Biaxially oriented polypropylene film, metal film laminated film and film capacitor
A polypropylene film, biaxially oriented technology, used in film/thick film capacitors, metal layered products, fixed capacitor dielectrics, etc., can solve the problems of limited heat resistance effect and unsatisfactory high temperature withstand voltage characteristics Achieving the effect of excellent withstand voltage characteristics
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Embodiment 1
[0126] A. Manufacture of polypropylene resin composition
[0127] Phthalic anhydride was added to the solution which mixed anhydrous magnesium chloride, decane, and 2-ethylhexyl alcohol, and heated, and it stirred further. After the above solution was cooled, it was added dropwise to titanium tetrachloride cooled to -20°C. Next, the temperature of the above-mentioned mixture was raised, and diisobutyl phthalate was added and stirred, and then, a solid was obtained by filtration. The obtained solid was washed with decane and hexane to obtain a titanium catalyst used for propylene polymerization.
[0128] Propylene polymerization was carried out using the aforementioned titanium catalyst, triethylaluminum as a cocatalyst, dicyclopentyldimethoxysilane, and hydrogen as a chain transfer agent. After the obtained product was inactivated, it was washed sufficiently with propylene monomer to obtain a polypropylene resin. The polypropylene resin had a melting point of 165° C., an MF...
Embodiment 2
[0133] A biaxially oriented polypropylene film having a thickness of 2.5 μm was obtained in the same manner as in Example 1 except that the stretching speed in the longitudinal stretching step was 3,550,000% / min. In addition, there was no film breakage at the time of film formation for 1 hour. Table 1 shows the physical properties of the obtained film.
Embodiment 3
[0135] The addition amount of triethylaluminum as a co-catalyst during the production of polypropylene resin was adjusted, and the mesopentad fraction (mmmm) of polypropylene resin was changed so that it became 0.950, except that it was the same as in Example 1 production, and a biaxially oriented polypropylene film with a thickness of 2.5 μm was obtained. In addition, there was no film breakage at the time of film formation for 1 hour. Table 1 shows the physical properties of the obtained film.
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