Application of bismuth telluride nanosheet loaded with cobalt-nickel-molybdenum particles in field of oxygen reduction
A technology of bismuth telluride and nanosheets is applied in the field of bismuth telluride nanosheets loaded with cobalt, nickel and molybdenum particles and its synthesis, which can solve the problems of high price and limited application, and achieves simple operation, shortened reaction time, and solves particle agglomeration. Effect
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Embodiment 1
[0023] Take 0.315gBiCl 3 , 0.34gNa 2 TeO 3 , 0.48g PVP (w = 40000), 0.58g NaOH in 36ml ethylene glycol, stirred at room temperature for 2h.
[0024] Transfer the above to a polytetrafluoroethylene high-temperature reactor, and keep the temperature at 220° C. for 36 hours.
[0025] The samples were taken out, washed by centrifugation with deionized water and absolute ethanol three times, and then dried for use.
[0026] Take 0.07g of dried bismuth telluride nanoplatelets after alkali treatment and put them in the Co-Ni-Mo source mixed solution, the volume ratio of ethylene glycol: water in the mixed solution is 1:1, and the total amount of the solution is 20ml. The concentration of nickel sulfate in the solution is 0.0285M, the concentration of sodium molybdate is 0.00565M, the concentration of cobalt nitrate is 0.000694M, the concentration of trisodium citrate is 0.0249M, the concentration of PVP is 0.0000625M, stir at room temperature for 50min, and then directly Add 0.08...
Embodiment 2
[0029] Take 0.315gBiCl 3 , 0.34gNa 2 TeO 3 , 0.52g PVP (w = 40000), 0.62g NaOH in 36ml ethylene glycol, stirred at room temperature for 2h.
[0030] Transfer the above to a polytetrafluoroethylene high-temperature reactor, and keep the temperature at 220° C. for 36 hours.
[0031] The samples were taken out, washed by centrifugation with deionized water and absolute ethanol three times, and then dried for use.
[0032] Take 0.07g of dried bismuth telluride nanoplatelets after alkali treatment and put them in the Co-Ni-Mo source mixed solution, the volume ratio of ethylene glycol: water in the mixed solution is 1:1, and the total amount of the solution is 20ml. The concentration of nickel sulfate in the solution is 0.0287M, the concentration of sodium molybdate is 0.00567M, the concentration of cobalt nitrate is 0.00694M, the concentration of trisodium citrate is 0.0251M, the concentration of PVP is 0.0000625M, stir at room temperature for 70min, and then directly Add 0.08g...
Embodiment 3
[0035] Take 0.315gBiCl 3 , 0.34gNa 2 TeO 3 , 0.50g PVP (w = 40000), 0.60g NaOH in 36ml ethylene glycol, stirred at room temperature for 2h.
[0036] Transfer the above to a polytetrafluoroethylene high-temperature reactor, and keep the temperature at 220° C. for 36 hours.
[0037] The samples were taken out, washed by centrifugation with deionized water and absolute ethanol three times, and then dried for use.
[0038]Take 0.07g of dried bismuth telluride nanoplatelets after alkali treatment and put them in the Co-Ni-Mo source mixed solution, the volume ratio of ethylene glycol: water in the mixed solution is 1:1, and the total amount of the solution is 20ml. The concentration of nickel sulfate in the solution is 0.0286M, the concentration of sodium molybdate is 0.00566M, the concentration of cobalt nitrate is 0.0347M, the concentration of trisodium citrate is 0.0250M, the concentration of PVP is 0.0000625M, stir at room temperature for 60min, and then directly Add 0.08g o...
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