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Preparation method of anti-rust agent of concentrated solution for hydraulic support

A technology of hydraulic support and concentrate, applied in the petroleum industry, lubricating composition and other directions, can solve the problems of high raw material cost, poor cost performance, unsatisfactory anti-rust effect, etc., and achieve the effect of environmental friendliness

Inactive Publication Date: 2019-07-12
PETROCHINA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] The common features of the above-mentioned examples are: without exception, they all contain one or two of boron, sodium nitrite or molybdate, and the third is to add commercially available water-soluble antirust agents. Ester, etc., but the anti-rust effect is not ideal, the amount of anti-rust agent is large, the cost of raw materials is high, and the cost performance is poor.

Method used

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  • Preparation method of anti-rust agent of concentrated solution for hydraulic support
  • Preparation method of anti-rust agent of concentrated solution for hydraulic support
  • Preparation method of anti-rust agent of concentrated solution for hydraulic support

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0059] At room temperature of 15°C, add 30% demineralized water, 45% triethanolamine, and 10% monoethanolamine into the reaction kettle, stir evenly, then add 5% sebacic acid, 2% adipic acid until the system is clear, then add 7% sodium benzoate and 1% benzotriazole, stirred for 30 minutes, and the product was obtained after the system became clear.

Embodiment 2

[0061] At room temperature of 25°C, add 20% demineralized water, 47.5% triethanolamine, and 15% monoethanolamine into the reaction kettle, stir evenly, then add 6% sebacic acid, 3% adipic acid until the system is clear, then add 8% sodium benzoate and 0.5% benzotriazole, stirred for 45 minutes, and the product was obtained after the system became clear.

Embodiment 3

[0063] At room temperature of 35°C, add 28.5% demineralized water, 40% triethanolamine, 15% monoethanolamine into the reaction kettle, stir evenly, then add 6% sebacic acid, 2% adipic acid until the system is clear, then add 8% sodium benzoate and 0.5% benzotriazole, stirred for 60 minutes, and the product was obtained after the system became clear.

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Abstract

The invention discloses a preparation method of an anti-rust agent of an environment-friendly totally-synthetic concentrated solution for a hydraulic support. Monoethanolamine, triethanolamine, sebacic acid, adipic acid, sodium benzoate and BTA (benzotriazole) are used as raw materials, and a composite anti-rust agent component is prepared under normal pressure and at room temperature. Compared with the prior art, the anti-rust agent of the concentrated solution for the hydraulic support contains no sodium nitrite, boron, molybdate and other substances and has the characteristics that the anti-rust agent for the hydraulic support is environmentally friendly, can be prepared from common and available raw materials at room temperature, and can be applied to preparation of multiple brand products suitable for different water hardness and the like.

Description

technical field [0001] The invention relates to a water-soluble antirust agent, in particular to a concentrated liquid antirust agent for an environment-friendly hydraulic support. Background technique [0002] As the working medium of the hydraulic support, the hydraulic support fluid not only plays the role of power transmission, but also plays the role of lubrication, cooling, anti-corrosion and anti-rust. Compared with the traditional emulsified hydraulic support fluid, oil separation and soap separation are easy to occur during use. Due to the relatively stable performance of the precipitate, which is not easy to degrade and block the filter components of the hydraulic system, the fully synthetic hydraulic support is concentrated Liquid has attracted more and more attention because of its excellent high and low temperature and storage stability, and no oil and soap precipitation. [0003] The grades of hydraulic support fluid products need to be distinguished according...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M173/02C10N30/12C10N40/08
CPCC10M173/02C10M2201/02C10M2207/123C10M2207/127C10M2207/141C10M2215/042C10M2215/223C10N2010/02C10N2030/12C10N2040/08C10N2030/44
Inventor 尤龙刚汤仲平徐小红李铭陈志忠郎需进
Owner PETROCHINA CO LTD