Film forming agent, and cosmetic composition and cosmetic using same
A technology of cosmetics and compositions, applied in the direction of cosmetics, cosmetics, cosmetic preparations, etc., which can solve the problems of water resistance, insufficient persistence, greasy and sticky, and the inability to mix a large amount of film-forming agents, etc., to achieve excellent hair adhesion, Easy design and high stability effect
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Embodiment 1
[0151] (monomer emulsification)
[0152] 0.53 parts by weight of sodium lauryl sulfate was measured in the beaker 1, and 51.72 parts by weight of ion-exchanged water was added and stirred to obtain an aqueous solution. 10.09 parts by weight of methyl methacrylate, 3.18 parts by weight of butyl acrylate, and 13.23 parts by weight of carbosiloxane dendrimer represented by the general formula (1) were added to the beaker 2 to make them uniform. Add the mixture in beaker 2 to beaker 1, stir for a few minutes, use a homogenizer at a pressure of 400-500Kg / cm 2 The mixture was passed through several times to obtain a milky white monomer emulsion with an average particle diameter of 153 nm.
[0153] (Radical Polymerization)
[0154] Into a separable flask, 8.00 parts by weight of ion-exchanged water and a part of the obtained monomer emulsion were charged, and the temperature was raised to 70° C. while stirring. After reaching 70° C., the obtained remaining monomer emulsion and a 1...
Embodiment 2
[0156] Use the following formula, change the polymerization temperature to 80°C, change the emulsifier from sodium lauryl sulfate to laureth-1 phosphate, neutralize the emulsifier with 50% sodium hydroxide before use, in addition, It carried out similarly to Example 1.
[0157] (monomer emulsification)
[0158] Beaker 1:
[0159] Laureth-1 phosphate (90%): 0.67 parts by weight
[0160] 50% sodium hydroxide: 0.17 parts by weight
[0161] Ion-exchanged water: 46.87 parts by weight
[0162] Beaker 2:
[0163] Methyl methacrylate: 11.49 parts by weight
[0164] Butyl acrylate: 3.61 parts by weight
[0165] Carbosiloxane dendrimers represented by general formula (1): 15.06 parts by weight
[0166] 2-phenoxyethanol: 0.30 parts by weight
[0167] Average particle size of monomer emulsion:
[0168] Milky white with an average particle size of 117nm.
[0169] (Radical Polymerization)
[0170] Separable flasks:
[0171] Ion-exchanged water: 6.75 parts by weight
[0172] mon...
Embodiment 3
[0178] Use the following formula, change the polymerization temperature to 80°C, change the emulsifier from sodium lauryl sulfate to laureth-1 phosphate, neutralize the emulsifier with 50% sodium hydroxide before use, in addition, It carried out similarly to Example 1.
[0179] (monomer emulsification)
[0180] Beaker 1:
[0181] Sodium lauryl phosphate: 0.60 parts by weight
[0182] Ion-exchanged water: 49.72 parts by weight
[0183] Beaker 2:
[0184] Methyl methacrylate: 11.45 parts by weight
[0185] Butyl acrylate: 3.62 parts by weight
[0186] Carbosiloxane dendrimers represented by general formula (1): 15.07 parts by weight
[0187] 2-phenoxyethanol: 0.30 parts by weight
[0188] Average particle size of monomer emulsion:
[0189] Milky white with an average particle size of 125nm.
[0190] (Radical Polymerization)
[0191] Separable flasks:
[0192] Ion-exchanged water: 4.17 parts by weight
[0193] monomer emulsion
[0194] 1% potassium persulfate aqueous...
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