A kind of UV isolation oil suitable for instant lottery printing and preparation method thereof
An acrylic resin and modified technology, which is applied in coatings, epoxy resin coatings, etc., can solve the problems of poor adhesion of the scratch-off ink layer, unfavorable spreading of the scratch-off ink, unfavorable scratch-off layer and easy scraping, etc. , to achieve the effect of easy curing, good adhesion and simple preparation method
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Embodiment 1
[0038] UV isolation oil components:
[0039] 10g of epoxy acrylic resin, 10g of modified acrylic resin, 0.1g of polydimethylsiloxane, 0.05g of trimethylcyclosiloxane, 66g of reactive diluent, 12g of photoinitiator and 3g of co-initiator.
[0040] Wherein, the reactive diluent is 1,6-hexanediol acrylate and trimethylolpropane triacrylate with a mass ratio of 1:5, and the photoinitiator is 1-hydroxycyclohexanebenzene with a mass ratio of 1:2 ketones and benzophenones;
[0041] Preparation of modified acrylic resin:
[0042] 1) Synthesis of acrylic resin
[0043] In a four-necked flask equipped with a reflux condenser and a stirrer, add 80 g of toluene, raise the temperature to 120 ° C, and slowly add 50 g of acrylic acid, 25 g of methyl methacrylate, 30 g of ethyl acrylate, tert-butyl peroxide dropwise under stirring. Mixed solution of 1.5g of hydrogen oxide, reacted for 1.5h, added 0.5g of tert-butyl hydroperoxide, kept warm for 0.75h, cooled while stirring, and cooled to 40...
Embodiment 2
[0054] UV isolation oil components:
[0055] 8g of epoxy acrylic resin, 12g of modified acrylic resin, 0.08g of polydimethylsiloxane, 0.08g of trimethylcyclosiloxane, 75g of reactive diluent, 10g of photoinitiator and 5g of co-initiator.
[0056] Wherein, the reactive diluent is 1,6-hexanediol acrylate and trimethylolpropane triacrylate with a mass ratio of 1:6, and the photoinitiator is 1-hydroxycyclohexanebenzene with a mass ratio of 1:3 ketones and benzophenones;
[0057] Preparation of modified acrylic resin:
[0058] 1) Synthesis of acrylic resin
[0059] In a four-neck flask equipped with a reflux condenser and a stirrer, add 40 g of toluene, raise the temperature to 110 ° C, and slowly add 40 g of acrylic acid, 20 g of methyl methacrylate, 20 g of ethyl acrylate, tert-butyl peroxide dropwise under stirring. Mixed solution of 0.3g of hydrogen oxide, reacted for 1h, added 0.1g of tert-butyl hydroperoxide, kept warm for 0.5h, cooled while stirring, and cooled to 40°C to...
Embodiment 3
[0070] UV isolation oil components:
[0071] 12g of epoxy acrylic resin, 8g of modified acrylic resin, 0.1g of polydimethylsiloxane, 0.05g of trimethylcyclosiloxane, 60g of reactive diluent, 13g of photoinitiator and 2g of co-initiator.
[0072] Wherein, the reactive diluent is 1,6-hexanediol acrylate and trimethylolpropane triacrylate with a mass ratio of 1:5, and the photoinitiator is 1-hydroxycyclohexanebenzene with a mass ratio of 1:3 ketones and benzophenones;
[0073] Preparation of modified acrylic resin:
[0074] 1) Synthesis of acrylic resin
[0075] In a four-neck flask equipped with a reflux condenser and a stirrer, add 80 g of toluene, raise the temperature to 125 ° C, and slowly add 60 g of acrylic acid, 30 g of methyl methacrylate, 40 g of ethyl acrylate, tert-butyl peroxide dropwise under stirring. Mixed solution of 2g of hydrogen oxide, after reacting for 2 hours, add 1g of tert-butyl hydroperoxide, keep warm for 1 hour, cool while stirring, and cool down to...
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