Kit for detecting multiple mutation sites of KRAS gene
A technology for detecting kits and mutation sites, which is applied in the fields of molecular biotechnology and genetic testing, can solve the problems of wasting treatment costs, KRAS mutant patients cannot benefit, and delay treatment, so as to reduce complexity and reduce primers and probes Interaction and the effect of reducing the cost of detection reagents
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Embodiment 1
[0031] The detection principle of embodiment 1 Kras gene multiple mutation detection kit (see figure 1 )
[0032] A pair of PCR primers are designed to amplify the target region of the KRAS gene mutation site to amplify the target region to be detected. Targeted design of a shared auxiliary probe, design of detection probes for each hot spot mutation, and labeling of fluorescent groups and quenching groups. At the same time, in order to further increase the specificity, the specific probe also introduces LNA bases to increase the binding specificity of the probe and increase the difference with the wild probe. In the reaction, the auxiliary probe and the detection probe can anneal and hybridize with the amplified target template to form a single-base overlapping intrusion structure, which can be specifically recognized by the Afu enzyme, thereby cutting the first base complementary to the template of the detection probe base chemical bonds, resulting in signal molecules. Si...
Embodiment 2
[0049] The sensitivity of embodiment 2 Kras gene multiple mutation detection kit
[0050] In this example, KRAS gene mutation DNA templates with different concentrations and gene mutation percentages were detected using the Kras gene multiple mutation detection kit, which was used to verify the sensitivity of the kit of the present invention. The detected hot spot mutation c.34G> A is used as an example for sensitivity verification.
[0051] Reaction conditions:
[0052] 40μL amplification system includes: 4μL 10×buffer, 200-500μmol / L dNTP, 200-500nmol / LPCR upstream and downstream primers and probes (SEQ ID NO.1 to SEQ ID NO.11), 3U Taq DNA polymerase, 60U Afu enzyme and template DNA. Taking the detected hotspot mutation c.34G>A as an example, the added template is the kit reference product whose concentration is determined by a UV spectrophotometer, and the mutation percentage is determined by mixing the corresponding mutant plasmid and the reference copy number ratio of hu...
Embodiment 3
[0054] Example 3 Validation Results of Different Combination Probe Systems of Kras Gene Multiple Mutation Detection Kit
[0055] This example is to verify that the Kras gene multiple mutation detection kit can be flexibly combined to detect specific Kras gene mutation sites. The combination of the hot spot mutation sites shown in Table 2 is used as an example to verify the results under the conditions of the quadruple system. Single detection to determine the detection accuracy of the kit of the present invention.
[0056] In order to better verify the flexibility and accuracy of the detection kit of the present invention, taking the hot spot mutation site shown in Table 2 as an example, the quadruple mutation probe system detects the corresponding four target templates respectively, and simultaneously prepares each hot spot mutation The detection system detects the corresponding single target template.
[0057] Reaction conditions:
[0058] 40μL amplification system include...
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