Multifunctional composite filter screen material for air purifier and preparation method thereof
An air purifier and composite material technology, which is applied in chemical instruments and methods, botanical equipment and methods, separation methods, etc., can solve the problems of few multi-functional composite filter screens and high cost of purifiers, and achieve improved specific surface area and Adsorption capacity, beneficial to enrichment, and the effect of improving visible light response
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Embodiment 1
[0034] (1) Preparation of N-aryl-2-(benzisothiazolin-3-one-2-yl)formamide organic antibacterial agent. Weigh 20mmol of bistrichloromethyl carbonate and 10mL of toluene, add to a three-necked flask with a volume of 100mL equipped with stirring, reflux condenser and constant pressure funnel and stir, add 30mmol of o-methyl to the constant pressure funnel The mixed solution of aniline and 10mL of toluene was slowly added dropwise to the flask. When the dropwise addition was completed, the reaction was heated under reflux for 5h. When the reaction was completed, 30mmol of benzisothiazolin-3-one was directly added to the flask, and Add 20mL of toluene to carry out reflux reaction. After the reaction is completed, naturally cool to room temperature, filter under reduced pressure, wash with acetone to remove unreacted substances, and place in a vacuum drying oven to dry at 50°C for 24h. The white needle-like crystals obtained were N-aryl-2-(benzisothiazolin-3-one-2-yl)formamide;
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Embodiment 2
[0037] (1) Preparation of N-aryl-2-(benzisothiazolin-3-one-2-yl)formamide organic antibacterial agent. Weigh 20mmol of bistrichloromethyl carbonate and 10mL of toluene, add to a three-necked flask with a volume of 100mL equipped with stirring, reflux condenser and constant pressure funnel and stir, add 30mmol of o-methyl to the constant pressure funnel The mixed solution of aniline and 10mL of toluene was slowly added dropwise to the flask. When the dropwise addition was completed, the reaction was heated under reflux for 5h. When the reaction was completed, 30mmol of benzisothiazolin-3-one was directly added to the flask, and Add 20mL of toluene to carry out reflux reaction. After the reaction is completed, naturally cool to room temperature, filter under reduced pressure, wash with acetone to remove unreacted substances, and place in a vacuum drying oven to dry at 50°C for 24h. The white needle-like crystals obtained were N-aryl-2-(benzisothiazolin-3-one-2-yl)formamide; (2),...
Embodiment 3
[0039] (1) Preparation of N-aryl-2-(benzisothiazolin-3-one-2-yl)formamide organic antibacterial agent. Weigh 20mmol of bistrichloromethyl carbonate and 10mL of toluene, add to a three-necked flask with a volume of 100mL equipped with stirring, reflux condenser and constant pressure funnel and stir, add 30mmol of o-methyl to the constant pressure funnel The mixed solution of aniline and 10mL of toluene was slowly added dropwise to the flask. When the dropwise addition was completed, the reaction was heated under reflux for 5h. When the reaction was completed, 30mmol of benzisothiazolin-3-one was directly added to the flask, and Add 20mL of toluene to carry out reflux reaction. After the reaction is completed, naturally cool to room temperature, filter under reduced pressure, wash with acetone to remove unreacted substances, and place in a vacuum drying oven to dry at 50°C for 24h. The white needle-like crystals obtained were N-aryl-2-(benzisothiazolin-3-one-2-yl)formamide; (2),...
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