Aqueous ink set for ink jet recording and ink jet recording method
A technology of inkjet recording and water-based ink, applied in the direction of copying/marking methods, inks, applications, etc., can solve the problems of not being able to obtain high image quality, and cannot fully suppress bleeding, etc.
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[0275] Hereinafter, the present invention will be further described in detail through examples.
[0276] (Method for producing polymer (A))
Synthetic example 1
[0278] Butyllithium (BuLi) as the polymerization initiator and styrene (St) as the first monomer were figure 1 The tube reactors P1 and P2 in the import figure 1 The T-shaped micro-mixer M1 in the living anion polymerization to form a polymer.
[0279] Next, the resulting polymer was passed through figure 1 In the tubular reactor R1 and moved to figure 1 The T-shaped micro-mixer M2 in the figure 1 The reaction modifier (α-methylstyrene (α-MeSt)) introduced in tubular reactor P3 in 2000 was used to capture the growing ends of the polymer.
[0280] Next, tert-butyl methacrylate (t-BMA) as the second monomer was figure 1 The shown tubular reactor P4 is introduced into the T-shaped micro-mixer M3, and passed through figure 1 The above-mentioned polymers moving in the tubular reactor R2 undergo continuous living anionic polymerization. Thereafter, the reaction was quenched with methanol to produce a block copolymer (PA-1).
[0281] At this time, the entire microreactor was e...
manufacture example 1
[0333] (Manufacturing method of production example 1 aqueous pigment dispersion (C-1))
[0334] The following step 1 is carried out: 150 parts by mass of a phthalocyanine-based pigment Fastogen Blue pigment (manufactured by DIC Corporation: C.I. pigment 15:3) as a pigment, 30 parts by mass of a polymer (P-1) as a polymer (A), and as 150 mass parts of triethylene glycol of water-soluble organic solvent, 20 mass parts of 34% potassium hydroxide aqueous solution drop in the intensive mixer of 1.0L (Japan Eirich Co., Ltd.), at rotor peripheral speed 2.94m / s, disk peripheral speed 1m / s for 25 minutes of mixing.
[0335] Next, the following step 2 was carried out: After slowly adding 450 parts by mass of ion-exchanged water to the kneaded product in the intensive mixer container while stirring continuously, 185 parts by mass of ion-exchanged water was added and mixed to obtain a pigment concentration of 15.0%. Aqueous Pigment Dispersion (C-1).
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