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Preparation method of indium tin oxide transparent heat-insulation paint

A technology of thermal insulation coating and indium tin oxide, which is applied in the field of materials, can solve the problems of low light transmittance, low compatibility of matrix resin, poor dispersibility, etc., and achieves broad application prospects, high light transmittance and good thermal insulation performance. Effect

Inactive Publication Date: 2018-12-11
张家港市东威新材料技术开发有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The key to transparent thermal insulation coatings is the nano-semiconductor material that is selective to sunlight. At present, it is mainly tin antimony oxide. Among them, tin antimony oxide has become an acceptable product in the market due to its relatively low cost, but tin antimony oxide is due to its special nanometer Structural properties, there are problems of easy agglomeration, poor dispersion and low compatibility with the matrix resin, resulting in poor heat insulation effect and low light transmittance of the final heat insulation coating

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0022] A preparation method of indium tin oxide transparent heat-insulating paint, comprising:

[0023] (1) In parts by weight: add 10 to 20 parts of deionized water to 20 to 30 parts of nano-indium tin oxide, and grind for 30 minutes in a grinder at 400 to 800 r / min to obtain a nano-indium tin oxide slurry;

[0024] (2) Weigh the following raw materials according to the composition in parts by weight: 50-150 parts of water-based polyurethane, 1-3 parts of hollow glass microspheres, 2-5 parts of thickener, 1-2 parts of leveling agent, at 1000-2000r / min Stir and disperse for 10 to 30 minutes under the condition of rotating speed, then add 0.5 to 1.5 parts of defoamer, and continue to stir for 5 to 15 minutes to obtain a coating precursor;

[0025] (3) Mix the nano-indium tin oxide slurry in step (1) with the coating precursor in step (2) at a weight ratio of 1:30 to 80, then add 1 to 3 parts of dispersant, and ultrasonically disperse 1 to 2 hours to obtain indium tin oxide tra...

Embodiment 1

[0032] (1) In parts by weight: add 10 parts of deionized water to 20 parts of nano-indium tin oxide with a particle size of 5 nm, and grind for 30 minutes in a grinder at 400 r / min to obtain a nano-indium tin oxide slurry;

[0033] (2) Weigh the following raw materials according to the composition in parts by weight: 50 parts of water-based polyurethane, 1 part of hollow glass microspheres, 2 parts of thickener, 1 part of leveling agent, stir and disperse at 1000r / min for 10min, then add disinfectant 0.5 parts of foaming agent, continue to stir for 5 minutes to obtain the coating precursor;

[0034] (3) Mix the nano-indium tin oxide slurry in step (1) with the coating precursor in step (2) at a weight ratio of 1:30, then add 1 part of dispersant, and ultrasonically disperse for 1 hour to obtain oxidized Indium tin transparent thermal insulation coating.

Embodiment 2

[0036] (1) In parts by weight: add 12.5 parts of deionized water to 25 parts of nano-indium tin oxide with a particle diameter of 10 nm, and grind for 30 min in a grinder at 600 r / min to obtain a nano-indium tin oxide slurry;

[0037] (2) Weigh the following raw materials according to the composition in parts by weight: 80 parts of water-based polyurethane, 1.5 parts of hollow glass microspheres, 3 parts of thickener, 1.3 parts of leveling agent, stir and disperse at 1500r / min for 20min, then add disinfectant 0.8 parts of foaming agent, continue stirring for 10 minutes to obtain a coating precursor;

[0038] (3) Mix the nano-indium tin oxide slurry in step (1) with the coating precursor in step (2) according to the weight ratio of 1:50, then add 2 parts of dispersant, and ultrasonically disperse for 1.5h to obtain Indium tin oxide transparent thermal insulation coating.

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Abstract

The invention discloses a preparation method of indium tin oxide transparent heat-insulation paint. The preparation method comprises the following steps: (1) based on parts by weight: adding 10 to 20parts of de-ionized water into 20 to 30 parts of nano indium tin oxide; grinding for 30min in a grinding machine with the speed of 400 to 800r / min, so as to obtain nano indium tin oxide slurry; (2) weighing the following raw materials in parts by weight: 50 to 150 parts of waterborne polyurethane, 1 to 3 parts of hollow glass beads, 2 to 5 parts of a thickening agent and 1 to 2 parts of a flattingagent; stirring and dispersing for 10 to 30min under the condition that the rotary speed is 1000 to 2000r / min; then adding 0.5 to 1.5 parts of a de-foaming agent and continually stirring for 5 to 15min to obtain a paint precursor; (3) mixing the nano indium tin oxide slurry in step (1) and the paint precursor in step (2) according to the weight ratio of 1 to (30 to 80); then adding 1 to 3 parts of a dispersant and carrying out ultrasonic dispersion for 1 to 2h to obtain the indium tin oxide transparent heat-insulation paint. The paint disclosed by the invention has relatively good heat insulation performance and also has high light transmittance and has a wide application prospect when being applied to building glass or automobile glass.

Description

technical field [0001] The invention relates to the field of material technology, in particular to a preparation method of indium tin oxide transparent heat-insulating paint. Background technique [0002] With the development of economy, the global demand for energy is increasing day by day. In the ever-increasing total energy consumption, building energy consumption is relatively large. The development of building energy-saving materials is the fundamental way of building energy conservation. For buildings, the heat lost through doors and windows accounts for about 50% of the heating and air conditioning energy consumption of the entire building. However, 60% of the heat loss through ordinary windows is transmitted by infrared rays. Therefore, after the heat convection and conduction of doors and windows are controlled, reducing infrared radiation becomes particularly important. [0003] As a new energy-saving material, transparent insulating water-based nano-coating can...

Claims

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Application Information

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IPC IPC(8): C09D175/04C09D7/61
CPCC08K2003/2231C08K2201/011C08L2201/10C08L2205/03C09D7/61C09D7/70C09D175/04C08L33/02C08L71/02C08K7/28C08K3/22
Inventor 赵云龙
Owner 张家港市东威新材料技术开发有限公司
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