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Rapid demulsifying agent for emulsified explosive and application thereof

A technology of emulsified explosives and demulsifiers, which is applied in the direction of non-explosive/non-thermal agent components, explosives, offensive equipment, etc. It can solve the problems of dangerous measurement, long time spent, and difficulty in ensuring accurate results, etc., to achieve simple and convenient application, The effect of improving safety and ensuring safety

Inactive Publication Date: 2018-11-23
JIANGXI GANZHOU GUOTAI SPECIALTY CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the safety of demulsification and demulsification, everyone is most concerned about the speed of demulsification, that is, after the emulsion explosive is mixed with the demulsifier, it is required to change the form of the emulsion explosive as soon as possible, so as to achieve demulsification and demulsification. The improved demulsifier has indeed improved the demulsification speed to a certain extent, but it still cannot meet the demulsification speed required by the industry
For today's demulsifiers, after mixing with emulsion explosives, it generally takes 1-2 hours to change the form of emulsion explosives and complete demulsification and detonation. This is far from meeting the requirements of rapid demulsification. Therefore, in the emulsion explosives production industry In order to improve the safety of demulsification and explosive demulsification, it is urgent to develop a demulsifier that can realize rapid emulsion explosive
[0005] In addition, the determination of the content of ammonium nitrate in emulsion explosives or emulsion matrix has always been a pain point, and it is difficult to ensure that the determination of ammonium nitrate components can be accurately and quickly achieved in a completely safe situation, that is, the current emulsion explosives or emulsion matrix The determination of the content of ammonium nitrate components in the medium is generally carried out under the condition of incomplete demulsification and elimination of explosion. The demulsification and detonation of the time, the follow-up measurement is difficult to ensure the accuracy of the results, and it takes a long time, so it is difficult to accurately detect the power of the emulsion explosive, and cannot fully guarantee the safety of the emulsion explosive

Method used

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  • Rapid demulsifying agent for emulsified explosive and application thereof
  • Rapid demulsifying agent for emulsified explosive and application thereof
  • Rapid demulsifying agent for emulsified explosive and application thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0022] Demulsifier 1 for emulsion explosives, the volume ratio of its components is: absolute ethanol: anhydrous petroleum ether = 1: 1.5. According to the volume ratio, mix absolute ethanol and anhydrous petroleum ether evenly to obtain demulsifier 1.

Embodiment 2

[0024] Demulsifier II for emulsion explosives, the volume ratio of its components is: absolute ethanol: anhydrous petroleum ether = 1.25: 1.5. According to the volume ratio, mix absolute ethanol and anhydrous petroleum ether evenly to obtain demulsifier 2.

Embodiment 3

[0026] Demulsifier III for emulsion explosives, the volume ratio of its components is: absolute ethanol: anhydrous petroleum ether = 1:1. According to the volume ratio, mix absolute ethanol and anhydrous petroleum ether evenly to obtain demulsifier 3.

[0027] Test comparison and results:

[0028] Demulsifier 1, demulsifier 2, demulsifier 3 obtained respectively, and the sample demulsifier 4 obtained under the existing common formula and preparation method, respectively take 60ml of these four kinds of demulsifiers, and then take an equal amount of demulsifier 4 Parts of consistent emulsion explosives 2g, and four parts of emulsion explosives were dropped into four parts of demulsifiers respectively, and the change form of four parts of emulsion explosives was tested to realize the time of demulsification and detonation.

[0029] From the experimental data, it can be concluded that the demulsifier 1 changes the form of the emulsion explosive, so that the time to achieve demul...

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Abstract

The invention discloses a rapid demulsifying agent for emulsified explosive and application thereof. The demulsifying agent is prepared from the following components according to the volume ratio: theratio of absolute ethyl alcohol to anhydrous petroleum ether is (1 to 1.5) to 1.5. The application of the demulsifying agent comprises the specific steps: weighing a test sample of the emulsified explosive or an emulsified matrix; adding the demulsifying agent into the test sample and uniformly stirring; adding a neutral formaldehyde solution and water into the test sample; dropwise adding an acid-base indicator and carrying out titration, so as to obtain the mass percent concentration C(NH4NO3)=0.1*V*0.08004*20 / M*100% of ammonium nitrate in the emulsified explosive or the emulsified matrix;the demulsifying agent can realize rapid demulsifying and detonation elimination of the emulsified explosive and the safety of the demulsifying and detonation elimination is improved; meanwhile, the invention also provides the application of the demulsifying agent; the component content of the ammonium nitrate in the emulsified explosive or the emulsified matrix can be rapidly and accurately determined, so that the power of the emulsified explosive is accurately detected, and furthermore, the needed utilization amount of different occasions is reasonably calculated and the utilization safety of the emulsified explosive is ensured.

Description

Technical field [0001] The invention relates to a demulsifier for emulsion explosives, and in particular to a rapid demulsifier for emulsion explosives and its application. Background technique [0002] Emulsion explosives use the action of emulsifiers to evenly disperse droplets of oxidants and salt aqueous solutions in an oil phase continuous medium containing porous materials such as dispersed bubbles or hollow glass beads, forming a water-in-oil (W / O ) emulsion-like water-containing industrial explosive is a new type of industrial explosive developed in the 1970s. The earliest emulsion explosives were non-detonator sensitive and had to be detonated with the help of relay detonators. Later, with the in-depth research on emulsion explosives, the emulsion explosives developed later also had detonator sensitivity and good water resistance. At the same time, it has the advantages of good explosive performance, low mechanical sensitivity and good safety. At the same time, the...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C06B23/00C06B31/28
CPCC06B23/00C06B31/28
Inventor 卢志坚何厚金侯成举李祖全
Owner JIANGXI GANZHOU GUOTAI SPECIALTY CHEM
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