Self-compensating shrinkage and slump-retaining copolymer and preparation method thereof
A slump-preserving type and copolymer technology, which is applied in the field of building materials, can solve the problems of poor slump-preserving effect of slow release of water reducers, and achieve the effect of improving workability and volume stability
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Embodiment 1
[0028] A self-compensating shrinkage slump-preserving copolymer, the components of which are in parts by weight: 2 parts of acrylic acid, 1 part of sodium propylene sulfonate, and 2.5 parts of methoxy polyethylene glycol maleate monoester with a mass concentration of 60%. , 30 parts of alkylene-based polyoxyethylene ether, 1.5 parts of ammonium persulfate, 3 parts of NaOH solution with a mass concentration of 30%, and 50 parts of water;
[0029] The molecular weight of the methoxy polyethylene glycol monoester is 500-2500;
[0030] The molecular weight of the alkylene polyoxyethylene ether is 3400-6000.
[0031] Its preparation method comprises the following steps:
[0032] Step 1, acrylic acid and ammonium persulfate of specified quality are respectively prepared into 20% aqueous solution for subsequent use;
[0033] Step 2, pump the measured water into the reactor, put a specified amount of methoxypolyethylene glycol maleic acid monoester and alkylene polyoxyethylene ether...
Embodiment 2
[0046] A self-compensating shrinkage-retaining copolymer, the components of which are in parts by weight: 2.5 parts of acrylic acid, 1.5 parts of sodium propylene sulfonate, and 3 parts of methoxy polyethylene glycol monomaleic acid monoester with a mass concentration of 60%. , 35 parts of alkylene-based polyoxyethylene ether, 2 parts of ammonium persulfate, 4 parts of NaOH solution with a mass concentration of 30%, and 55 parts of water;
[0047] The molecular weight grade of described methoxypolyethylene glycol maleate monoester is 500~700;
[0048] The molecular weight of the alkylene polyoxyethylene ether is 4000-5000.
[0049] Its preparation method comprises the following steps:
[0050] Step 1, acrylic acid and ammonium persulfate of specified quality are respectively prepared into 20% aqueous solution for subsequent use;
[0051] Step 2, pump the measured water into the reactor, put a specified amount of methoxypolyethylene glycol maleic acid monoester and alkylene p...
Embodiment 3
[0064] A self-compensating shrinkage-retaining copolymer, the components of which are in parts by weight: 3 parts of acrylic acid, 2 parts of sodium propylene sulfonate, and 4 parts of methoxy polyethylene glycol maleate monoester with a mass concentration of 60%. , 35 parts of alkylene-based polyoxyethylene ether, 2.5 parts of ammonium persulfate, 5 parts of NaOH solution with a mass concentration of 30%, and 60 parts of water;
[0065] The molecular weight grade of described methoxypolyethylene glycol maleate monoester is 500~700;
[0066] The molecular weight of the alkylene polyoxyethylene ether is 4000-5000.
[0067] Its preparation method comprises the following steps:
[0068] Step 1, acrylic acid and ammonium persulfate of specified quality are respectively prepared into 20% aqueous solution for subsequent use;
[0069] Step 2, pump the measured water into the reactor, put a specified amount of methoxypolyethylene glycol maleic acid monoester and alkylene polyoxyethy...
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Abstract
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