Method for preparing nano-scale catalyst through ultrasonic atomization plasma reaction
A plasma and catalyst technology, which is used in the field of ion reaction to prepare nano-scale catalysts, can solve the problems of high temperature agglomeration of catalyst active components, and achieve the effects of high catalytic oxidation capacity, improved efficiency and high efficiency.
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Embodiment 1
[0047] Preparation of 5wt% Nanoscale Ag / Al by Ultrasonic Atomized Plasma Reaction 2 o 3 catalyst:
[0048] (1) Add 20 mL of 3.94% AgNO to the ultrasonic nebulizer 3 Solution, pass 200mL / min carrier gas nitrogen into the ultrasonic nebulizer, the gas is bubbled through the ultrasonic nebulizer, and the nebulized gas containing the reaction precursor is brought out; the nebulization rate is 10mL / h.
[0049] (2) The nano-scale aerosol gas containing the catalytic active ingredient flowing out from the ultrasonic atomizer is passed into the mixer and mixed evenly with supplementary nitrogen gas with a flow rate of 100mL / min.
[0050] (3) Continuously and slowly pass the nanoscale aerosol gas containing the catalyst active component through the Al containing 2g 1.6-2.0mm 2 o 3 The tubular dielectric barrier discharge reactor of small balls, the catalyst carrier small balls are arranged between two metal electrodes of the reactor. Turn on the switch of the tube electric furnace...
Embodiment 2
[0055] adjust AgNO 3 concentration of the solution, and ensure that Al 2 o 3 The amount of pellets, experimental temperature, discharge power, discharge time and other factors are the same, and Ag / Al with different loadings are prepared 2 o 3 Catalysts, Ag / Al with different loadings 2 o 3 The absorbance of the catalyst as a function of wavelength is shown in image 3 shown. It is known from experiments that Ag / Al 2 o 3 The absorbance of the catalysts reached the peak at a wavelength of about 250nm, and the catalytic performance of the catalyst with 5wt.% Ag loading was the best, followed by 2wt.% Ag loading, and 1wt.% Ag loading was the worst.
Embodiment 3
[0057] Precursor solution replaced with HAuCl 4 and H 2 PtCl 6 solution, adjust HAuCl 4 and H 2 PtCl 6 concentration of the solution, and ensure that Al 2 o 3 The amount of pellets, experimental temperature, discharge power, discharge time and other factors are the same, and Au / Al with different loadings are prepared 2 o 3 Catalysts and Pt / Al with different loadings 2 o 3 catalyst.
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