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Graphene film rolled materials and preparation method thereof

A graphene film roll and graphene film technology are applied in the preparation of graphene film roll materials, graphene film roll materials and their preparation fields, and can solve problems such as graphene product bottlenecks, supply chain shortages, electromagnetic wave pollution, and the like, Achieve the effect of stable product quality, easy operation and increased service life

Inactive Publication Date: 2018-08-28
苏州天煜新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The upgrading of electronic equipment brings great convenience and excellent experience to people's life, but also brings some problems: (1) more heat generation; (2) more serious electromagnetic wave pollution
At present, domestic and international heat dissipation products mainly use artificial graphite, natural graphite and metal materials for heat dissipation. This product is mainly used to replace artificial graphite, which is a high thermal conductivity material. Artificial graphite coil is one of the main products in the current market. The limitation of production capacity has led to a shortage of domestic product supply chains, and there is often a lack of raw materials. However, graphene products have accumulated over the years and many companies have bottlenecks in production and market applications.

Method used

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  • Graphene film rolled materials and preparation method thereof
  • Graphene film rolled materials and preparation method thereof
  • Graphene film rolled materials and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] The preparation of embodiment 1 TYGO-015JC model product

[0022] A method for preparing a graphene film roll material, comprising the following steps:

[0023] a) ultrasonic immersion and stirring of graphene oxide in water;

[0024] B) Graphene oxide solution is coated on the PI film, dry continuously, obtain the rolled graphene film base material that removes PI film;

[0025] c) Carry out high-temperature carbonization with the roll-shaped graphene film base material in a sintering furnace by temperature programming to form a graphene film bubble-like coil;

[0026] D) Graphene film foamed roll material is placed in a high-temperature furnace for graphitization, and the graphene film substrate is obtained by cooling after graphene is completed;

[0027] E) and the graphene film substrate product that step d) obtains is taken out, after the graphene film substrate product is carried out calendering with calender, finally produce the graphene film of roll shape.

...

Embodiment 2

[0033] The preparation of embodiment 2 TYGO-025J model product

[0034] A method for preparing a graphene film roll material, comprising the following steps:

[0035] a) ultrasonic immersion and stirring of graphene oxide in water;

[0036] B) Graphene oxide solution is coated on the PI film, dry continuously, obtain the rolled graphene film base material that removes PI film;

[0037] c) Carry out high-temperature carbonization with the roll-shaped graphene film base material in a sintering furnace by temperature programming to form a graphene film bubble-like coil;

[0038] D) Graphene film foamed roll material is placed in a high-temperature furnace for graphitization, and the graphene film substrate is obtained by cooling after graphene is completed;

[0039] E) and the graphene film substrate product that step d) obtains is taken out, after the graphene film substrate product is carried out calendering with calender, finally produce the graphene film of roll shape.

[...

Embodiment 3

[0045] Embodiment 3 Preparation of TYGO-040J model product

[0046] A method for preparing a graphene film roll material, comprising the following steps:

[0047] a) ultrasonic immersion and stirring of graphene oxide in water;

[0048] B) Graphene oxide solution is coated on the PI film, dry continuously, obtain the rolled graphene film base material that removes PI film;

[0049] c) Carry out high-temperature carbonization with the roll-shaped graphene film base material in a sintering furnace by temperature programming to form a graphene film bubble-like coil;

[0050] D) Graphene film foamed roll material is placed in a high-temperature furnace for graphitization, and the graphene film substrate is obtained by cooling after graphene is completed;

[0051] E) and the graphene film substrate product that step d) obtains is taken out, after the graphene film substrate product is carried out calendering with calender, finally produce the graphene film of roll shape.

[0052] ...

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Abstract

The invention discloses a preparation method of graphene film rolled materials. The preparation method comprises the following steps: preparing a graphene oxide solution; coating the solution onto a PI (polyimide) film, and drying to obtain the graphene film base materials; performing high-temperature carbonization and graphitization on the graphene film base materials, and calendering the graphene film by adopting a calendering machine to obtain a rolled graphene heat dissipation film. An innovative operation way comprises the special following steps: slicing the rolled graphene film base materials into the required specifications so as to obtain the graphene film base materials with various specifications and ensure that the graphene film base materials are in a rolled shape; then putting the rolled graphene film base materials in a common double-layer jig; putting the jig into a sintering furnace, and setting a required temperature curve according to products with different thicknesses; performing high-temperature carbonization, graphitization and temperature reduction on the products; taking the graphitized graphene film base material products out, and calendering the productsby using the calendering machine to obtain the rolled graphite heat dissipation film. The method has the advantages of simple process and easiness for popularization, and moreover, the graphene film has the excellent shielding effect and extremely strong heat dissipation performance.

Description

technical field [0001] The invention relates to a graphene film roll material and a preparation method thereof. The produced product belongs to the technical field of nanomaterial graphene polymer material carbonization products, and is mainly used as heat dissipation and shielding materials in the electronics industry. Particularly refer to a kind of graphene thin film rolling material preparation method, the present invention also relates to a kind of graphene thin film. technical background [0002] With the expansion and popularization of electronic and electrical equipment applications, the performance and structure requirements of electronic equipment are becoming more and more stringent, including higher processing speed, higher processing frequency, smaller volume, lighter weight, and more high power. The upgrading of electronic equipment brings great convenience and excellent experience to people's life, but also brings some problems: (1) more heat generation; (2) ...

Claims

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Application Information

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IPC IPC(8): C01B32/184
Inventor 史广洲周建丽
Owner 苏州天煜新材料科技有限公司
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