Extraction method of rice bran oil and cosmetic composition comprising rice bran oil
A technology for cosmetic composition and rice bran oil, which is applied to cosmetics, cosmetic preparations, cosmetic preparations and other directions, can solve the problems of difficult solvent recovery, cumbersome extraction method, low extraction efficiency, etc., and achieves excellent moisturizing effect and repairing effect. , the effect of high extraction rate
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Embodiment 1
[0031] The extraction of embodiment 1 rice bran oil and condition optimization
[0032] Weigh 200g (accurate to 0.01g) of 60-mesh rice bran with an electronic balance, put the rice bran into the barrel, put the barrel into the extraction kettle, install the pressure ring and sealing ring, tighten the plug, and start the supercritical extractor , set the flow rate of carbon dioxide to 20L / h, and investigate the influence of pressure, temperature and extraction time on supercritical CO2 extraction. The extraction efficiency is evaluated based on the quality of rice bran oil extracted from 200g of rice bran (accurate to 0.01g).
Embodiment 11
[0033] The optimization of embodiment 1.1 extraction pressure
[0034]The flow rate of fixed carbon dioxide is 20L / h, the extraction temperature is 40°C, and the extraction time is 2 hours. The influence of extraction pressure on extraction efficiency is shown in Table 1 below:
[0035] The influence of table 1 extraction pressure on extraction efficiency
[0036] Extraction pressure / MPa 20 25 30 35 40 Mass of rice bran oil / g 28.11 34.15 38.87 38.92 39.01
[0037] It can be seen from Table 1 that the extraction amount of rice bran oil gradually increases with the increase of extraction pressure. The optimal extraction pressure is 30-40Mpa. When the extraction pressure was 30MPa, the extraction of rice bran oil did not increase significantly when the extraction pressure was increased. Considering comprehensively, the optimal extraction pressure is 30MPa.
Embodiment 12
[0038] The optimization of embodiment 1.2 extraction temperature
[0039] The flow rate of fixed carbon dioxide is 20L / h, the extraction pressure is 30MPa, and the extraction time is 2 hours. The influence of extraction temperature on extraction efficiency is shown in Table 2 below:
[0040] The influence of table 2 extraction temperature on extraction efficiency
[0041] Extraction temperature / ℃ 25 30 35 40 45 Mass of rice bran oil / g 27.63 31.05 35.22 38.87 33.52
[0042] It can be seen from Table 2 that the extraction temperature has a great influence on the extraction amount of rice bran oil, the optimum extraction temperature is 35-45°C, and the optimum extraction temperature is 40°C.
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