A kind of fluorescent ceramics and sapphire composite ceramic material and preparation method thereof
A technology of fluorescent ceramics and composite ceramics, applied in chemical instruments and methods, electronic equipment, other household appliances, etc., can solve the problems of low light transmittance, low thermal conductivity and thermal stability, and high density of sapphire and fluorescent ceramics , to achieve the effect of improving scattering and uniformity of outgoing light
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Embodiment 1
[0027] Polish the YAG:Ce fluorescent ceramic on one side to 0.15mm thick, with a surface roughness of 0.01μm; polish the sapphire on one side to 0.2mm, with a surface roughness of 0.01μm; weigh 1 g of YAG:Ce phosphor, 1g of quartz Glass powder, 0.5 g epoxy resin, mixed evenly to obtain phosphor colloid; evenly coated phosphor colloid on the polished surface of fluorescent ceramics, and then bonded with sapphire; placed the composite in an oven at 100 ° C, baked Dry for 2 hours until the colloid in the middle layer is solidified; place the cured composite in a high-temperature muffle furnace for sintering at 1400° C. to obtain the fluorescent ceramic and sapphire composite ceramic material. Using a power density of 5 W / mm 2 The blue laser excitation, ceramic light intensity is 3050lm.
Embodiment 2
[0029] Polish the YAG:Ce fluorescent ceramic on one side to 0.15mm thick, with a surface roughness of 0.02μm; polish the sapphire on one side to 0.2mm, with a surface roughness of 0.04μm; weigh 2 g of YAG:Ce phosphor, 1g of quartz Glass powder, 0.4 g epoxy resin, mixed evenly to obtain phosphor colloid; uniformly coat the phosphor colloid on one side of the fluorescent ceramic, and then bond it with sapphire; place the composite in an oven at 60°C, and dry 2 hours until the colloid in the middle layer is solidified; the cured composite is placed in a high-temperature muffle furnace at 1550° C. for sintering to obtain the fluorescent ceramic and sapphire composite ceramic material. Adopt power density of 100 W / mm 2 The blue laser excitation, the ceramic light intensity is 3102lm.
Embodiment 3
[0031] Polish LuAG:Ce fluorescent ceramics on one side to 0.25 mm, with a surface roughness of 0.04 μm; polish one side of sapphire to 0.2 mm, with a surface roughness of 0.01 μm; weigh 1.5 g of YAG:Ce phosphor powder, 1 g of quartz glass Powder, 0.5 g epoxy resin, mixed evenly to obtain phosphor colloid; uniformly coat the phosphor colloid on one side of the fluorescent ceramic, and then bond it with sapphire; place the composite in an oven at 80°C, and dry for 2 hours until the colloid in the middle layer is solidified; the cured composite is placed in a high-temperature muffle furnace for sintering at 1650° C. to obtain the fluorescent ceramic and sapphire composite ceramic material. Adopt power density of 200 W / mm 2 The blue laser excitation, ceramic light intensity is 2905lm.
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