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Copper nanowire and preparation method thereof

A technology of copper nanowires and copper alloys, which is applied in the fields of nanotechnology, nanotechnology, nanotechnology for materials and surface science, etc. problem, to achieve the effect of simple and feasible preparation method, good affinity and low cost

Active Publication Date: 2019-02-15
UNIV OF ELECTRONICS SCI & TECH OF CHINA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, these methods use a lot of pharmaceutical materials, take a long time or require relatively high equipment, resulting in not only high cost in the process of preparing copper nanowires, but also difficult to achieve large-scale preparation of copper nanowires.

Method used

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  • Copper nanowire and preparation method thereof
  • Copper nanowire and preparation method thereof
  • Copper nanowire and preparation method thereof

Examples

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Effect test

Embodiment 1

[0033] A kind of copper nano wire, its preparation method comprises the following steps:

[0034] (1) In an environment with a dew point of -50°C and an oxygen content of 10ppm, the lithium metal is heated to 200°C, and the lithium metal is in a molten state at this time;

[0035] (2) Metal copper is added in the metallic lithium of molten state, heat preservation 10min, mix, form the alloy of melting; Wherein, the atomic number ratio of copper and metallic lithium is 1:100;

[0036] (3) cooling the molten alloy to room temperature within 5min to obtain lithium-copper alloy CuLi100;

[0037] (4) Lithium-copper alloy CuLi100 is put into water, and metal lithium is removed through redox reaction of lithium and water to obtain copper nanowires.

Embodiment 2

[0039] A kind of copper nano wire, its preparation method comprises the following steps:

[0040] (1) In an environment with a dew point of -60°C and an oxygen content of 2ppm, the metal lithium is heated to 200°C, and the metal lithium is in a molten state at this time;

[0041] (2) Metal copper is added in the metallic lithium of molten state, heat preservation 10min, mix, form the molten alloy; Wherein, the atomic number ratio of copper and metallic lithium is 1:60;

[0042] (3) cooling the molten alloy to room temperature within 5min to obtain lithium-copper alloy CuLi60;

[0043] (4) Lithium-copper alloy CuLi60 is put into water, and metal lithium is removed through redox reaction of lithium and water to obtain copper nanowires.

Embodiment 3

[0045] A kind of copper nano wire, its preparation method comprises the following steps:

[0046] (1) In an environment with a dew point of -70°C and an oxygen content of 1ppm, the lithium metal is heated to 800°C, and the lithium metal is in a molten state at this time;

[0047] (2) Metal copper is added in the metallic lithium of molten state, heat preservation 10min, mix, form the molten alloy; Wherein, the atomic number ratio of copper and metallic lithium is 2:3;

[0048] (3) cooling the molten alloy to room temperature within 5min to obtain lithium-copper alloy Cu2Li3;

[0049] (4) Lithium-copper alloy Cu2Li3 is put into water, and metal lithium is removed through redox reaction of lithium and water to obtain copper nanowires.

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Abstract

The invention provides a copper nanowire and a preparation method thereof. The preparation method comprises the following steps that in the environment with the dew point no more than -50 DEG C and the oxygen content mo more than 10ppm, lithium metal is heated to 200-800DEG C, and therefore the lithium metal is in the molten condition; copper is added in to the lithium metal in the molten condition, heat preservation is conducted and lasts for 5-15min, and mixing is conducted to form molten alloy; the molten alloy is cooled to the room temperature, and lithium-copper alloy is manufactured; andthe lithium in the lithium-copper alloy is removed, and the copper nanowire is manufactured. The copper nanowire is manufactured by a single method, the temperature in the preparation method is low,and the shape and appearance of the copper nanowire can be controlled. In addition, the cost of the preparation method is low, and the copper nanowire can be prepared at a large scale. The prepared copper nanowire can be used as a three-dimensional fluid collector of a lithium battery, and can be directly used in the fields of transparent conductive films, conductive ink and the like.

Description

technical field [0001] The invention belongs to the technical field of copper nanowires, and in particular relates to a copper nanowire and a preparation method thereof. Background technique [0002] Copper nanowires have high electronic conductivity, good photoelectric performance and catalytic performance, and have potential application prospects in the fields of three-dimensional current collectors, microelectronic devices, chemistry, transparent conductive films, transparent electrodes, and conductive inks. However, its high cost and inability to prepare on a large scale limit its wide commercial application. [0003] At present, the main methods for preparing copper nanowires include liquid-phase synthesis, vapor-phase deposition, and template methods. However, these methods use a lot of pharmaceutical materials, take a long time or have relatively high requirements for equipment, which not only leads to high costs in the process of preparing copper nanowires, but also...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F9/16B22F1/00H01M10/052B82Y40/00B82Y30/00
CPCH01M10/052B82Y30/00B82Y40/00B22F9/16B22F1/0547Y02E60/10
Inventor 李晶泽贾维尚姚泽宇刘芋池屈思吉李超
Owner UNIV OF ELECTRONICS SCI & TECH OF CHINA
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