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Wear-resistant transparent flame-retardant polycarbonate material and preparation method thereof

A technology of flame-retardant polycarbonate and polycarbonate, which is applied in the field of wear-resistant transparent flame-retardant polycarbonate material and its preparation, can solve the problems of affecting the light transmittance of the material and reducing the mechanical properties, so as to achieve good reinforcement effect and improve The effects of mechanical properties and light transmittance are small

Active Publication Date: 2018-12-25
PUYANG SHENGTONGJUYUAN ADVANCED MATERIALS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When the added amount reaches the ideal flame retardant effect, it will reduce the original mechanical properties of the material to a certain extent, and at the same time affect the light transmittance of the material.

Method used

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  • Wear-resistant transparent flame-retardant polycarbonate material and preparation method thereof

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Effect test

preparation example Construction

[0027] The preparation method of the transparent flame retardant masterbatch includes the steps of: adding all raw material components into a high-speed mixer with a rotation speed of 700-800r / min and mixing for 10-30min to obtain a mixture; The diameter ratio is (36-40):1, and the barrel temperature is 220-240 ° C in a twin-screw extruder, melted and mixed for 10-15 minutes under the protection of nitrogen, and then extruded and granulated to obtain a transparent flame-retardant masterbatch .

[0028]The invention provides a wear-resistant transparent flame-retardant polycarbonate material. The raw material components include: 90-95 parts by weight of polycarbonate, 5-10 parts by weight of transparent flame-retardant masterbatch, ZnO / SiO 2 0.5-1 weight part of the nanocomposite, 0.1-1 weight part of the antioxidant and 1-3 ppm of the coloring agent.

[0029] Among them, the polycarbonate is a bisphenol A type aromatic polycarbonate with a weight average molecular weight of 2...

Embodiment 1

[0037] This embodiment provides a transparent flame retardant masterbatch, the raw material components are calculated by weight, including: 85 parts of siloxane copolycarbonate, 8 parts of phosphorus flame retardant, 3 parts of heat stabilizer and 2 parts of dispersant; Among them, the siloxane copolycarbonate is a transparent siloxane copolycarbonate with a silicon content of 3% and a weight average molecular weight of 20,000 to 30,000; the phosphorus-based flame retardant is made of resorcinol-bis(diphenylphosphoric acid ester) and bisphenol A-bis(diphenyl phosphate) in a weight ratio of 1:1; the heat stabilizer is 2,4-bis[(dodecylthio)methyl]-6- methylphenol (DD); the dispersant is polyethylene wax;

[0038] The preparation method of the transparent flame retardant masterbatch includes the steps of: adding all raw material components into a high-speed mixer with a rotation speed of 750r / min and mixing for 10 minutes to obtain a mixture; putting the mixture into a 1. In a t...

Embodiment 2

[0042] This embodiment provides a transparent flame retardant masterbatch. The raw material components are calculated in parts by weight, including: 90 parts of siloxane copolycarbonate, 5 parts of phosphorus flame retardant, 2 parts of heat stabilizer and 1 part of dispersant; Among them, the siloxane copolycarbonate is a transparent siloxane copolycarbonate with a silicon content of 3% and a weight average molecular weight of 20,000 to 30,000; the phosphorus-based flame retardant is made of resorcinol-bis(diphenylphosphoric acid ester) and bisphenol A-bis(diphenyl phosphate) in a weight ratio of 1:1; the heat stabilizer is 2,4-bis[(dodecylthio)methyl]-6- methylphenol (DD); the dispersant is polyethylene wax;

[0043] The preparation method of the transparent flame retardant masterbatch includes the steps of: adding all raw material components into a high-speed mixer with a rotation speed of 700r / min and mixing for 30 minutes to obtain a mixture; 1. In a twin-screw extruder ...

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Abstract

The invention relates to a wear-resistant transparent flame-retardant polycarbonate material and a preparation method thereof. The wear-resistant transparent flame-retardant polycarbonate material comprises the following raw materials in parts by weight: 90-95 parts of polycarbonate, 5-10 parts of transparent flame-retardant masterbatches, 0.5-1 part of ZnO / SiO2 nano composite and 0.1-1 part of anantioxidant. The prepared polycarbonate material has high flame retardancy, high light transmitting rate and good wear resistance, and the other original mechanical properties of the material can beimproved. The flame-retardant masterbatches serve as the raw material components, the consistency is good, and the quality of the product is uniform and stable; and a double-screw extruder serves as processing equipment, and the technological process is simple and continuous.

Description

technical field [0001] The invention relates to the technical field of polycarbonate modified materials, in particular to a wear-resistant transparent flame-retardant polycarbonate material and a preparation method thereof. Background technique [0002] Polycarbonate is a heat-shrinkable engineering plastic with excellent comprehensive properties. It has high light transmittance, high impact resistance, high toughness, high heat resistance, weather resistance and excellent electrical insulation. It is widely used in the automotive industry, Instrumentation, electronic appliances and other fields. Polycarbonate itself has a certain degree of flame retardancy, but it cannot meet the occasions that require a higher level of flame retardancy. At the same time, polycarbonate has poor wear resistance. [0003] In order to ensure flame retardancy, the traditional addition of halogen-containing flame retardants has good flame retardancy, less addition, and less impact on mechanical...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L69/00C08K13/06C08K9/06C08K3/22C08K3/36C08K5/523C08J3/22
CPCC08J3/226C08J2369/00C08J2469/00C08K2003/2296C08K2201/003C08K2201/011C08K2201/014C08L69/00C08L2201/02C08L2201/10C08L2205/03C08K13/06C08K9/06C08K3/22C08K3/36C08K5/523
Inventor 殷鹏刚郭胜立史吉华
Owner PUYANG SHENGTONGJUYUAN ADVANCED MATERIALS CO LTD
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