Temperature-resistant and anti-salt type functional polymer and preparation method thereof
A temperature-resistant, salt-resistant, functional technology, applied in the field of functional polymers and their preparation, can solve the problems of many chemical reagents, limited heat-resistant and salt-resistant capabilities, and cumbersome operations, so as to improve the temperature-resistant and salt-resistant capabilities, change Structure and performance, the effect of ensuring stability
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[0031] 1: Preparation of functional monomer 1
[0032] Put 5g of undecylamine and 5g of 1-bromoundecane into the reactor, then add 25g of acetonitrile, heat and stir at 40°C, until the amine salt appears at the bottom of the bottle, add 25ml of 6mol / L sodium hydroxide solution to it , stirred until the solution was separated, the upper layer was yellow, and the lower layer was a colorless transparent liquid. The lower layer of liquid was removed and dried in vacuum to obtain white flaky crystals. Add 2.5g of white flaky crystals to 2.5g of acryloyl chloride, keep the temperature at 0-5°C and stir vigorously to obtain functional monomer 1; the specific chemical reaction formula is as follows:
[0033]
[0034] 2: Preparation of functional monomer 2
[0035] Add 5g of vinylbenzenesulfonic acid, 5g of 4-maleimidophenol and 25ml of DMF solvent into the reactor, and add 2.5g of sodium hydroxide, stir at 40°C for 1 hour, and obtain the functional monomer di ; The specific chem...
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