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Halogen-free and flame-retardant glass fiber reinforced nylon composite and preparation method thereof

A nylon composite material and glass fiber technology, which is applied in the field of halogen-free flame-retardant glass fiber reinforced nylon composite material and its preparation, can solve the problems of material mechanical property loss and achieve the effect of guaranteed strength and excellent flame-retardant effect

Inactive Publication Date: 2019-01-18
HEFEI GENIUS NEW MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in order to ensure the flame retardancy of the product, the mechanical properties of the material have a certain degree of loss.

Method used

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  • Halogen-free and flame-retardant glass fiber reinforced nylon composite and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Weigh 50 parts of dry PA-M1013B, 15 parts of PPS-MT9320C0, 15 parts of halogen-free flame retardant compounding agent (10 parts of red phosphorus flame retardant masterbatch, 2 parts of cyanuric acid melamine salt and organic nano-montmorillonite soil 2 parts), 0.1 part of antioxidant 1098, 0.1 part of antioxidant 168, 5 parts of compatibilizer POE-G, 0.2 part of lubricant EBS, mixed and added to the extruder, and then 15 parts of ER14-1000- 988A is added from the glass fiber port, extruded through the extruder, water-cooled and cut into pellets. Among them, the processing temperature of the extruder is 220°C, 260°C, 270°C, 280°C, 290°C, 295°C from the feeding port to the die port, the main engine speed is 180rpm, and the vacuum degree is -0.03MPa.

Embodiment 2

[0029] Weigh 45 parts of dry PA-M1013B, 5 parts of PPS-MT9320C0, 15 parts of halogen-free flame retardant compounding agent (10 parts of red phosphorus flame retardant masterbatch, 2 parts of cyanuric acid melamine salt and organic nano-membrane 2 parts of soil removal), 0.1 part of antioxidant 1010, 0.1 part of antioxidant 168, 5 parts of compatibilizer POE-G, 0.5 part of lubricant Lico Wax E, mixed and added to the extruder, and then 30 parts ER14-1000-988A is added from the glass fiber inlet; extruded through the extruder, water-cooled and cut into pellets. Among them, the processing temperature of the extruder is 220°C, 260°C, 270°C, 280°C, 290°C, 295°C from the feeding port to the die port, the speed of the main machine is 200rpm, and the vacuum degree is -0.05MPa.

Embodiment 3

[0031] Weigh 39 parts of dry PA-Alphalon 27, 15 parts of PPS-MT9320C0, 25 parts of halogen-free flame retardant compounding agent (15 parts of red phosphorus flame retardant masterbatch, 5 parts of melamine cyanurate and organic nano 5 parts of montmorillonite), 0.1 part of antioxidant 1098, 0.2 part of antioxidant 168, 1 part of compatibilizer POE-G, 0.3 part of lubricant A-C540A, mixed and added to the extruder, and then 20 parts ER14-1000-988A is added from the glass fiber inlet; extruded through the extruder, water-cooled and cut into pellets. Among them, the processing temperature of the extruder is 220°C, 260°C, 270°C, 280°C, 290°C, 295°C from the feeding port to the die port, the main engine speed is 350rpm, and the vacuum degree is -0.05MPa.

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Abstract

The invention discloses a halogen-free and flame-retardant glass fiber reinforced nylon composite and a preparation method thereof, and belongs to the field of production of halogen-free and flame-retardant reinforced nylon and polyphenylene sulfide composites. The halogen-free and flame-retardant glass fiber reinforced nylon composite is prepared from 25-50 parts of nylon, 5-15 parts of polyphenylene sulfide, 10-30 parts of glass fiber, 15-25 parts of a halogen-free and flame-retardant mixture, 1-5 parts of a compatilizer, 0.1-0.3 parts of an antioxidant and 0.1-0.5 parts of a lubricant by mixing and extruding. The halogen-free and flame-retardant mixture is prepared from flame-retardant red phosphorus masterbatch, melamine cyanurate and organic nano-montmorillonite in a mass ratio being5:1:1-5:3:3 by compounding. By compounding polyphenylene sulfide and nylon, hardness, wear resistance and creep resistance of the material are improved; meanwhile, flame retardance of the composite isimproved by the halogen-free and flame-retardant mixture, oxygen index reaches 28 or higher, and finally, the halogen-free and flame-retardant glass fiber reinforced nylon composite product with excellent combination property is obtained.

Description

technical field [0001] The invention belongs to the technical field of polymer composite materials, and in particular relates to a halogen-free flame-retardant glass fiber reinforced nylon composite material and a preparation method thereof. technical background [0002] In view of the current electronic and electrical market, in order to meet market needs, higher requirements are put forward on the strength, rigidity, impact resistance, flame retardancy and other aspects of engineering plastic products. [0003] Materials such as reinforced nylon and flame-retardant reinforced nylon have been developed one after another. However, in order to ensure the flame retardancy of the product, the mechanical properties of the material are lost to a certain extent. [0004] As a new high-performance engineering plastic, polyphenylene sulfide has the characteristics of high strength, good wear resistance, excellent creep resistance, high temperature resistance, chemical resistance, f...

Claims

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Application Information

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IPC IPC(8): C08L77/02C08L77/06C08L81/02C08L51/06C08K13/06C08K9/04C08K3/34C08K3/02C08K5/3492C08K7/14B29B9/06B29C48/92
CPCB29B9/06C08K2003/026C08K2201/003C08K2201/011C08L77/02C08L77/06C08L2201/02C08L2201/22C08L2203/20C08L2205/03C08L2205/035C08L2205/08C08L81/02C08L51/06C08K13/06C08K9/04C08K3/346C08K3/02C08K5/34928C08K7/14
Inventor 杨桂生王华李晓庆朱敏
Owner HEFEI GENIUS NEW MATERIALS
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