Target airflow mill and method for preparing economical sintered neodymium iron boron blank

A jet mill, NdFeB technology, applied in electrical components, inductance/transformer/magnet manufacturing, circuits, etc., can solve the problems that powder cannot be used directly, the particle size fluctuates greatly, and the production cost increases. Small particle size, improved magnetic properties, and the effect of saving raw materials

Active Publication Date: 2018-09-28
京磁材料科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In order to obtain high-performance sintered NdFeB magnets, it is required that the crystal grains of the magnets be as small and uniform as possible, and that the peripheries of the crystal grains be evenly wrapped with a layer of neodymium-rich phase as thin as possible. The powder preparation technology is mainly realized by the method of fluidized bed jet mill pulverization. This pulverization method requires a large amount of powders to collide with each other. Under certain conditions, the number of powders is proportional to the probability of collision. Therefore, after pulverization The relationship between the particle size of the powder and the quantity of the powder is very significant. However, in the later stage of crushing, the quantity of powder decreases, and it is bound to produce powder with large particle size fluctuations. This part of the powder with large particle size deviation cannot be directly used. Especially when preparing high-performance sintered NdFeB permanent magnets, they cannot be used directly. In the end, the accumulation of this part of raw materials will cause inevitable waste and greatly increase the production cost.

Method used

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  • Target airflow mill and method for preparing economical sintered neodymium iron boron blank
  • Target airflow mill and method for preparing economical sintered neodymium iron boron blank
  • Target airflow mill and method for preparing economical sintered neodymium iron boron blank

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Effect test

Embodiment 1

[0044] The method for preparing economical sintered NdFeB blanks based on the target jet mill includes: after hydrogen absorption and crushing of NdFeB alloy castings, adding a mixture of zinc stearate and n-hexane, and then mixing them evenly through a powder mixer , to get coarse powder, wherein the total addition of zinc stearate and n-hexane mixture is 1‰ of the quality of the NdFeB alloy casting sheet, and the mass fraction of zinc stearate is 70%; The feed inlet is fed into the housing, and then dispersed nitrogen gas with a pressure of 0.3 MPa is introduced into the dispersed nitrogen flow inlet, and crushed nitrogen gas with a pressure of 0.8 MPa is fed into the crushed nitrogen flow inlet at the same time. After the coarse powder is crushed, first After being screened by the turbine classifier, a fine powder with a particle size of less than 4.5 μm is obtained, and then the fine powder is screened by a cyclone separator to obtain a target powder with a particle size of...

Embodiment 2

[0046] The method for preparing economical sintered NdFeB blanks based on the target jet mill includes: after hydrogen absorption and crushing of NdFeB alloy castings, adding a mixture of zinc stearate and n-hexane, and then mixing them evenly through a powder mixer , to get coarse powder, wherein the total addition of zinc stearate and n-hexane mixture is 0.5‰ of the quality of the NdFeB alloy casting sheet, and the mass fraction of zinc stearate is 50%; The feed inlet is fed into the housing, and then the dispersed nitrogen gas with a pressure of 0.2MPa is fed into the dispersed nitrogen flow inlet, and the pulverized nitrogen gas with a pressure of 0.6MPa is fed into the pulverized nitrogen gas flow inlet at the same time. After the coarse powder is crushed, first After being screened by the turbine classifier, a fine powder with a particle size of less than 4.5 μm is obtained, and then the fine powder is screened by a cyclone separator to obtain a target powder with a parti...

Embodiment 3

[0048] The method for preparing economical sintered NdFeB blanks based on the target jet mill includes: after hydrogen absorption and crushing of NdFeB alloy castings, adding a mixture of zinc stearate and n-hexane, and then mixing them evenly through a powder mixer , to get coarse powder, wherein, the total addition of zinc stearate and n-hexane mixture is 0.3‰ of the quality of the NdFeB alloy casting sheet, and the mass fraction of zinc stearate is 30%; The feed inlet is fed into the housing, and then dispersed nitrogen gas with a pressure of 0.1MPa is introduced into the dispersed nitrogen flow inlet, and crushed nitrogen gas with a pressure of 0.4MPa is fed into the crushed nitrogen flow inlet at the same time. After the coarse powder is crushed, first After being screened by the turbine classifier, a fine powder with a particle size of less than 4.5 μm is obtained, and then the fine powder is screened by a cyclone separator to obtain a target powder with a particle size o...

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Abstract

The invention discloses a target airflow mill, comprising: a housing vertically arranged, the lower part of the side wall of the housing being provided with a downward inclined feed opening and at least one horizontal dispersed nitrogen flow inlet, and the center of the bottom of the housing being provided with a pulverized nitrogen flow inlet; and an impact path pipe coaxially fixed in the housing, the impact path pipe comprising a thick pipe section and a thin pipe section integrally formed and connected from top to bottom, and an alloy target being coaxially fixed in the thick pipe section.Also provided is a method for preparing an economical sintered neodymium iron boron blank, comprising the steps of: crushing a neodymium iron boron alloy casting piece to obtain coarse powder; feeding the coarse powder into the housing, introducing dispersed nitrogen and crushed nitrogen, and crushing and screening the coarse powder to obtain target powder; and preparing a blank from the target powder. The method can prepare small-sized and uniform neodymium iron boron powder and a blank with good magnetic properties, and can save raw materials and reduce the production cost.

Description

technical field [0001] The invention relates to a jet mill and a method for preparing NdFeB blanks. More specifically, the present invention relates to a target jet mill and a method for preparing economical sintered NdFeB blanks. Background technique [0002] In order to obtain high-performance sintered NdFeB magnets, it is required that the crystal grains of the magnets be as small and uniform as possible, and that the peripheries of the crystal grains be evenly wrapped with a layer of neodymium-rich phase as thin as possible. The powder preparation technology is mainly realized by the method of fluidized bed jet mill pulverization. This pulverization method requires a large amount of powders to collide with each other. Under certain conditions, the number of powders is proportional to the probability of collision. Therefore, after pulverization The relationship between the particle size of the powder and the quantity of the powder is very significant. However, in the lat...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01F41/02B22F9/04
CPCB22F9/04B22F2009/044H01F41/0253
Inventor 刘润海刘月玲马驰
Owner 京磁材料科技股份有限公司
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