A kind of compound and its preparation method and application in cosmetics
A compound and target compound technology, applied in the field of new compounds and their preparation, can solve the problems of uneven quality of whitening cosmetics
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Embodiment 1
[0061] (1) Weigh 1 kg of dried leaves of Paleum chinensis, crush them, add 10L of 75% ethanol for reflux extraction, and concentrate the extract to obtain the crude extract;
[0062] (2) The crude extract extract was dispersed in 1L of water, extracted three times with an equal volume of chloroform, collected the chloroform extract, and concentrated to obtain the chloroform extract;
[0063] (3) Extract the extract with chloroform, separate it with a silica gel column, first elute with chloroform-methanol (50:1) for 10 column volumes, discard the eluent, and then use chloroform-methanol ( 20:1) to elute 10 column volumes, collect the eluate, and concentrate it into an extract;
[0064] (4) The extract obtained in step (3) is further separated by preparative high performance liquid chromatography, wherein the high performance liquid chromatography conditions are: C18 chromatographic column, the mobile phase is 75% methanol for elution, and the eluent is recovered. That is, the...
Embodiment 2
[0066] ((1) Weigh 1 kg of dried leaves of Paleopsis chinensis, crush them, add 10L of 75% ethanol for reflux extraction, and concentrate the extract to obtain the crude extract;
[0067] (2) The crude extract extract was dispersed in 1L of water, extracted three times with an equal volume of chloroform, collected the chloroform extract, and concentrated to obtain the chloroform extract;
[0068] (3) Extract the extract with chloroform, separate it with a silica gel column, first elute with chloroform-methanol (50:1) for 10 column volumes, discard the eluent, and then use chloroform-methanol ( 20:1) to elute 10 column volumes, collect the eluate, and concentrate it into an extract;
[0069] (4) The extract obtained in step (3) is further separated by preparative high performance liquid chromatography, wherein the high performance liquid chromatography conditions are: C18 chromatographic column, the mobile phase is 75% methanol for elution, and the eluent is recovered. That is,...
PUM
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