Organic material, preparation method thereof and application of organic material in electroluminescent devices
A technology of organic materials and light-emitting devices, applied in the field of organic electroluminescence display, can solve the problems of affecting the service life of materials, destruction of film uniformity, low glass transition temperature, etc., to achieve good film stability and improve carrier transmission efficiency. , the effect of high hole mobility
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Embodiment 1
[0049] Synthesis of (Compound 1)
[0050] The synthetic route is as follows:
[0051]
[0052] Compound 1
[0053] 1) Synthesis of compound 1-2
[0054] 1000ml three-necked flask, equipped with magnetic stirring, after argon replacement, add 46.1g (0.48mol) of sodium tert-butoxide, 27.94g (purity 99%, 0.3mol) of 2-aniline, and 67.25g of 3-bromo-9-toluene Base-9H-carbazole (purity 99%, 0.2 mol) and toluene 400ml. After argon replacement again, 3 ml of tri-tert-butylphosphine and 0.46 g of tris(diphenylbenzylacetone)dipalladium were added in sequence. After the addition, start stirring and heat up to 100°C, and control the temperature at 100-110°C for 5 hours. After cooling down to 30°C, the filtrate was obtained by suction filtration through a silica gel column, and the filtrate was rotary evaporated, dissolved in dichloromethane, washed twice with 4mol / L hydrochloric acid solution, separated, dried with anhydrous sodium sulfate, suction filtered, and rotary evaporated...
Embodiment 2
[0059] Synthesis of (Compound 2)
[0060] The synthetic route is as follows:
[0061]
[0062] Compound 2
[0063] 1) Synthesis of compound 2-1
[0064] 1000 ml three-necked flask, equipped with magnetic stirring, after argon replacement, add 46.1 g (0.48 mol) of sodium tert-butoxide, 27.94 g (purity 99%, 0.3 mol) of 2-aniline, and 67.25 g of 3-bromo-9-benzene Base-9H-carbazole (purity 99%, 0.2 mol) and xylene 400ml. After argon replacement again, 3 ml of tri-tert-butylphosphine and 0.46 g of tris(diphenylbenzylacetone)dipalladium were added in sequence. After the addition, start stirring and heat up to 110°C, and control the temperature at 110-120°C for 5 hours. After cooling down to 30°C, the filtrate was obtained by suction filtration through a silica gel column, and the filtrate was rotary evaporated, dissolved in dichloromethane, washed twice with 4mol / L hydrochloric acid solution, separated, dried with anhydrous sodium sulfate, suction filtered, and rotary evapora...
Embodiment 3
[0069] Synthesis of (Compound 3)
[0070] The synthetic route is as follows:
[0071]
[0072] Compound 3
[0073] 1) Synthesis of compound 3-1
[0074] 1000 ml three-necked flask, equipped with magnetic stirring, after argon replacement, add 46.1 g (0.48 mol) of sodium tert-butoxide, 27.94 g (purity 99%, 0.3 mol) of 2-aniline, and 67.25 g of 6-bromo-1-methyl phenyl-9-phenyl-9H-carbazole (purity 99%, 0.2 mol) and toluene 400ml. After argon replacement again, 3 ml of tri-tert-butylphosphine and 0.46 g of tris(diphenylbenzylacetone)dipalladium were added in sequence. After the addition, start stirring and heat up to 100°C, and control the temperature at 100-110°C for 5 hours. After cooling down to 30°C, the filtrate was obtained by suction filtration through a silica gel column, and the filtrate was rotary evaporated, dissolved in dichloromethane, washed twice with 4mol / L hydrochloric acid solution, separated, dried with anhydrous sodium sulfate, suction filtered, and r...
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