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Preparation method of novel compound sweetener

A compound sweetener and a new technology, applied in the field of sweeteners, can solve the problems of large pollution degree, development restriction, bad taste, etc., and achieve the effects of reasonable compounding, pure sweetness and ideal cost.

Inactive Publication Date: 2019-09-06
SHANDONG BENYUE BIOTECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] With the improvement of people's living standards, people's demand for dietary quality is getting higher and higher. As the main flavoring substance, sweeteners are constantly innovating and increasing, adding many wonderful experiences to people's diets. Among them, sodium saccharin is the earliest However, due to the high degree of pollution in the production process, the development is limited, cyclamate, steviol glycoside and mogroside have bad taste, and traditional sucrose has the disadvantage of high calories, especially not suitable for people with high blood sugar and diabetes. The deficiencies of the above-mentioned various sweeteners require the generation of a new type of compound sweetener to adapt to changes in market demand

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A preparation method of a novel compound sweetener, comprising the following steps:

[0022] Add 90 grams of erythritol, 1 gram of neotame, 10 grams of cyclamate and 5 grams of hesperetin dihydrochalcone-7-O-glucoside into purified water and dissolve at 30°C to prepare a sugar solution. The temperature of the prepared sugar solution is raised to 65°C, adding diglyceride to adjust the pH value of the sugar solution between 1-6, cooling down to 10°C at a cooling rate of 5°C / h for crystallization, crystallization for 24 hours, and suction filtration And at a temperature of 55° C., dried for 8 hours to obtain white crystals, the mouthfeel test was between 100-200, the mouthfeel was soft, and had a creamy mouthfeel.

[0023] Wherein, the preparation method of the hesperetin dihydrochalcone-7-O-glucoside is obtained by using neohesperetin dihydrochalcone as a starting material and removing rhamnose by rhamnosidase.

Embodiment 2

[0025] A preparation method of a novel compound sweetener, comprising the following steps:

[0026] 85 grams of glucose, 3 grams of neotame, 5 grams of cyclamate and 7 grams of hesperetin dihydrochalcone-7-O-glucoside were added to purified water and dissolved at 40°C to prepare a sugar solution. The prepared Heat the sugar solution to 70°C, add citric acid to adjust the pH value of the sugar solution between 1-6, cool down to 20°C at a cooling rate of 5°C / h for crystallization, crystallize for 24 hours, suction filter and dry at 50°C Dry for 9 hours at a temperature of 100°F to obtain white crystals. The taste test is between 200-400. The taste is soft and has a creamy taste.

Embodiment 3

[0028] A preparation method of a novel compound sweetener, comprising the following steps:

[0029] 80 grams of xylitol, 5 grams of neotame, 0.5 grams of cyclamate and 10 grams of hesperetin dihydrochalcone-7-O-glucoside were added to purified water and dissolved at 25°C to prepare a sugar solution. The temperature of the obtained sugar solution was raised to 60°C, adding citric acid to adjust the pH value of the sugar solution between 1-6, cooling to 0°C at a cooling rate of 2°C / h for crystallization, crystallization for 24 hours, suction filtration and Dry at 40°C for 10 hours to obtain white crystals. The taste test is between 10-100. The taste is light and has a creamy taste.

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Abstract

The invention belongs to the technical field of sweeteners, and particularly relates to a preparation method of a novel compound sweetener. The preparation method of the novel compound sweetener comprises the following steps: mixing a sweet carrier, neotame, cyclamate and hesperidin dihydrochalcone-7-O-glucoside according to a certain mass ratio, and dissolving with purified water at a low temperature to prepare a sugar solution; heating the sugar solution obtained in the step (1) to the temperature of 60-70 DEG C, and adding diglyceride or citric acid to enable the pH value of the sugar solution to be 1-6; and cooling to the temperature of 0-20 DEG C, crystallizing for 24-48 h, and drying to obtain the novel compound sweetener. The preparation method of the novel compound sweetener provided by the invention is reasonable in compound, the sweet taste has a creamy taste, the sweet taste is pure, the cost is not high, the novel compound sweetener can be used as a sweetener, a flavoring agent or a flavoring agent, and the novel compound sweetener can be widely applied to products such as foods, medicines, feeds and daily chemicals.

Description

technical field [0001] The invention belongs to the technical field of sweeteners, and in particular relates to a preparation method of a novel compound sweetener. Background technique [0002] With the improvement of people's living standards, people's demand for dietary quality is getting higher and higher. As the main flavoring substance, sweeteners are constantly innovating and increasing, adding many wonderful experiences to people's diets. Among them, sodium saccharin is the earliest However, due to the high degree of pollution in the production process, the development is limited, cyclamate, steviol glycoside and mogroside have bad taste, and traditional sucrose has the disadvantage of high calories, especially not suitable for people with high blood sugar and diabetes. The deficiency of above-mentioned various sweeteners needs the generation of a kind of novel compound sweetener to adapt to the demand change of market. Contents of the invention [0003] The purpos...

Claims

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Application Information

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IPC IPC(8): A23L27/30A23L27/21A23L27/20A23K20/105A23K20/111A23K20/121A61K47/18A61K47/20A61K47/22A61K8/44A61K8/46A61K8/60A61Q19/00
CPCA23L27/32A23L27/30A23L27/21A23L27/204A23L27/203A23L27/2052A23K20/105A23K20/111A23K20/121A61K47/183A61K47/20A61K47/22A61K8/44A61K8/466A61K8/602A61Q19/00A23V2002/00A61K2800/10A23V2250/2484A23V2250/246A23V2200/16
Inventor 陈良王振东刘传滨
Owner SHANDONG BENYUE BIOTECH
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