a ti 3 sic 2 -al 2 o 3 -sic-al composite material and preparation method thereof
A technology of ti3sic2-al2o3-sic-al and composite materials, which is applied in the field of Ti3SiC2-Al2O3-SiC-Al composite materials and their preparation, can solve the problem of poor surface wear resistance, low hardness, and poor anti-friction and wear resistance of composite materials. question
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[0031] Ti of the present invention 3 SiC 2 -Al 2 o 3 -The preparation method of SiC-Al composite material, this method comprises the steps:
[0032] 1) Preparation of Al-based alloy: the mass percentage of each element of Al-based alloy is: Al, 45-90wt.%; Ti, 3-25wt.%; Mg, 1-6wt.%; Si, 5-30wt.%;
[0033] Weigh the corresponding raw materials according to the mass percentage of the above elements, put the pure aluminum ingot into 0.5mol / L NaOH solution, after 1-3 hours, after the surface oxide skin is completely removed, put it in a graphite crucible, and then put the titanium ingot, Place magnesium powder and silicon blocks together in a graphite crucible, then place the graphite crucible in an energy-saving box-type resistance furnace model SX-G04132 to heat up to 700-1100°C for melting, keep it warm for 0.5-4h, and stir until completely dissolved , that is, the Al-based alloy liquid in molten state is obtained;
[0034] 2) Treatment of SiC ceramics: Cut the SiC ceramic ...
Embodiment 1
[0041] This embodiment Ti 3 SiC 2 -Al 2 o 3 The preparation method of the -SiC-Al composite material is as follows:
[0042] 1) Preparation of aluminum-based alloy: the mass percentage of each element of the aluminum-based alloy is composed of: Al, 78wt%; Ti, 10wt%; Mg, 2wt%; Si, 10wt%;
[0043] Weigh the corresponding raw materials according to the above-mentioned mass percentages of each element, and each raw material is respectively Al ingot (purity 99.9%), Ti ingot (purity 99.9%), Mg powder (purity 99.9%), Si block (purity 99.5%), pure aluminum Put the ingot into the NaOH solution of 0.5mol / L. After 2 hours, after the surface oxide skin is completely removed, take 156gAl ingot and place it in a graphite crucible, then put 20gTi, 20gSi, and 4gMg in the graphite crucible together, and place the graphite crucible In an energy-saving box-type resistance furnace model SX-G04132, the temperature was raised to 800°C with a heating rate of 20°C / min, kept at this temperature fo...
Embodiment 2
[0051] This embodiment Ti 3 SiC 2 The specific steps of the preparation method of the / SiC / Al composite material are the same as in Example 1, except that the mass percentage of each element of the aluminum-based alloy consists of: Al, 83wt%; Ti, 5wt%; Mg, 2wt%; Si, 10wt% %.
[0052] According to the test and analysis process of embodiment 1, the composite material obtained in this embodiment is analyzed and tested, and the specific result is: through the fracture toughness test, the average fracture toughness of the composite material obtained in this embodiment is 4.3MPam 1 / 2 , compared to pristine SiC ceramics (2.2MPam 1 / 2 ) increased by 2.1MPam 1 / 2 ; Under the same conditions, the friction and wear performance test is carried out, and the average friction coefficient of the measured material is 0.45, and the average wear rate is 4.2×10 -3 mm 3 / min, compared to original SiC ceramics (friction coefficient 0.55, wear rate 5×10 -3 mm 3 / min), the friction coefficient i...
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