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Binding material and binding method of sputtering target

A sputtering target and binding technology, applied in the field of sputtering coating, can solve problems such as difficult-to-bind target binding

Active Publication Date: 2021-10-22
PIONEER MATERIALS INC CHENGDU
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] The purpose of the present invention is to provide a binding material and a binding method, which can easily solve the above-mentioned problems existing in the traditional indium binding, and can realize the binding of traditional targets and targets that are difficult to bind

Method used

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  • Binding material and binding method of sputtering target
  • Binding material and binding method of sputtering target
  • Binding material and binding method of sputtering target

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Experimental program
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Effect test

preparation example Construction

[0040] Preparation of the binding material: carbon nanotubes (inner diameter <6nm, length 500nm-30000nm, accounting for 10wt% of the mass of the silica gel) are mixed into the silica gel to form CNT silica gel, which is prepared by mechanically stirring for 1-5 minutes after adding a conductive dispersant . The stirring speed is 50-200 rpm, and the principle is not to increase the temperature of the CNT silica gel too much, so as to avoid the partial curing of the CNT silica gel due to high temperature.

[0041]Bonding of CNT silica gel: Uniformly coat CNT silica gel with a thickness of 0.1 mm or more on the bonding surfaces of the back plate and the target by coating. Then place the back plate and the target material in a horizontal manner, so that the joint surfaces are in contact with each other and apply appropriate pressure (depending on the type of target material, a small pressure should be applied to brittle and soft materials, and a gravity of 2 to 50Kg should be appl...

Embodiment 1

[0043] Embodiment 1 is mixed with the conductive performance of carbon nanotube silica gel

[0044] The resistivity of silica gel not doped with carbon nanotubes is greater than 200MΩ-cm. In order to verify that doping with carbon nanotubes (addition of 5wt% to 13wt%) can improve the conductivity of silica gel, the conductivity of doped carbon nanotubes with different thicknesses can be improved. The performance was studied and the results are shown in Table 1 below:

[0045] Table 1 Conductivity of silica gel with different thickness without adding / adding carbon nanotubes

[0046] Silicone thickness ResistivityΩ-cm Sheet resistance Ω / □ Silica gel not doped with carbon nanotubes (any thickness) >>200M(insulator) >>200M(insulator) Silica gel doped with carbon nanotubes (0.3mm) 4.9X10 -1

[0047] It can be seen from the above table 1 that the silica gel not mixed with carbon nanotube silica gel is an insulator at any thickness, and does not have ele...

Embodiment 2

[0048] Example 2 Indium and CNT silica gel sputtering coating XRD at different power sources

[0049] Using CIGS copper indium gallium selenide (Cu 22.68%, In 16.21%, Ga 6.78%, Se 54.33%) as the target, and the substrate temperature during sputtering is 550°C, to study indium binding or CNT silica gel binding under different power sources The sputtered coating XRD diffraction pattern, the results are as follows Figure 1 to Figure 6 shown.

[0050] figure 1 , image 3 and Figure 5 Three XRD patterns of indium binding with figure 2 , Figure 4 and Figure 6 The three XRD patterns of CNT silica gel binding show a typical chalcopyrite crystal structure. The typical structure of copper indium gallium selenide film is chalcopyrite crystal structure, and when Ga and In and Ga(Ga / (In+Ga )) has an atomic ratio of 0.3 and its 2θ values ​​are 26.897°, 44.645°, and 52.94°, and its characteristic peaks correspond to the diffraction peaks of (112), (220), and (312) crystal planes ...

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Abstract

The invention provides a binding material for a sputtering target and belongs to the technical field of sputtering coating. The binding material is obtained by mixing carbon nanotubes into silica gel to form CNT silica gel, adding a conductive dispersant and then mechanically stirring. The present invention also provides a binding method for binding the target. The binding material is coated on the bonding surface of the back plate and the target, so that the bonding surfaces are in contact with each other and pressure is applied. The silica gel of the nanotubes is fully cured to realize the binding of the target. The present invention mixes carbon nanotubes into silica gel, utilizes the electrical and thermal conductivity of carbon nanotubes to make the originally non-conductive and thermally conductive silica gel into thermally conductive and electrically conductive silica gel, and uses the silica gel with electrical and thermal conductivity as the target material binding. By adopting the binding material of the present invention, stable, safe and low-temperature targets can be obtained for planar targets, rotating targets, thick targets, thin targets, metals, non-metals, oxide ceramic targets, and chalcogen-containing targets that are difficult to bind. binding.

Description

technical field [0001] The invention belongs to the technical field of sputtering coating, and relates to a binding material, in particular to a binding material and a binding method for a sputtering target. Background technique [0002] The sputtering process is a method of making thin films. Through sputtering, the compound of the target can be plated on the preset object. The thickness of the obtained film is uniform and environmentally friendly. Therefore, sputtering is often used in semiconductor coatings, especially when the film thickness is 10nm. Semiconductor coating between -5000nm. For example, to coat a piece of flat glass with gold, silver, copper, or other metal or oxide compounds, as long as the target of gold, silver, copper, or other metal or oxide compounds is installed in the vacuum chamber On the target base (Sputter cathode), apply the appropriate current and voltage to the target base and cooperate with the appropriate argon atmosphere to obtain the re...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C14/34
CPCC23C14/3407
Inventor 林刘毓张力平丘立安
Owner PIONEER MATERIALS INC CHENGDU