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Treatment method for hydrochloric acid production tail gas

A treatment method and tail gas technology are applied in the chemical industry to achieve the effects of avoiding excessively high aggregation temperature, absorbing hydrochloric acid tail gas well, and improving tail gas absorption efficiency

Pending Publication Date: 2019-07-09
RUYUAN DONGYANGGUANG ELECTROCHEM FACTORY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved in the present invention is to overcome the defects and deficiencies in the absorption of existing hydrochloric acid tail gas, and provide a treatment method for hydrochloric acid tail gas. The treatment method of the present invention uses a water jet pump and an absorption tower to control the temperature in the absorption tower. Monitoring, effectively avoiding safety problems such as hydrogen chloride gas volatilization caused by high absorption temperature, and improving the overall tail gas absorption efficiency

Method used

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  • Treatment method for hydrochloric acid production tail gas
  • Treatment method for hydrochloric acid production tail gas

Examples

Experimental program
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Effect test

Embodiment 1

[0042] A treatment method for hydrochloric acid tail gas, its production process is as follows figure 1 shown, including the following steps:

[0043] S1. Spray vacuuming: The absorption liquid is pumped from the circulation tank to the spray absorption device to absorb the hydrochloric acid tail gas generated by the point furnace, and provide a vacuum for the synthesis furnace system. The vacuum degree is -50KPa, absorbing liquid gas and liquid The separated exhaust gas enters the exhaust gas absorption device, and the liquid enters the circulation tank;

[0044] S2. Tail gas absorption: pump the absorption liquid from the circulation tank to the tail gas absorption device under pressure, and countercurrently absorb the tail gas after gas-liquid separation;

[0045] S3. Tail gas absorption switching: After the synthesis furnace is in normal operation, switch the generated hydrochloric acid tail gas to the tail gas absorption device for countercurrent absorption, and stop ent...

Embodiment 2

[0060] A treatment method for hydrochloric acid tail gas, its production process is as follows figure 1 shown, including the following steps:

[0061] S1. Spray vacuuming: pump the absorption liquid from the circulation tank to the spray absorption device to absorb the hydrochloric acid tail gas generated by the point furnace, and provide a vacuum for the synthesis furnace system. The vacuum degree is -10KPa, and the absorption liquid, gas and liquid The separated exhaust gas enters the exhaust gas absorption device, and the liquid enters the circulation tank;

[0062] S2. Exhaust gas absorption: the absorption liquid is pumped from the circulation tank to the exhaust gas absorption device, and the exhaust gas after gas-liquid separation is absorbed countercurrently;

[0063] S3. Tail gas absorption switching: After the synthesis furnace is in normal operation, switch the generated hydrochloric acid tail gas to the tail gas absorption device for countercurrent absorption, and...

Embodiment 3

[0074] A treatment method for hydrochloric acid tail gas, its production process is as follows figure 1 shown, including the following steps:

[0075] S1. Spray vacuuming: pump the absorption liquid from the circulation tank to the spray absorption device to absorb the hydrochloric acid tail gas generated by the point furnace, and provide a vacuum for the synthesis furnace system. The vacuum degree is -10KPa, and the absorption liquid, gas and liquid The separated exhaust gas enters the exhaust gas absorption device, and the liquid enters the circulation tank;

[0076] S2. Exhaust gas absorption: the absorption liquid is pumped from the circulation tank to the exhaust gas absorption device, and the exhaust gas after gas-liquid separation is absorbed countercurrently;

[0077] S3. Tail gas absorption switching: After the synthesis furnace is in normal operation, switch the generated hydrochloric acid tail gas to the tail gas absorption device for countercurrent absorption, and...

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Abstract

The invention provides a treatment method for hydrochloric acid production tail gas. The treatment method comprises the following steps: an absorption liquid is pumped to a spray absorption device toabsorb the tail gas generated in hydrochloric acid production by furnace ignition and provide a vacuum degree for a synthetic furnace system, the tail gas enters a tail-gas absorption device, the tail-gas absorption device countercurrently absorbs tail gas subjected to gas-liquid separation, after the synthetic furnace normally operates, the produced hydrochloric acid production tail gas is sent to the tail-gas absorption device for countercurrent absorption, and after the absorption liquid is saturated, the saturated absorption liquid is conveyed out for preparing a relevant recycled product.The treatment method for the hydrochloric acid production tail gas provided by the invention adopts a combination of a water jet pump and an absorption tower, and does not require high-temperature vacuum adsorption, thereby effectively avoiding safety problems such as hydrogen chloride gas volatilization caused by too-high absorption temperature, and realizing improvement of tail gas absorption efficiency through synergistically regulating and controlling liquid supply temperature and liquid outlet temperature of the absorption liquid, wherein the absorption efficiency of hydrogen chloride gas and chlorine gas are all 95% or more; the absorption tower does not contain a filler, so that aggregation temperature is prevented from being too high; and multi-stage spray nozzles are arranged, sothat high-efficiency safe absorption is realized.

Description

technical field [0001] The invention relates to the technical field of chemical industry, more specifically, to a method for treating hydrochloric acid tail gas. Background technique [0002] Synthetic furnaces produce various products such as hydrochloric acid and hydrogen chloride. The main raw materials are chlorine and hydrogen. During the production process of the product, a large amount of tail gas will be volatilized. During production, chlorine or hydrogen chloride will be taken out by the tail gas. If chlorine or hydrogen chloride is not treated with an effective and feasible process method, it will not only cause a large amount of waste of production raw materials, but also cause serious environmental pollution problems. The existing treatment method is often evacuated by a single water jet pump. If it is less than the emission standard, the exhaust gas absorption rate is not high, and the spray absorption will easily cause the temperature to be too high, causing e...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D53/18
CPCB01D53/18B01D2257/2025B01D2257/2045
Inventor 胡智勇郑阳伟邹建生吴志坚李诚邓勇新周宇华翟光望邹赤
Owner RUYUAN DONGYANGGUANG ELECTROCHEM FACTORY
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