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LED preparation method and LED

A light-emitting layer and electron technology, applied in electrical components, circuits, semiconductor devices, etc., can solve the problems of the effect of luminous efficiency, the reduction of the number and concentration of photons, the consumption of electrons and holes, etc. Effect of Luminous Efficiency

Active Publication Date: 2019-07-26
JIANGXI EPITOP OPTOELECTRONICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] However, in the preparation process of the existing GaN-based LED, the GaN layer grown on the AlN substrate will generate many dislocations, and the dislocations will extend to the light-emitting layer, resulting in many dislocations in the light-emitting layer, which will consume electrons. and the number of holes, resulting in a decrease in the number and concentration of photons, which has a great impact on the luminous efficiency of LEDs

Method used

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Embodiment 1

[0058] figure 2 It is a schematic flow chart of the LED manufacturing method provided by Embodiment 1 of the present invention. Such as figure 2 As shown, this embodiment provides a method for manufacturing an LED, comprising: forming an AlN layer on a substrate; growing an undoped GaN layer and an N-type GaN layer sequentially on the AlN layer; growing an electron diffusion layer on the N-type GaN layer ; growing a stress release layer on the electron diffusion layer; growing a light emitting layer on the stress release layer; growing a P-type GaN layer on the light emitting layer.

[0059] In this embodiment, GaN-based LEDs are grown on the substrate by MOCVD reaction. The substrate can be (0001) surface sapphire, and high-purity hydrogen, high-purity nitrogen, or a mixture of high-purity hydrogen and high-purity nitrogen can be used as the carrier gas , high-purity ammonia gas is used as the N source; in metal-organic sources, trimethylgallium (TMGa) and triethylgallium...

Embodiment 2

[0124] In this embodiment, the step S140 in the first embodiment: growing the stress release layer on the electron diffusion layer specifically includes the following steps:

[0125] Step c1: After S130, stop feeding metal-organic source and SiH 4 , maintain for 200-300 seconds, keep the pressure at 150-400 torr, continuously feed 30-300 liters / min of nitrogen as a carrier gas, continuously feed 30-200 liters / min of ammonia, reduce the temperature of the reaction chamber to 850 -950°C.

[0126] Step d1: maintain the reaction temperature at 850-950°C and the pressure at 100-300 torr, feed 30-300 liters / minute of nitrogen as a carrier gas for 300-400 seconds, and continuously feed 30-200 liters / minute of nitrogen at the same time Ammonia, 50-200 ml / min of the first gallium source and 2-10 ml / min of SiH at 200ppm 4 , grow a Si-doped N-type GaN layer with a thickness of 30-60nm on the electron diffusion layer, and the Si doping concentration is 1 E+18atoms / cm 2 -1E+19atoms / cm ...

Embodiment 3

[0135] In the LED manufacturing method provided in this embodiment, the above step S140 specifically includes the following steps:

[0136] Step c2: after S130, stop feeding metal-organic source and SiH 4 , maintained for 200 seconds, the pressure gradually changed from 150 torr to 250 torr, the continuous nitrogen gas was gradually changed from 50 liters / minute to 100 liters / minute, and the continuous ammonia gas was gradually changed from 60 liters / minute to 50 liters / min, the temperature of the reaction chamber gradually changes from 1000°C to 900°C.

[0137] Step d2: maintain the reaction temperature at 900°C and the pressure at 250 torr, and continue to feed 100 liters / minute of nitrogen as a carrier gas for 300 seconds, while continuously feeding 50 liters / minute of ammonia and 100 ml / minute of the first Gallium source and 6 mL / min of 200 ppm SiH 4 , grow a Si-doped N-type GaN layer with a thickness of 30-60nm on the electron diffusion layer, and the Si doping concent...

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Abstract

The invention provides an LED preparation method and an LED. The LED preparation method provided by the invention comprises the steps of forming an AlN layer on a substrate; growing an undoped GaN layer and an N-type GaN layer on the AlN layer in sequence; growing an electron diffusion layer on the N-type GaN layer; growing a stress release layer on the electron diffusion layer; growing a light-emitting layer on the stress release layer; and growing a P-type GaN layer on the light-emitting layer. According to the LED preparation method provided by the invention, the electron and hole recombination probability is relatively high; and the light-emitting efficiency of the LED is relatively high.

Description

technical field [0001] The present invention relates to the technical field of light-emitting diodes (Light-Emitting Diode, LED for short), in particular to a method for preparing an LED and the LED. Background technique [0002] LED (Light Emitting Diode, Light Emitting Diode) is a semiconductor device that generates light by recombination of electrons and holes to generate photons. At present, gallium nitride (GaN)-based LED chips are widely used due to their advantages of environmental protection, high efficiency, energy saving and long life. [0003] At present, GaN-based LEDs use Metal-organic Chemical Vapor Deposition (MOCVD) technology to grow epitaxial layer light-emitting structures on sapphire substrates using InGaN / GaN, a common material for quantum wells, as the main light-emitting material. . figure 1 It is the structure of the existing GaN-based LED. Such as figure 1 As shown, the structure includes an AlN substrate 110 and an undoped GaN layer 120, an N-ty...

Claims

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Application Information

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IPC IPC(8): H01L33/00H01L33/02H01L33/12H01L33/32
CPCH01L33/0075H01L33/02H01L33/12H01L33/325
Inventor 张宇康建杨天鹏戚雪林周荣
Owner JIANGXI EPITOP OPTOELECTRONICS
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