Natural algistat and preparation method and application thereof
An algae inhibitor, a natural technology, applied in the direction of botanical equipment and methods, applications, herbicides and algicides, etc., can solve the problems that cannot meet the requirements of algae control in lake ecosystems, and improve the efficiency and operation of algae bloom control. Convenience and the effect of reducing the cost of algae bloom control
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[0048] In a further preferred embodiment of the present invention, the preparation method of the crustacean extract comprises the following steps: first extracting chitin from shrimp shells or crab shells, and then deacetylating the chitin to obtain the crustacean extract.
[0049] The preparation method of the crustacean extract has simple process and convenient operation, and can effectively reduce the preparation cost of the natural algastatic agent.
[0050] In a further preferred embodiment of the present invention, the preparation method of chitin comprises the following steps: putting chitin into NaOH solution, performing deacetylation reaction, and obtaining crustacean extract.
[0051] In a preferred embodiment of the present invention, putting chitin into NaOH solution makes it easier to carry out the deacetylation reaction, which is more conducive to improving the deacetylation rate and improving the solubility of the crustacean extract.
[0052] In a preferred embodi...
Embodiment 1
[0088] The present embodiment provides a natural algastatic agent, including the following raw materials in parts by mass: 10 parts of crustacean extract, 64 parts of Houttuynia cordata extract and 10 parts of sodium alginate. The preparation method includes the following steps:
[0089] (1) Preparation of crustacean extract: select shrimp / crab shells to remove impurities, and wash with water. Soak the cleaned shrimp / crab shells in 5%-10% hydrochloric acid solution for 3 days, remove calcium salt, filter, wash with water until neutral, put in 10% NaOH solution, heat to boil for 3 hours, filter, wash with water, Then use 0.4% potassium permanganate to oxidize for 2h, then use 0.2% NaHSO 3 React until the color of potassium permanganate fades completely, and dry to obtain white flake chitin; put chitin in 50% NaOH solution, keep the temperature at 100°C, stir at a speed of 50r / min, and stir for about 50min to carry out the deacetylation reaction , then filtered, washed, and dri...
Embodiment 2
[0094]The present embodiment provides a natural algastatic agent, comprising the following raw materials in parts by mass: 15 parts of crustacean extract, 51.5 parts of Houttuynia cordata extract and 25 parts of sodium alginate, the step (1) of the preparation method Same as step (2) and Example 1, the difference is that in step (3), in the crustacean extract solution obtained from the configuration, the mass concentration of the crustacean extract is 15%; the alginic acid obtained from the configuration In the sodium solution, the mass concentration of sodium alginate is 12.5%; in the prepared houttuynia solution, the mass concentration of the houttuynia solution is 75%;
[0095] In step (4), after the crustacean extract solution and the sodium alginate solution were left to stand overnight, 20mL of the sodium alginate solution was added to 10mL of the crustacean extract solution under stirring, and the stirring was continued for 3h to obtain a mixed solution, Add 70 mL of Ho...
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