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Decocted extract with efficacy of sleep promoting and preparation method of decocted extract with efficacy of sleep promoting

A sleep aid and efficacy technology, applied in the direction of food science, etc., can solve the problems of large ethanol, consumption, and many operation steps, and achieve the effects of small impact, wide source of raw materials, and reduced side effects

Pending Publication Date: 2019-06-21
HUNAN BUTIAN PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Both of the above two processes require secondary alkalization and ethanol reaction system, and there are many operation steps and consume a large amount of ethanol

Method used

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  • Decocted extract with efficacy of sleep promoting and preparation method of decocted extract with efficacy of sleep promoting
  • Decocted extract with efficacy of sleep promoting and preparation method of decocted extract with efficacy of sleep promoting
  • Decocted extract with efficacy of sleep promoting and preparation method of decocted extract with efficacy of sleep promoting

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Described carboxymethyl pachyrhin is prepared by following method:

[0032] S1. Cultivation of Poria cocos: aseptically inoculate Poria cocos hyphae in wort juice liquid medium, and cultivate at 28°C for 4 days;

[0033] S2. Preparation of Poria cocos polysaccharide: Ferment the cultured Poria cocos medium at 35°C for 2 days, heat to a slight boil, extract for 1 hour, filter, add 3 times the amount of mixed solvent of chloroform and n-butanol, the chloroform and n-butanol The mixed volume ratio is 4:1, shaken, centrifuged, add 3 times the amount of 95% ethanol, overnight, filter to obtain a precipitate, wash 2 times with ether to obtain pachyman;

[0034] S3. Preparation of Poria Cocos Polysaccharide: Add 10g of Poria cocos polysaccharide into 100mL0.5mol / L sodium periodate solution for selective oxidation, adjust the pH value to 3 with trifluoroacetic acid, moderate acid hydrolysis, acid hydrolysis time is 30min, filter , washing the solid with water to obtain Poria c...

Embodiment 2

[0038] Described carboxymethyl pachyrhin is prepared by following method:

[0039] S1. Cultivation of Poria cocos: aseptically inoculate Poria cocos hyphae in wort liquid culture medium, and cultivate at 28° C. for 5 days;

[0040] S2. Preparation of Poria cocos polysaccharide: Ferment the cultured Poria cocos medium at 35°C for 2 days, heat to a slight boil, extract for 2 hours, filter, add 5 times the volume of a mixed solvent of chloroform and n-butanol, the chloroform and n-butanol The mixed volume ratio is 6:1, shaken, centrifuged, add 3 times the amount of 95% ethanol, overnight, filter to obtain a precipitate, wash 3 times with ether to obtain pachymane;

[0041] S3. Preparation of Poria Cocos Polysaccharide: Add 10g of Poria cocos polysaccharide into 30mL 1.5mol / L sodium periodate solution for selective oxidation, adjust the pH value to 4 with trifluoroacetic acid, moderate acid hydrolysis, acid hydrolysis time is 1h, filter , washing the solid with water to obtain Po...

Embodiment 3

[0045] Described carboxymethyl pachyrhin is prepared by following method:

[0046] S1. Cultivation of Poria cocos: aseptically inoculate Poria cocos hyphae in wort juice liquid medium, and cultivate at 28°C for 4 days;

[0047] S2. Preparation of Poria cocos polysaccharide: Ferment the cultured Poria cocos medium at 35°C for 2 days, heat to a slight boil, extract for 2 hours, filter, add a mixed solvent of chloroform and n-butanol, the mixing volume ratio of chloroform and n-butanol 5:1, shake, centrifuge, add 3 times the amount of 95% ethanol, overnight, filter to get precipitate, wash 3 times with diethyl ether to obtain pachyrhin;

[0048] S3. Preparation of Poria Cocos Polysaccharide: Add 10g of Poria cocos polysaccharide into 50mL 1.0mol / L sodium periodate solution for selective oxidation, adjust the pH value to 3.6 with trifluoroacetic acid, moderate acid hydrolysis, acid hydrolysis time is 45min, filter , washing the solid with water to obtain Poria cocos polysaccharid...

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Abstract

The invention provides decocted extract with an efficacy of sleep promoting. The decocted extract is prepared from, by weight, 25-35 parts of carboxymethylpachymaran, 12-17 parts of casein hydrolysate, 5-10 parts of taurine, 10-15 parts of bamboo leaf flavonoid, 20-25 parts of semen ziziphi spinosae, 10-20 parts of fructus lycii, 10-20 parts of bulbus lilii, 10-20 parts of semen nelumbinis, 5-10 parts of semen euryales and 45-55 parts of honey. The decocted extract is extensive in raw material source, a preparation method is simple, and the prepared decocted extract has great efficacies of sleep promoting, nerve calming, brain nourishing, memory improving, senescence delaying, immunity enhancing and the like and has a promising application prospect.

Description

technical field [0001] The invention relates to the technical field of traditional Chinese medicine health care, in particular to a ointment with the effect of helping sleep. Background technique [0002] In recent years, the worldwide decline in environmental quality and the increase in people's life pressure have led to an increasing number of people in a sub-healthy state. At the same time, with the continuous improvement of living standards, people are paying more and more attention to personal health issues. With the enhancement of people's health awareness, people gradually began to choose healthy food and beverages. This demand caused the market share of carbonated beverages to decline continuously. Tea beverages, coarse grain beverages, fruit juice beverages and functional beverages began to be favored by people. To enhance immunity, it is necessary to ensure the content of amino acids in physical strength. The existence of amino acids in the human body not only prov...

Claims

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Application Information

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IPC IPC(8): A23L33/105A23L33/125A23L33/175A23L33/19A23L21/25
Inventor 孙梦锦戴鑫汶戴甲木龙孝金邹奇张豪唐心文
Owner HUNAN BUTIAN PHARMA