Preparation method of multifunctional metal/metallic glass blended fabric with enhanced stretching
A technology of metallic glass and blended fabrics, applied in textile, textile, papermaking, fabrics and other directions, can solve the problems of hindering the slippage of the main shear belt, unstable metallic glass fibers, etc. The effect of elongation at break
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[0024] Example 1:
[0025] (1) Pd powder with purity ≥99.9%, Cu powder with purity ≥99.9%, Ni powder with purity ≥99.9% and P powder with purity ≥99.9% with a mass ratio of 35:25:10:15 at 0.03MPa Under vacuum conditions, first heat up to 900°C, hold for 5 minutes, then heat to 1600°C, hold for 15 minutes, cool to 1000°C, hold for 10 minutes, then heat up to 1450°C, hold for 20 minutes, and then place it at room temperature to obtain the master alloy , The master alloy was crushed into pieces and added to the 10mg / mL graphene oxide aqueous solution, mixed evenly, stirred to volatilize the solvent to obtain a graphene oxide modified metallic glass mixture, where the graphene oxide modified metallic glass mixture was oxidized The content of graphene is 0.01 wt%.
[0026] (2) Add the graphene oxide-modified metallic glass mixture to the vacuum heating and curing equipment in batches, and under an inert gas atmosphere, all the metallic glass mixtures to be modified by graphene oxide ar...
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[0030] Example 2:
[0031] (1) Pd powder with a purity of ≥99.9%, Cu powder with a purity of ≥99.9%, Ni powder with a purity of ≥99.9% and P powder with a purity of ≥99.9% with a mass ratio of 42:30:15:20 at 0.05MPa Under vacuum conditions, first raise the temperature to 1000°C, after holding for 10 minutes, then heating to 1650°C, after holding for 20 minutes, cooling to 1050°C, after holding for 15 minutes, then raising to 1550°C, holding for 30 minutes, and then placing it at room temperature to obtain the master alloy , The master alloy was crushed into pieces and added to the 15mg / mL graphene oxide aqueous solution, after mixing uniformly, stirred to volatilize the solvent to obtain a graphene oxide modified metallic glass mixture, where the graphene oxide modified metallic glass mixture was oxidized The content of graphene is 0.05 wt%.
[0032] (2) Add the graphene oxide-modified metallic glass mixture to the vacuum heating curing equipment in batches, and under an inert gas...
Example Embodiment
[0036] Example 3:
[0037] (1) Pd powder with a purity of ≥99.9%, Cu powder with a purity of ≥99.9%, Ni powder with a purity of ≥99.9% and P powder with a purity of ≥99.9% with a mass ratio of 40:27:10:18 at 0.04MPa Under vacuum conditions, first heat up to 950°C, heat up for 6 minutes, then heat up to 1620°C, after hold for 18 minutes, cool down to 1030°C, heat up for 14 minutes, then heat up to 1500°C, hold for 25 minutes, and place it at room temperature to obtain the master alloy , The master alloy was crushed into pieces and added to the 13mg / mL graphene oxide aqueous solution. After mixing evenly, the solvent was stirred and volatilized to obtain a graphene oxide-modified metallic glass mixture, where the graphene oxide-modified metallic glass mixture was oxidized The content of graphene is 0.03wt%.
[0038] (2) Add the graphene oxide-modified metallic glass mixture to the vacuum heating curing equipment in batches, and under an inert gas atmosphere, all the metallic glass m...
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