is achieved by combining application effects of actual production. By means of the method, defects of a wave plate shape and a warping plate shape easily occurring in the production of thinner stainless steel strip steel are eliminated well, theoretical guidance and technical support are provided for withdrawal and straightening of stainless steel, and quality of strip steel is greatly improved. Besides, a process parameter query and addition system interface has strong visuality so that the production is scientific and systematic, and the problem that the process parameters of work shifts are different due to personal experience factors of operators is solved. An adding system guarantees that technical personnel can add process parameters capable of enabling strip steel to obtain good plate shapes after a series of statistics according to actual conditions, so that a database can be kept updated frequently, and process parameter setting can be improved and optimized continuously. Therefore, the method for setting the process parameters of the stainless steel strip steel withdrawal and straightening machine unit has a wide application prospect.
Owner:NINGBO BAOXIN STAINLESS STEEL

After-forging hydrogen diffusion and annealing method of forging material

ActiveCN103014259AOptimizing Process ParametersEliminate white spot defectsHydrogenAir cooling
The invention discloses an after-forging hydrogen diffusion and annealing method of a forging material, which is completed in an annealing furnace. For a large forging material, the after-forging hydrogen diffusion and annealing method comprises the following steps of: 1, normalizing a forged forging material at a temperature of 850-890 DEG C and remaining for 4-10h; 2, air-cooling the forging material normalized in the step 1 to 300-330 DEG C, remaining for 3-8h; 3, raising the temperature of the forging material air-cooled in the step 2 to 660-680 DEG C, homogenizing the temperature for 1-2h/100mm, insulating the heat; 4, air-cooling the forging material insulated in the step 3 to 400 DEG C and furnace-cooling to 300-330 DEG C and remaining for 6-8h, then raising the temperature of the forging material to 660-680 DEG C, homogenizing the temperature for 1-2h/100mm and then insulating the heat; and 5, cooling the forging material insulated by temperature homogenization in the step 4 to below 200 DEG C and discharging, wherein the total time of the heat insulation in the steps 3 and 4 is 7-16h/100mm. The after-forging hydrogen diffusion and annealing method is simple in process and strong in adaptability for the large-specification forging material, and avoids the white dot defect of the forging material.
Owner:DAYE SPECIAL STEEL CO LTD

Camera-based real-time shooting 3D printing process monitoring method and device

The invention discloses a camera-based real-time shooting 3D printing process monitoring method and device. A camera is mounted on the upper portion of a sealing forming chamber and shoots the morphology in the molten layer 3D printing process. A light source is mounted on the inner side of the top of the sealing forming chamber. The light source is lightened in a pulse manner while exposure of the camera is achieved, the light source is extinguished after exposure of the camera is finished, and the morphology data of the layer are transmitted into a computer and stored in real time through the camera. By means of manual error analysis or intelligent error analysis, for defect parts existing in the printing process, the positions, time and reasons of defect generating can be accurately located, and effective bases are provided for optimizing and adjusting relevant parameters. The device is simple in structure and convenient to operate, integrity of data of each layer is guaranteed, process parameters are optimized, correction is achieved in time in the processing process, and part precision is greatly improved; or, after processing, by means of morphology analysis, problems existing in the processing process are found.
Owner:SOUTH CHINA UNIV OF TECH

A method of separating and purifying quercetagetin from tagetes erecta

A method of separating and purifying quercetagetin from tagetes erecta is provided. The method includes a step of drying tagetes erecta dry flowers, grinding into powder, dipping with ethanol or performing reflux extraction, subjecting a filtrate after filtration to rotary evaporation until a product is dry and dissolving the product to a methanol-water mixed solvent; a step of performing one-dimensional liquid chromatogram, wherein DAISO C18 is adopted as a chromatographic column, a mobile phase adopting water as an A phase and methanol as a B phase is adopted, isocratic elution is performed for 20 min with the concentration of the B phase in the mobile phase being 50-55%, eluate from the 6 min to the 12 min is collected according to an ultraviolet absorption spectrum, adopted as a target component, and subjected to rotary evaporation until a product is dry, and the product of the rotary evaporation is dissolved into the methanol-water mixed solution again; and a step of performing two-dimensional liquid chromatogram, wherein Acchrom X-Amide is adopted as a chromatographic column, a mobile phase adopting water as an A phase and acetonitrile as a B phase is adopted, isocratic elution is performed for 40 min with the concentration of the B phase in the mobile phase being 92-98%, and eluate from the 27 min to the 33 min is collected according to an ultraviolet absorption spectrum, adopted as the target component, and subjected to rotary evaporation until a product is dry to obtain quercetagetin the purity of which is 99% or above.
Owner:TIANJIN YAOYU BIOLOGICAL TECH
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