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Lithium battery diaphragm and preparation method thereof

A lithium battery diaphragm and raw material technology, applied in the field of lithium battery diaphragm and its preparation, can solve the problems of diaphragm porosity, poor gas permeability, etc., achieve improved puncture strength, improved charge and discharge performance, closed cell temperature, and increased capacity retention Effect

Inactive Publication Date: 2019-05-14
HUNAN AIHUA GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

A production method of a lithium battery separator, which is characterized in that it comprises the following steps: 1) using a plastic film as a base material, and irradiating the plastic film with high-energy particles; 2) immersing the irradiated plastic film in an acid solution Lithium battery diaphragm can be obtained by etching reaction in the container of alkali solution or alkali solution; the porosity and air permeability of the diaphragm are poor, and further improvement is still needed

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A lithium battery separator of the present embodiment comprises the following raw materials in parts by weight:

[0026] 50 parts of polypropylene resin, 20 parts of polyethylene resin, 8-14 parts of graphene modified liquid, 4-8 parts of polyetherimide, 4-7 parts of aluminum oxide, 3-6 parts of rare earth lanthanum chloride, scaly 1-3 parts of mica, 4-10 parts of pore-forming agent, and 1-3 parts of pore-forming auxiliary agent.

[0027] The preparation method of the graphene-modified solution in this embodiment is to activate the graphene first, then add it to the olive oil in the oil bath, add it while stirring, then add nano-montmorillonite, and stir until the raw materials are fully mixed , you can.

[0028] The activation treatment of this embodiment uses ammonium bifluoride and ethanolamine to prepare the activator according to the weight ratio of 1:2, and the inter-activator and graphene are mixed and ultrasonically dispersed according to the weight ratio of 1:...

Embodiment 2

[0037] A lithium battery separator of the present embodiment comprises the following raw materials in parts by weight:

[0038] 60 parts of polypropylene resin, 30 parts of polyethylene resin, 14 parts of graphene modified liquid, 8 parts of polyetherimide, 7 parts of alumina, 6 parts of rare earth lanthanum chloride, 3 parts of scaly mica, 10 parts of pore-forming agent 3 parts, 3 parts of pore-forming additives.

[0039] The preparation method of the graphene-modified solution in this embodiment is to activate the graphene first, then add it to the olive oil in the oil bath, add it while stirring, then add nano-montmorillonite, and stir until the raw materials are fully mixed , you can.

[0040] In the activation treatment of this example, ammonium bifluoride and ethanolamine were used to prepare an activator at a weight ratio of 1:4, and an interactivator and graphene were mixed and ultrasonically dispersed at a weight ratio of 3:1 for 40 minutes.

[0041] The olive oil i...

Embodiment 3

[0047] A lithium battery separator of the present embodiment comprises the following raw materials in parts by weight:

[0048] 55 parts of polypropylene resin, 25 parts of polyethylene resin, 11 parts of graphene modified liquid, 6 parts of polyetherimide, 5.5 parts of alumina, 4.5 parts of rare earth lanthanum chloride, 2 parts of scaly mica, 6 pore-forming agents 2 parts, 2 parts of pore-forming additives.

[0049]The preparation method of the graphene-modified solution in this embodiment is to activate the graphene first, then add it to the olive oil in the oil bath, add it while stirring, then add nano-montmorillonite, and stir until the raw materials are fully mixed , you can.

[0050] In the activation treatment of this embodiment, ammonium bifluoride and ethanolamine were used to prepare an activator at a weight ratio of 1:3, and an interactivator and graphene were mixed and ultrasonically dispersed at a weight ratio of 2:1 for 35 minutes.

[0051] The olive oil in t...

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Abstract

The invention relates to the technical field of lithium batteries, in particular to a lithium battery diaphragm and a preparation method thereof. The lithium battery diaphragm is prepared from the following raw materials in parts by weight: 50-60 parts of polypropylene resin, 20-30 parts of polyethylene resin, 8-14 parts of graphene modified liquid, 4-8 parts of polyetherimide, 4-7 parts of aluminum oxide, 3-6 parts of rare earth lanthanum chloride, 1-3 parts of scaly mica, 4-10 parts of a pore-forming agent, and 1-3 parts of a pore-forming addition agent. The lithium battery diaphragm takes the polypropylene resin and the polyethylene resin as base materials and takes the polyetherimide as auxiliaries, through the added aluminum oxide, rare earth lanthanum chloride and the scaly mica, thepuncture strength of the diaphragm can be improved, and after graphene is modified, compatibility between the graphene and the diaphragm raw materials is improved.

Description

technical field [0001] The invention relates to the technical field of lithium batteries, in particular to a lithium battery diaphragm and a preparation method thereof. Background technique [0002] A lithium battery is a primary battery that uses lithium metal or lithium alloy as the negative electrode material and uses a non-aqueous electrolyte solution. It is different from a rechargeable battery. Lithium-ion batteries are different from lithium-ion polymer batteries. Due to the very active chemical properties of lithium metal, the processing, storage and use of lithium metal have very high environmental requirements. Therefore, lithium batteries have not been used for a long time. With the development of microelectronics technology at the end of the 20th century, miniaturized equipment is increasingly The increase puts high demands on the power supply. Lithium batteries have entered a large-scale practical stage; lithium batteries are divided into two categories: Lithiu...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01M2/16H01M2/14H01M10/0525H01M50/403H01M50/446H01M50/489
CPCY02E60/10
Inventor 殷宝华贾明夏商曹文
Owner HUNAN AIHUA GRP