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Preparation method of novel high-sensitivity 3D printing flexible sensor

A flexible sensor and 3D printing technology, applied in the field of sensors, can solve the problems of reduced service life, performance stability and sensitivity, single appearance of flexible sensors, and limited use of precision processing, so as to ensure performance and sensitivity, and good line width and arrays, performance-enhancing effects

Active Publication Date: 2019-09-17
WUYI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Secondly, the conventional manufacturing process usually adopts compression molding, and the appearance of the produced flexible sensor is relatively simple, the function is also simple, and the size is large.
Due to the large size of flexible sensors made by conventional processes, their use in precision machining is limited, and their service life, performance stability and sensitivity are reduced.

Method used

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  • Preparation method of novel high-sensitivity 3D printing flexible sensor
  • Preparation method of novel high-sensitivity 3D printing flexible sensor
  • Preparation method of novel high-sensitivity 3D printing flexible sensor

Examples

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Embodiment 1

[0033] A method for preparing a novel high-sensitivity 3D printed flexible sensor, comprising the following steps:

[0034] S1), at room temperature, mix 2g of PDMS and 3.7g of flake Ag, and mix evenly through Mixer equipment at a speed of 1000 / min;

[0035] S2), at normal temperature, mix 43mg of Rh catalyst and 45mg of PMHS crosslinking agent with the solution prepared in step S1), and then perform Mixer to mix evenly;

[0036] S3), at room temperature, mix the second-phase solution composed of 50 mg of deionized water and 7 mg of IL with the solution prepared in step S2), and use a Mixer to rotate at 2000 rpm for 2 minutes to mix evenly;

[0037] S4), at room temperature, use Rolling to process and mix the solution completed in step S3), with a gap of 8 μm;

[0038] S5), drying the colloidal solution prepared in step S4), and keeping it warm for 10 minutes at a temperature of 120° C.;

[0039] S6), placing the Ag-PDMS rheological body of the capillary suspension on the 3D...

Embodiment 2

[0041] A method for preparing a novel high-sensitivity 3D printed flexible sensor, comprising the following steps:

[0042] S1), at room temperature, mix 2g of PDMS and 3.7g of flake Ag, and mix evenly through Mixer equipment at a speed of 1000 / min;

[0043] S2), at normal temperature, mix 43mg of Rh catalyst and 45mg of PMHS crosslinking agent with the solution prepared in step S1), and then perform Mixer to mix evenly;

[0044] S3), at room temperature, mix the second-phase solution composed of 50 mg of deionized water and 4 mg of IL with the solution prepared in step S2), and use a Mixer to rotate at 2000 rpm for 2 minutes to mix evenly;

[0045] S4), at room temperature, use Rolling to process and mix the solution completed in step S3), with a gap of 8 μm;

[0046] S5), drying the colloidal solution prepared in step S4), and keeping it warm for 10 minutes at a temperature of 120° C.;

[0047]S6), placing the Ag-PDMS rheological body of the capillary suspension on the 3D ...

Embodiment 3

[0049] A method for preparing a novel high-sensitivity 3D printed flexible sensor, comprising the following steps:

[0050] S1), at room temperature, mix 2g of PDMS and 3.7g of flake Ag, and mix evenly through Mixer equipment at a speed of 1000 / min;

[0051] S2), at normal temperature, mix 43mg of Rh catalyst and 45mg of PMHS crosslinking agent with the solution prepared in step S1), and then perform Mixer to mix evenly;

[0052] S3), at room temperature, mix the second-phase solution composed of 50 mg of deionized water and 2 mg of IL with the solution prepared in step S2), and use a Mixer to rotate at 2000 rpm for 2 minutes to mix evenly;

[0053] S4), at room temperature, use Rolling to process and mix the solution completed in step S3), with a gap of 8 μm;

[0054] S5), drying the colloidal solution prepared in step S4), and keeping it warm for 10 minutes at a temperature of 120° C.;

[0055] S6), placing the Ag-PDMS rheological body of the capillary suspension on the 3D...

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Abstract

The invention provides a preparation method of a novel high-sensitivity 3D printing flexible sensor. The method is based on a capillary suspension, PDMS is used as a first phase liquid, IL is used as a second phase liquid, a silver powder or silver sheet is used as a conductive carrier, Rh is used as a catalyst, PMHS is used as a crosslinking agent, the suspension is composed of the first phase liquid and the second phase liquid, and then combined with the silver powder or silver sheet to form a conductance-type sensor flexible conductive material colloid. According to the method, a main body of a high telescopic deformation polymer colloid is formed by the PDMS colloid, the PMHS crosslinking agent and the Rh catalyst, and hydrophobic Ag particles provide electrical conductivity. The Ag-PDMS colloid of a flexible sensor based on the capillary force suspension is prepared by using the first phase liquid and the second phase liquid. Compared with a conventional sensor colloid, the performance of the flexible sensor colloid is improved, links of silver particles are increased through a second phase solution, silver particle strings are formed, and thus electrical conductivity is effectively increased.

Description

technical field [0001] The invention relates to the technical field of sensors, in particular to a method for preparing a novel high-sensitivity 3D printed flexible sensor. Background technique [0002] Flexible sensors have very promising applications, including in medical electronics, environmental monitoring, and wearables. For example, in the field of environmental monitoring, equipment with flexible sensors can monitor the level of typhoons and rainstorms. On the wearable side, flexible sensors can test relevant parameters of the skin. [0003] The flexible sensor is mainly composed of metal materials (gold At, silver Ag, copper Cu), inorganic semiconductor materials (zinc oxide ZnO, zinc sulfide ZnS), organic materials, active materials and flexible substrates (polydimethylsiloxane PDMS) . The colloid formed by conventional flexible sensors has low electrical conductivity, a high mass percentage of metal materials, high cost, and limited stretching deformation. [...

Claims

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Application Information

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IPC IPC(8): B01J13/00C08K3/08C08L83/04B33Y70/00
CPCB01J13/00C08K3/08B33Y70/00C08K2003/0806C08L2203/20C08K2201/001C08L83/04
Inventor 陈毅湛曾庆光李远兴赵丽特金婷婷余志豪
Owner WUYI UNIV