Supported hydrochloric acid decolorizing agent as well as preparation method and decolorization process thereof
A supported reagent and decolorizing agent technology, applied in chemical instruments and methods, halogen/halogen acid, chlorine/hydrogen chloride purification, etc., can solve the problems of difficult resin handling, waste of resources, environmental pollution, etc., and achieve short production cycle and effect. Good, short depigmentation time
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[0018] Example 1
[0019] The components of the new loaded reagent used for hydrochloric acid decolorization are: 10% MCM-41 treated with trimethoxysilylpropylamine and trimethylchlorosilane (the specific treatment process is: 20 grams of trimethyl The oxysilylpropylamine was dissolved in 160 ml of anhydrous methylene chloride, and the solution was added to a suspension of 1600 ml of anhydrous chloroform containing 28 g of ordered mesoporous material MCM-41. The mixture was kept at 65°C Stir for 24 hours. Then the solid was filtered and washed with dichloromethane (2*200ml) and dried under vacuum at 160°C for 5 hours. Then the dried solid was added to 1000ml of anhydrous chloroform, while adding 50g of three Methylchlorosilane was stirred at room temperature for 24 hours, and then filtered to obtain a solid powder, which was washed with acetone (3*200ml) and ether (3*200ml), and dried under vacuum at 120°C for 5 hours. The above-mentioned ordered mesoporous material MCM-41 treat...
Example Embodiment
[0020] Example 2
[0021] The components of the new load-type reagent for hydrochloric acid decolorization are: 20% MCM-41 treated with trimethoxysilylpropylamine and trimethylchlorosilane (the specific treatment process is: 20 grams of trimethyl The oxysilylpropylamine was dissolved in 160 ml of anhydrous methylene chloride, and the solution was added to a suspension of 1600 ml of anhydrous chloroform containing 28 g of ordered mesoporous material MCM-41. The mixture was kept at 65°C Stir for 24 hours. Then the solid was filtered and washed with dichloromethane (2*200ml) and dried under vacuum at 160°C for 5 hours. Then the dried solid was added to 1000ml of anhydrous chloroform, while adding 50g of three Methylchlorosilane was stirred at room temperature for 24 hours, and then filtered to obtain a solid powder, which was washed with acetone (3*200ml) and ether (3*200ml), and dried under vacuum at 120°C for 5 hours. The above ordered mesoporous material MCM-41 treated with trim...
Example Embodiment
[0022] Example 3
[0023] The components of the new load-type reagent for hydrochloric acid decolorization are: 20% MCM-41 treated with trimethoxysilylpropylamine and trimethylchlorosilane (the specific treatment process is: 20 grams of trimethyl The oxysilylpropylamine was dissolved in 160 ml of anhydrous methylene chloride, and the solution was added to a suspension of 1600 ml of anhydrous chloroform containing 28 g of ordered mesoporous material MCM-41. The mixture was kept at 65°C Stir for 24 hours. Then the solid was filtered and washed with dichloromethane (2*200ml) and dried under vacuum at 160°C for 5 hours. Then the dried solid was added to 1000ml of anhydrous chloroform, while adding 50g of three Methylchlorosilane was stirred at room temperature for 24 hours, and then filtered to obtain a solid powder, which was washed with acetone (3*200ml) and ether (3*200ml), and dried under vacuum at 120°C for 5 hours. The above-mentioned ordered mesoporous material MCM-41 treated...
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