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Heat-stable high-impact polycrystalline diamond composite sheet and preparation method thereof

A polycrystalline diamond, high impact resistance technology, applied in metal processing equipment, transportation and packaging, etc., can solve the problems of polycrystalline diamond layer composite sheet failure, reduce the thermal stability and wear resistance of polycrystalline diamond layer, etc. The effect of reducing the harmful residual stress at the interface, improving the impact resistance and collapse resistance, and improving the impact resistance

Active Publication Date: 2021-02-26
KINGDREAM PLC CO +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

But at the same time, a higher cobalt content will reduce the thermal stability and wear resistance of the polycrystalline diamond layer, because the large difference in thermal expansion coefficient between cobalt and diamond will cause microcracks between the bonds of diamond grains under heated conditions, resulting in fragmentation of the polycrystalline diamond layer and early failure of the compact

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  • Heat-stable high-impact polycrystalline diamond composite sheet and preparation method thereof
  • Heat-stable high-impact polycrystalline diamond composite sheet and preparation method thereof
  • Heat-stable high-impact polycrystalline diamond composite sheet and preparation method thereof

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preparation example Construction

[0040] The steps of the preparation method of the heat-stable high impact-resistant polycrystalline diamond composite sheet proposed by the present invention are as follows:

[0041] The first step is to mix double-layer diamond powder with different particle sizes;

[0042] In the second step, the mixed double-layer diamond powder, the cemented carbide substrate 200 with a parallel groove-like interface, and various assembly components are assembled internally and externally to form an external composite mold (internal assembly refers to the use of metal materials) The cup wraps the cemented carbide matrix 200 and diamond powder, and the small parts formed are called the inner composite mold; the outer assembly refers to wrapping the inner composite mold with various salt parts and pyrophyllite blocks, and the small parts formed are called the outer composite mold. );

[0043] The third step is to put the outer synthetic mold into the six-sided top press, and sinter it into a ...

Embodiment 1

[0068] This embodiment is a thermally stable high-impact polycrystalline diamond composite sheet with a diameter of 15.88 mm and a height of 13.22 mm. First, mix the diamond powder of the surface layer and the transition layer: the main particle size of the surface layer powder is 10-20mm, and the main particle size of the transition layer powder is 25-35mm. The mixed double-layer powder is fired at 650-750° C. for 30-90 minutes in a hydrogen atmosphere. Put the fired double-layer powder into the metal cup sequentially according to the ratio of the thickness of the surface layer to 1.0mm and the thickness of the transition layer to 1.5mm, and the cemented carbide substrate with parallel groove interface, and perform internal assembly to obtain the internal composite mold. The inner synthetic mold is subjected to heat treatment at 500-1200° C. for 90-150 minutes in an argon atmosphere. Externally assemble the heat-treated inner composite mold with other assembly components to ...

Embodiment 2

[0074] This embodiment is a thermally stable high-impact polycrystalline diamond composite sheet with a diameter of 15.88 mm and a height of 13.22 mm. First, mix the diamond powder of the surface layer and the transition layer: the main particle size of the surface layer powder is 15-25mm, and the main particle size of the transition layer powder is 35-45mm. The mixed double-layer powder is fired at 650-750° C. for 30-90 minutes in a hydrogen atmosphere. Put the fired double-layer powder into the metal cup sequentially according to the ratio of surface layer thickness of 1.0mm and transition layer thickness of 2.0mm, and cemented carbide substrate with parallel groove interface, and perform internal assembly to obtain an internal composite mold. The inner synthetic mold is subjected to heat treatment at 500-1200° C. for 90-150 minutes in an argon atmosphere. Externally assemble the heat-treated internal composite mold with other assembly components to obtain an external compo...

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Abstract

The invention discloses a heat-stable high-impact polycrystalline diamond composite sheet, which comprises a cemented carbide substrate and a polycrystalline diamond layer, wherein the polycrystalline diamond layer includes a transition layer close to the cemented carbide substrate and a transition layer away from the hard alloy substrate. The surface layer on one side of the alloy matrix, the surface layer and the transition layer of the polycrystalline diamond layer are composed of diamond powder formulations with different particle sizes, the main particle size of the surface layer powder is 5-25 microns, and the main particle size of the transition layer powder is 25-45 microns. The thickness ratio to the transition layer is 1:1‑1:3. The heat-stable high-impact polycrystalline diamond composite sheet proposed by the invention can improve drilling efficiency, shorten the drilling-production cycle, prolong the service life and effectively reduce the drilling-production cost.

Description

technical field [0001] The invention relates to the technical field of superhard materials, in particular to a heat-stable high-impact polycrystalline diamond composite sheet and a preparation method thereof. Background technique [0002] Polycrystalline diamond compact (PDC) generally consists of two layers of material - the upper layer of polycrystalline diamond layer and the lower layer of cemented carbide substrate. Generally, it is made of diamond powder and cemented carbide matrix by sintering and compounding under high temperature and high pressure (HTHP). Diamond composite sheet has both the high wear resistance of the diamond layer and the high toughness of the cemented carbide matrix, and is a very important cutting element for oil and gas drilling tools. [0003] With the continuous development of the oil and gas development industry and the development of unconventional energy such as shale gas and shale oil, the production conditions and requirements for drilli...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22F1/00B22F3/14B22F7/04B22F3/24C22C26/00
CPCC22C26/00B22F3/14B22F3/24B22F7/04B22F2003/241B22F1/052
Inventor 田红平陈文婷徐磊张烈华刘洋
Owner KINGDREAM PLC CO