Fused ring organic compound and mixture and organic electronic device comprising same

A technology of organic compounds and mixtures, which is applied in the field of organic electronic devices and fused-ring organic compounds, can solve the problems of efficiency, lifespan and thermal stability, etc., and achieve excellent electron transport properties and stability, simple material synthesis, and improved electrical efficiency. The effect of luminescence efficiency and device lifetime

Pending Publication Date: 2019-05-03
GUANGZHOU CHINARAY OPTOELECTRONICS MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the efficiency, lifetime and thermal stability of the above materials need to be improved.

Method used

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  • Fused ring organic compound and mixture and organic electronic device comprising same
  • Fused ring organic compound and mixture and organic electronic device comprising same
  • Fused ring organic compound and mixture and organic electronic device comprising same

Examples

Experimental program
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preparation example Construction

[0256] According to the above-mentioned preparation method, a functional layer is formed with a thickness of 5nm-1000nm.

[0257] The present invention also relates to the use of the above-mentioned condensed ring organic compound or mixture in organic electronic devices.

[0258] The present invention further relates to an organic electronic device comprising a condensed ring organic compound or high polymer or mixture as described above.

[0259] The organic electronic device can be selected from, but not limited to, organic light emitting diode (OLED), organic photovoltaic cell (OPV), organic light emitting cell (OLEEC), organic field effect transistor (OFET), organic light emitting field effect transistor, organic Lasers, organic spintronic devices, organic sensors and organic plasmon emitting diodes (Organic Plasmon Emitting Diode), etc., are particularly preferred organic electroluminescent devices, such as OLED, OLEEC, organic light emitting field effect tube.

[0260]...

Embodiment 1

[0277]

[0278] Synthesis of intermediate 3: 30 g of 1-naphthol (intermediate 1), 59 g of o-bromoiodobenzene (intermediate 2) were dissolved in 300 mL of dry THF, and 8 g of NaH was added. Under nitrogen atmosphere, stir at room temperature for 12h. Carefully add methanol to quench the reaction, wash with water to separate the liquid, and obtain intermediate 3. MS (ASAP): 299.17 by column chromatography.

[0279] Synthesis of Intermediate 4: Dissolve 40g of Intermediate 3 in 400mL of dry THF, slowly drop into 66mL of 2M n-BuLi at -78°C under nitrogen atmosphere, stir for 1 hour, and slowly drop into Intermediate 4 (35g) THF solution. Then return to room temperature. The reaction was quenched by adding water, washed with water to separate the liquid, and separated by column chromatography to obtain the crude product. After drying, dissolve in 300 mL of a mixed solvent of glacial acetic acid and hydrochloric acid (glacial acetic acid: hydrochloric acid = 10:1 (volume ratio...

Embodiment 2

[0283]

[0284] Synthesis of Comp 2: 50 g of Intermediate 6, 34 g of Intermediate 8 and 4.5 g of Pd (PPh 3 ) 4 Dissolved in 600mL toluene, refluxed under nitrogen atmosphere for 12h. The solvent was spin-dried, extracted and separated, and recrystallized to obtain compound Comp 2.MS (ASAP): 689.82.

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Abstract

The invention relates to a fused ring organic compound and a mixture and organic electronic device comprising the same. The fused ring organic compound shown in a general formula (I) has excellent electron transport properties and stability, material synthesis is simple, and when a synthesized material is applied to a device host material, the luminous efficiency and stability of the device can beimproved, and the production cost of the device can be reduced. In addition, a co-host can be formed through cooperation of the fused ring organic compound with another host with a hole transport property or a bipolar property, the electroluminescent efficiency and the service life of the device can be improved further.

Description

[0001] This application claims the priority of the Chinese patent application submitted to the China Patent Office on December 27, 2017, with the application number 2017114476394 and the title of the invention is "a fused ring organic compound, its mixture and its application in organic electronic devices", The entire contents of which are incorporated by reference in this application. technical field [0002] The invention relates to the technical field of display devices, in particular to condensed ring organic compounds, mixtures thereof and organic electronic devices. Background technique [0003] The diversity and synthesis of organic electroluminescent materials have laid a solid foundation for the realization of large-area new display devices. In order to improve the luminous efficiency of organic light-emitting diodes, fluorescent and phosphorescent light-emitting material systems have been developed so far. Organic light-emitting diodes using fluorescent materials h...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07D405/14C07D495/10C07D493/10C07D405/04C07D495/04C07D409/04C07D405/10C07D491/107C07D519/00C09K11/06H01L51/50H01L51/54
CPCY02E10/549
Inventor 谭甲辉张晨潘君友
Owner GUANGZHOU CHINARAY OPTOELECTRONICS MATERIALS
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