Carboxylic acid derivatization beta-carboline and preparation method thereof
A derivatization and carboline technology, which is applied in the fields of chemistry and medicine, can solve problems such as insufficient structural diversity, and achieve the effects of wide application range of substrates, strong functional group tolerance, and mild reaction conditions
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[0020] In order to further understand the present invention, the preferred embodiments of the present invention are described below in conjunction with the examples, but it should be understood that these descriptions are only to further illustrate the features and advantages of the present invention, rather than limiting the claims of the present invention.
[0021] The preparation method of the examples in the present invention is as follows: in an organic solvent, add methyl-β-carboline, catalyst and condensation agent, react at a certain temperature for a certain period of time, and obtain a crude product after filtering the reaction mixture, and the crude product is re- The product is obtained after crystallization or column purification. Embodiment 1-15, methyl-beta-carboline reaction material used, catalyst, initiator, organic solvent, reaction temperature, reaction time and productive rate are shown in Table 1. The compound structures of the products are shown in Table...
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