Unlock instant, AI-driven research and patent intelligence for your innovation.

Layered molecular sieve and preparation method thereof

A molecular sieve and layered technology, applied in the field of layered molecular sieves and its preparation, to achieve good application prospects, high crystallinity, and good technical effects

Active Publication Date: 2022-07-12
CHINA PETROLEUM & CHEM CORP +1
View PDF14 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] There are two main sources of molecular sieves. One is obtained from natural minerals, and the other is obtained through artificial synthesis. Some molecular sieves can be obtained through both methods, but some molecular sieves can only be obtained through one of the two.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Layered molecular sieve and preparation method thereof
  • Layered molecular sieve and preparation method thereof
  • Layered molecular sieve and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Mix 40% silica sol, aluminum hydroxide, templating agent Q1, and water in a molar ratio of 1SiO 2 :0.05Al 2 O 3 :0.15Q1:80H 2 O mixed uniformly, the above mixture was transferred into a reaction kettle and crystallized at 170° C. for 120 hours. After the reaction was completed, after washing and drying, a layered molecular sieve was obtained. The related structure of Q1 is shown in Table 1.

Embodiment 2

[0030] Combine 40% silica sol, alumina, templating agent Q2, and water in a molar ratio of 1SiO 2 :0.5Q2:100H 2 O mixes evenly, and the above mixture is transferred into a reaction kettle for crystallization at 150° C. for 100 hours. After the reaction is completed, after washing and drying, a layered molecular sieve is obtained. The related structure of template Q2 is shown in Table 1.

Embodiment 3

[0032] Combine silica, alumina, template Q2, and water in a molar ratio of 1SiO 2 :0.01Al 2 O 3 :0.2Q2:100H 2 O mixed uniformly, the above mixture was transferred into a reaction kettle and crystallized at 150° C. for 120 hours. After the reaction was completed, after washing and drying, a layered molecular sieve was obtained. The related structure of template Q2 is shown in Table 1.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to a layered molecular sieve material and a preparation method thereof, and mainly solves the technical problem of the novel layered molecular sieve material not involved in the prior art. The present invention provides a new layered molecular sieve material, comprising the following chemical composition in molar ratio: 1SiO 2 :(0~0.1)Al 2 O 3 :(0.1~0.3)Q:(1~10)H 2 O, wherein the template agent Q is a technical solution of a gemini quaternary ammonium salt or a quaternary amine base, which better solves the above-mentioned technical problems and obtains a new layered molecular sieve material, which can be used in the field of industrial catalysis.

Description

technical field [0001] The invention relates to a layered molecular sieve and a preparation method thereof, belonging to the technical field of molecular sieve synthesis. Background technique [0002] Zeolite molecular sieves are widely used due to their unique channel shape selectivity, unique solid acid properties and excellent ion exchange properties, and have shown their huge commercial application value in adsorption, separation and catalysis. For example, in the fields of petroleum refining and chemical industry, the application of Y zeolite has brought a sudden revolution to petroleum catalytic cracking technology, while other molecular sieve catalysts, such as ZSM-5 zeolite, mordenite, beta zeolite, MCM-22 zeolite , The application of SAPO-34 molecular sieve has also brought substantial breakthroughs to important petroleum refining and chemical technologies such as cracking, reforming, isomerization, aromatic hydrocarbon disproportionation and alkylation, and methano...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C01B39/48
CPCC01B39/48C01P2002/72C01P2004/03Y02P20/52
Inventor 沈少春杨为民王振东李应成沙鸥汪莹莹
Owner CHINA PETROLEUM & CHEM CORP