Gas barrier film, transfer method of gas barrier film, wavelength conversion film, retardation film with gas barrier layer, and organic el laminate
A technology of gas barrier film and gas barrier layer, applied in chemical instruments and methods, layered products, electrical components, etc., can solve problems such as difficulties
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Embodiment 1
[0271] Produced as Example 1 figure 1 (A) shows the gas barrier film 10a.
[0272]
[0273] As the substrate 12, a long-sized PET film (manufactured by TOYOBO CO., LTD., Cosmo shine A4100) having a width of 1000 mm, a thickness of 50 μm, and a length of 100 m was used.
[0274] On the unprimed surface side of this substrate 12, a release resin layer 20 was formed according to the following procedure.
[0275] As coating liquid A1 used as the peeling resin layer 20, the coating liquid of 10% of solid content concentration was prepared by dissolving COC resin (Mitsui Chemicals, Inc. APEL 6015T) using cyclohexane.
[0276] The coating solution A1 is filled in such as Figure 8 (A) The coating part 40 of the RtoR-based film-forming apparatus shown. The coating unit 40 used a die coater. Then, the substrate roll Ra in which the substrate 12 is wound into a roll is loaded at a predetermined position, and the substrate 12 is inserted along a predetermined conveyance path.
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Embodiment 2
[0294]Furthermore, an organic protective layer 24 shown below was formed on the inorganic layer 16. In the same manner as in Example 1, the following figure 2 (A) shows the gas barrier film 10b.
[0295] Polyurethane backbone acrylic polymer (ACRIT 8BR930 manufactured by TAISEI FINECHEMICAL CO., LTD.), photopolymerization initiator (Irg184 manufactured by BASF JAPAN LTD.), silane coupling agent (Shin -KBM5103 manufactured by Etsu Chemical Co., Ltd.) and softener (BYRONU1400 manufactured by TOYOBO CO., LTD.) were weighed and dissolved in methyl ethyl ketone to prepare a coating solution with a solid content concentration of 15%. As the coating liquid C1 to be the organic protective layer 24 .
[0296] Fill the coating liquid C1 in such as Figure 8 (A) The coating part 40 of the RtoR-based film-forming apparatus shown. The coating unit 40 used a die coater. Then, a substrate roll in which the substrate 12 (hereinafter, sometimes referred to as "film-forming base material Z...
Embodiment 3
[0299] The following coating liquid C2 was used as the coating liquid for the organic protective layer 24, and the thickness of the organic protective layer 24 was set to 3 μm. , A separator (FILM BYNA BD manufactured by FUJIMORI KOGYO CO., LTD.) was attached as the protective film 26, and in the same manner as in Example 2, the following figure 2 (B) shows the gas barrier film 10c.
[0300] Curing agent L-45 (manufactured by Soken Chemical & Engineering Co., Ltd.) was added to SK DYNE NT21 (manufactured by Soken Chemical & Engineering Co., Ltd.) at a ratio of 100:2, and diluted with butyl acetate to prepare a solid content concentration of 15 % of coating solution C2.
[0301] The organic protective layer 24 is an acrylic adhesive.
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Abstract
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