CO2 supercritical extraction based damp and heat clearing powder and preparation method thereof
A supercritical and extraction technology, applied in the direction of pharmaceutical formulas, medical preparations containing active ingredients, active ingredients of aluminum/calcium/magnesium, etc., can solve problems such as long recovery time, large wounds, and obvious scars, and achieve the speed of onset Fast, strong penetration, no toxic side effects
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Embodiment 1
[0018] ⑴The components are: dry alum 49%, clam shell powder 27%, camphor 24%.
[0019] (2) The process preparation steps are as follows:
[0020] 1) Raw material preparation: remove impurities from the raw material components, wash, dry, pulverize, pass through a 60-mesh sieve, and take the sieved material to obtain a mixed powder;
[0021] 2) Extraction: Using supercritical extraction equipment, put the mixed powder into the extraction kettle of the supercritical CO2 extraction equipment, add ethanol with an entrainer content of 60% to immerse the mixed powder, use supercritical CO2 as the extraction solvent, and extract at a temperature of 30 ℃, the extraction pressure is 30Mpa, the extraction time is 4h, and then the temperature is raised and the pressure is lowered for separation, and the product in the separation tank is collected to obtain the extraction powder;
[0022] 3) Packaging: Put the extraction powder under ultraviolet light for 20 minutes, and then put it into...
Embodiment 2
[0024] ⑴The components are: dry alum 50%, clam shell powder 25%, camphor 25%.
[0025] (2) The process preparation steps are as follows:
[0026] 1) Raw material preparation: remove impurities from the raw material components, wash, dry, pulverize, pass through a 60-mesh sieve, and take the sieved material to obtain a mixed powder;
[0027] 2) Extraction: Using supercritical extraction equipment, put the mixed powder into the extraction kettle of the supercritical CO2 extraction equipment, add ethanol with an entrainer content of 60% to immerse the mixed powder, use supercritical CO2 as the extraction solvent, and extract at a temperature of 45 ℃, the extraction pressure is 20Mpa, the extraction time is 5h, and then the temperature is raised and the pressure is lowered to separate, and the product in the separation tank is collected to obtain the extraction powder;
[0028] 3) Packaging: Put the extraction powder under ultraviolet light for 20 minutes, and then put it into a ...
Embodiment 3
[0030] ⑴The components are: dry alum 51%, clam shell powder 23%, camphor 26%.
[0031] (2) The process preparation steps are as follows:
[0032] 1) Raw material preparation: remove impurities from the raw material components, wash, dry, pulverize, pass through a 60-mesh sieve, and take the sieved material to obtain a mixed powder;
[0033] 2) Extraction: Using supercritical extraction equipment, put the mixed powder into the extraction kettle of the supercritical CO2 extraction equipment, add ethanol with an entrainer content of 60% to immerse the mixed powder, use supercritical CO2 as the extraction solvent, and extract at a temperature of 50 ℃, the extraction pressure is 15Mpa, the extraction time is 6h, and then the temperature is raised and the pressure is lowered for separation, and the product in the separation tank is collected to obtain the extraction powder;
[0034] 3) Packaging: Put the extraction powder under ultraviolet light for 20 minutes, and then put it into...
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