Low alpha epoxy molding compound and preparation method thereof
A technology of epoxy molding compound and epoxy resin, applied in low alpha epoxy molding compound, preparation of epoxy molding compound, epoxy molding compound field, can solve the problems of device deterioration, instant failure, missile runaway and the like
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[0084] The present invention also relates to the preparation method of epoxy molding compound, it comprises the following steps:
[0085] (1) each component is weighed and mixed to obtain a premixed powder,
[0086] (2) Heat and mix the premixed powder and extrude to obtain the product;
[0087] Wherein the temperature of heating in step (2) is about 90-120 ℃.
[0088] Wherein the step (1) also includes the step of cleaning the equipment used to prepare the epoxy molding compound. Cleaning is called A-level cleaning. After the equipment used in the preparation of epoxy molding compound is disassembled, it is moved to the soot blowing room for cleaning, and after the cleaning is completed, ensure that there is no dust, accumulated material, or solidified material inside the equipment. Cleaning includes brushing to remove solids such as dust, build-up, solidified material, etc. in the equipment, and / or wiping the equipment with acetone. Cleaning includes cleaning the equipmen...
Embodiment
[0118] The present invention is described in further detail with reference to the following examples, which are not intended to limit the scope of the present invention. All numbers in the examples are expressed as parts by weight.
[0119] raw material
[0120] Epoxy resin: biphenyl type epoxy resin, viscosity at 150°C is about 0.2 poise, epoxy equivalent is 190g / eq, purchased from Mitsubishi, generally has the following structure
[0121]
[0122] Multi-functional epoxy resin, the epoxy equivalent is 160g / eq, purchased from Kayaku, generally has the following structure
[0123]
[0124] Phenolic resin: multifunctional phenolic resin with a softening point of 110°C, purchased from Minghe, generally has the following structure
[0125]
[0126] Curing accelerator: imidazole compound, purchased from SHIKOKU;
[0127] Filler: spherical silica A, alpha value 0.00864 counts per hour -1 ·cm -2 , with a uranium content of 0.5ppb, a sphericity of 0.89, and a particle ...
PUM
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Abstract
Description
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