A kind of modified brine workover fluid and preparation method thereof
A workover fluid and brine technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of easy leakage and other problems, and achieve the effect of easy flowback and good plugging effect
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[0099] In a second aspect, embodiments of the present invention provide a method for preparing the above-mentioned modified brine workover fluid, which specifically includes the following steps:
[0100] According to the proportion, add a modifier to prevent brine scaling into the brine and stir evenly, then add a viscosifying suspending agent, stir the viscosifying suspending agent until it is evenly dispersed, then add salt-resistant plugging agent, oil-soluble resin and drilling The unidirectional pressure sealing agent is used for the liquid and stirred to disperse evenly to obtain the modified brine workover fluid.
[0101] It can be understood that, according to different brines, different modifiers for preventing brine scaling can be added. For the preparation method of the modifier for preventing brine scaling, refer to the above-mentioned Chinese patent application with the application number 201510907377.X and the title of the invention "a modifier for preventing bri...
Embodiment 1
[0112] This example provides the formulation and preparation method of the salt-tolerant plugging agent, and evaluates the performance of the salt-tolerant plugging agent.
[0113] The raw material formula of the salt-resistant leakage plugging agent of this embodiment is shown in Table 1.
[0114] Table 1
[0115]
[0116] The preparation method of the salt-resistant leakage plugging agent of the present embodiment is as follows:
[0117] Step 1, add 75kg of tap water into the iron bucket A, and then heat it to boiling.
[0118] Step 2, add 25kg of tap water to the iron bucket B, then add sodium tetraborate according to the formula in Table 1, stir to dissolve the sodium tetraborate, then add pregelatinized starch and cornstarch, stir to make the pregelatinized starch and cornstarch After dissolving, sodium chloride was added, and stirring was continued to obtain an emulsion-like mixed solution.
[0119] Step 3: Add the mixed solution obtained in iron bucket B into iron...
Embodiment 2
[0129] This example provides the formulation and preparation method of the viscosifying suspension, and evaluates the performance of the viscosifying suspension.
[0130] The formula of the viscosity-increasing suspending agent of the present embodiment is shown in Table 3.
[0131] In this example, the hydroxymethyl starch used is the product of Renqiu Gaoke Chemical Materials Co., Ltd.
[0132] table 3
[0133]
[0134]
[0135] After mixing hydroxymethyl starch, N,N'-methylenebisacrylamide and sodium thiosulfate according to the formula in Table 3, the viscosity-increasing suspension modifier of this example is obtained. The viscosity-increasing suspension modifier It is a white powdery solid.
[0136] The viscosity-increasing effect of the viscosity-increasing suspension agent 4 in this example on the brine workover fluid is evaluated below, and compared with partially hydrolyzed polyacrylamide (HPAM).
[0137] Viscosifying suspending agent 4 is added in salt bitt...
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