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Colla carapacis preparation process

A preparation process and technology of tortoise shell glue, applied in medical preparations containing active ingredients, blood diseases, extracellular fluid diseases, etc. Effect

Active Publication Date: 2018-10-23
河北君临药业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The above-mentioned methods 1, 2 and 4 have the disadvantage of long operating time, while method 3 will inevitably affect the amino acid content in the tortoise shell during steaming and brushing.

Method used

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  • Colla carapacis preparation process

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Raw material ratio:

[0032] Tortoise shell 250kg, soybean oil 2.6kg, rock sugar 2.4kg, rice wine 1.0kg

[0033] Preparation Process:

[0034] S1 Tortoise shell pre-treatment: Select a dry tortoise shell, use 40% NaOH solution to smear the carrion of the tortoise shell, the smear is based on the full coverage, after ultrasonic treatment with a frequency of 150KHz for 5 minutes, microwave treatment with a power of 0.8KW for 1.5 minutes, take it out, Repeat the above operation for 2 more times, after the last microwave treatment, put it into clean water, and after 100KHz ultrasonic treatment for 5min, wash it;

[0035] S2 is crushed, and the tortoise shell cleaned by S1 is frozen at -48°C, crushed at a low temperature, ground, and passed through an 80-mesh sieve to obtain tortoise shell powder;

[0036] S3 extraction: add water to the tortoise shell powder obtained in S2, boil the glue juice, add 1.4 times of water for the first time, boil the glue juice for 5 hours, fi...

Embodiment 2

[0044] Raw material ratio:

[0045] Tortoise shell 250kg, soybean oil 2.6kg, rock sugar 2.4kg, rice wine 1.0kg

[0046] Preparation Process:

[0047] S1 Tortoise shell pre-treatment: Select a dry tortoise shell, use 50% NaOH solution to smear the carrion of the tortoise shell, the smear is based on the full coverage, after ultrasonic treatment with a frequency of 200KHz for 5 minutes, microwave treatment with a power of 0.5KW for 1 minute, take it out, and then Repeat the above operation 2 times, after the last microwave treatment, put it into clean water, after 100KHz ultrasonic treatment for 5min, wash;

[0048] S2 is crushed, and the tortoise shell cleaned by S1 is frozen at -48°C, crushed at a low temperature, ground, and passed through an 80-mesh sieve to obtain tortoise shell powder;

[0049] S3 extraction: add water to the tortoise shell powder obtained in S2, boil the glue juice, add 1.2 times of water for the first time, boil the glue juice for 3 hours, filter the g...

Embodiment 3

[0057] Raw material ratio:

[0058] Tortoise shell 250kg, soybean oil 2.6kg, rock sugar 2.4kg, rice wine 1.0kg

[0059] Preparation Process:

[0060] S1 Tortoise shell pre-treatment: Select a dry tortoise shell, use 20% NaOH solution to smear the carrion of the tortoise shell, and the smear is based on the full coverage. After ultrasonic treatment with a frequency of 80KHz for 5 minutes, microwave treatment with a power of 8KW for 2 minutes, take it out, and repeat. The above operation was performed twice, after the last microwave treatment, put it into clean water, and after 100KHz ultrasonic treatment for 5 minutes, wash it;

[0061] S2 is crushed, and the tortoise shell cleaned by S1 is frozen at -48°C, crushed at a low temperature, ground, and passed through an 80-mesh sieve to obtain tortoise shell powder;

[0062] S3 extraction: add water to the tortoise shell powder obtained in S2, boil the glue juice, add 1.6 times of water for the first time, boil the glue juice for...

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Abstract

The invention relates to a colla carapacis preparation process. The colla carapacis preparation process includes steps: S1, carapax et plastrum testudinis pretreatment; S2, crushing; S3, extracting; S4, gelatin combining; S5, separating and concentrating; S6, skimming; S7, blending, collecting and gelling; S8, cutting and airing. The step of carapax et plastrum testudinis pretreatment includes: applying NaOH solution to carrion parts of carapax et plastrum testudinis, performing ultrasonic treatment for 5min and microwave treatment for 1-2min, repeating for 2-3 times, putting into clear waterafter the last-time microwave treatment is finished, ultrasonically treating for 5min, and cleaning. By adoption of the colla carapacis preparation process, the colla yield of carapax et plastrum testudinis can be effectively increased, and time shortening and product quality improvement are realized. A novel method is provided for colla carapacis preparation.

Description

technical field [0001] The invention relates to a preparation process of tortoise shell glue. Background technique [0002] Tortoise shell glue is a solid glue made from the plastron and carapace of turtles, dried in the sun, decocted, and concentrated. Its output is low, but its medicinal value is quite high. The effect of bone, and concurrently enriches blood and stops bleeding. [0003] The pretreatment step of removing the residual meat of the tortoise shell has a direct impact on the gelling rate of the tortoise shell. The methods disclosed in the prior art are as follows: 1. Soaking: soak the tortoise shell in clear water for 24 days in summer and 40 days in winter without changing the water When the skin, flesh and fascia are rotten and easily separated from the tortoise shell, take it out, wash it with clean water, and expose it to the sun and night until it has no odor. 2. Fermentation: CN103432170 discloses a method for boiling tortoise shell glue. Put the tortoi...

Claims

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Application Information

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IPC IPC(8): A61K35/586A61P7/04A61P7/06
CPCA61K35/586A61P7/04A61P7/06
Inventor 王红杰冯朝李新联郭峰张丽娟候少璞
Owner 河北君临药业有限公司
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