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53results about How to "Moderate surface tension" patented technology

Polymer waterborne polyester and preparation method thereof

The invention discloses polymer waterborne polyester. The polymer waterborne polyester is prepared in the mode that terephthalic acid (PTA), isophthalic acid (IPA), ethylene glycol (BG), diethylene glycol, ternary monomers, a catalyst and other auxiliaries serve as raw materials, and the raw materials and mother liquid are subjected to esterification and condensation polymerization for synthesis. A preparation method of the polymer waterborne polyester includes the steps that firstly, terephthalic acid (PTA), isophthalic acid (IPA), ethylene glycol (BG), diethylene glycol and ternary monomers are made into paste and evenly fed into an esterification kettle through a metering pump, the catalyst is added for an esterification reaction, the auxiliaries are added to monomers generated by the esterification reaction, the mixture is filtered and guided into a condensation polymerization kettle for a condensation polymerization reaction, when a certain process value is reached, the mixture is extruded out through nitrogen, and the transparent polyester product is prepared after cooling, grain-sized dicing, drying and screening. The polymer waterborne polyester replaces traditional acrylic and vinyl acetate products, and urea resin and cyanamide resin which are not environmentally friendly, has a series of advantages of being excellent in adhesive force, high in molecular weight, good in environment friendliness and the like, and can serve as a textile hardening agent to be widely used.
Owner:广州市弘浩纺织助剂有限公司

Method for inhibiting splashing in steelmaking process of converter

ActiveCN108486306ASmall splash rateSuitable breathabilityManufacturing convertersProcess efficiency improvementIron oxideMagnesium
The invention relates to a method for inhibiting the splashing in a steelmaking process of a converter, which belongs to the field of converter steelmaking. The method comprises the following steps: determining an appropriate addition amount of waste steel cold material and an addition amount of first batch materials for blowing according to the temperature, components and slag content of molten iron entering the converter as well as the slag residual situation of the previous process, enabling the alkalinity range of the steel slag to be 1.4 to 1.9 when an oxidation period of silicon and manganese is ended, wherein the content of MgO in the slag is 5 to 7 percent, the content of TFe is 18 to 24 percent, and the temperature of the molten iron is 1390 to 1420 DEG C; at a first carbon/phosphorus oxidation reaction selection point, adding a slag making material comprising calcium and magnesium in different batches for multiple times as well as a cold material comprising the iron oxide, wherein at the second carbon/phosphorus oxidation reaction selection point, the alkalinity range of the steel slag is 2.8 to 3.5, the MgO content in the slag is 7 to 10 percent, and the content of TFe is 15 to 20 percent; and in the later period of the blowing, operating by virtue of a pressure gun. By adopting the method, a slag making process is ensured to be adaptive to a reaction process of themolten iron in the blowing of the converter, so that the air permeability and viscosity of the furnace slag in the blowing process can be matched with the reaction rate of carbon removal, silicon removal and manganese removal of the molten steel, and the splashing problem in the steelmaking process of the converter is solved.
Owner:TIANJIN IRON & STEEL GRP

Quick-drying primer for renovating exterior wall tiles and preparation method thereof

The invention relates to quick-drying primer for renovating exterior wall tiles and a preparation method thereof. The preparation method comprises the following steps of adding water and a styrene-acrylic emulsion into a dispersion cylinder, sequentially adding a multifunctional auxiliary agent, a sterilization preservative, a dispersing agent, a wetting agent and a defoaming agent, and uniformlystirring, adding micron-sized titanium dioxide, coarse whiting powder and talcum powder, increasing the rotating speed and uniformly stirring, reducing the rotating speed, sequentially adding the styrene-acrylic emulsion, the defoaming agent, the antifreeze agent, the coalescing agent, the paint film reinforcing agent and the thickening agent, and uniformly stirring to obtain the quick-drying primer. The quick-drying primer prepared by the invention has excellent adhesive force on the surface of a ceramic tile, and has the characteristics of low cost, covering power, moderate surface tension,quick drying and the like; a paint film is excellent in water resistance, and the adhesive force is not changed after water resistance; the primer is simple and convenient to construct, the primer isa single-component material, and after the surface of the ceramic tile is simply sprayed with the primer, a further surface coating effect, such as stone imitation, embossment, solar heat reflection and self-cleaning, can be achieved instead of simple flat coating.
Owner:YANGZHOU POLYTECHNIC INST

Solid capacitor carbon foil nano conductive carbon paste and preparation method thereof

The invention relates to solid capacitor carbon foil nano conductive carbon paste and a preparation method thereof. The solid capacitor carbon foil nano conductive carbon paste comprises a polymer carrier and a nano conductive carbon fiber system dispersed in the polymer carrier, wherein the polymer carrier is formed by mixing an adhesive, a polymer solvent and a processing aid; the nano conductive carbon fiber system comprises a carbon nano tube and an acidified carbon nano tube acidified by a mixed solution of concentrated nitric acid and concentrated sulfuric acid; the adhesive is one or more of polyester acrylic resin, waterborne polyurethane resin, epoxy acrylic resin and polyurethane resin; the polymer solvent is several in butyl cellosolve, polyoxyethylene alkyl phenyl ether, methylbenzyl alcohol, N, N-dimethylformamide and terpilenol. The nano conductive carbon fiber system is dispersed in the polymer carrier, so that the microscopic coverage compactness of a carbon layer is improved; and the solid capacitor carbon foil nano conductive carbon paste is suitable for a solid capacitor carbon foil, protects a current collector, prevents the surface of the aluminum foil from being oxidized or corroded, and greatly reduces the ESR of a solid capacitor.
Owner:南通宇华新材料科技有限公司

Method for extracting and recovering acanthopanax total flavonoids by using deep eutectic solvent

The invention belongs to the technical field of extraction and purification of effective components of traditional Chinese medicines, and particularly discloses a method for extracting and recycling acanthopanax total flavonoids by using a deep eutectic solvent. The method comprises the following steps: by taking powder of acanthopanax roots as a raw material, adding a deep eutectic solvent with a certain water content, extracting acanthopanax total flavonoids under an ultrasonic-assisted condition, and enriching and recovering flavonoid compounds in an extracting solution by using macroporous resin, and meanwhile, after the water in the obtained eutectic recovery liquid is evaporated, extracting the acanthopanax total flavonoids again, wherein the acanthopanax total flavonoids can be repeatedly utilized for at least three times. The invention develops a novel process technology for extracting and enriching the acanthopanax total flavonoid compounds from the acanthopanax roots and stems by combining the eutectic solvent with the macroporous resin, the recycling of the eutectic solvent is realized, and the purposes of greenness, high efficiency and repeatable extraction are achieved. Compared with a traditional extraction method, the method has the advantages of no use of an organic solvent, simplicity and convenience in operation, time saving, safety, low cost and the like, and industrial production can be realized.
Owner:LIAOCHENG UNIV

Fast quenching amorphous alloy ribbon and preparation method thereof

This invention belongs to the field of metal material preparation, in particular relates to a fast quenching amorphous alloy ribbon and a preparation method thereof. The preparation method of the fast quenching amorphous alloy ribbon comprises the steps of batching, vacuum melting, secondary melting, ribbon spouting and collecting, and the chemical components are 70 to 85 percent of Fe, 0.001 to 4 percent of Nb, or at least one of Nb, Mo, W, V and Ta, 0.001 to 25 percent of Si, 0.001 to 15 percent of B, 0.001 to 2 percent of Cu, 0.005 to 0.08 percent of at least one of Al and Ti according to the atomic percent. In the ribbon spouting step, a dynamic stable arc weld pool with the both ends protruding outward is formed between a nozzle and a cooling roller, and the temperature of the weld pool is 1180 to 1300 DEG C; the width D of the nozzle gap is 0.1 to 0.4 millimeters, and the space length between the cooling roller and the nozzle is 0.1 to 0.4 millimeters; the thickness of the ribbon is 18 to 24 micrometers, and the roughness Ra is smaller than 2 micrometers. The ribbon has very thin thickness, excellent surface quality and magnetic property, and is suitable for producing high-quality magnet core elements. The ribbon is particularly suitable for being used under high frequency, and has lower high frequency loss and better frequency characteristics.
Owner:AT&M AMORPHOUS TECH CO LTD

Interface pretreatment liquid for silicon-oxygen pre-lithiation negative electrode as well as preparation method and application of interface pretreatment liquid

The invention relates to an interface pretreatment liquid for a silicon-oxygen pre-lithiation negative electrode as well as a preparation method and application of the interface pretreatment liquid. The interface pretreatment liquid comprises 0.1%-10% of solute and 90%-99.9% of solvent, the solvent is one or more selected from N-methyl pyrrolidone, ethylene carbonate, fluoroethylene carbonate, propylene carbonate, butylene carbonate, dimethyl carbonate, diethyl carbonate, ethyl methyl carbonate, gamma-butyrolactone, methyl formate, ethyl formate, methyl acetate, ethyl acetate, ethyl propionate, propyl propionate, ethyl butyrate, propyl butyrate, dimethyl sulfoxide, ethylene glycol dimethyl ether, 1, 3-dioxolane, dipolyethylene glycol dimethyl ether and dimethyl thionyl ether; and the solute is selected from one or more of lithium polysulfide, aluminum iodide, aluminum bromide, lithium nitrate and copper nitride. The solvent can fully infiltrate the internal pores of the lithium-rich negative plate and the surface of the negative active material, and the solute can react with the negative material, so that the stability of the SEI membrane is improved, and the first charge-discharge efficiency and long-term cycle performance of the battery are synergistically improved.
Owner:KUNSHAN BAOTRON NEW ENERGY TECH CO LTD

Enamel color material, preparation method thereof, and application in porcelain body painting enamel cultural relic repair

The invention discloses an enamel color material, a preparation method thereof, and an application of the enamel color material in porcelain body painting enamel cultural relic repair. The enamel color material is prepared from the following chemical components in percentage by mass: 33%-51% of silicon dioxide, 0%-3.8% of aluminum oxide, 8%-19% of boron oxide, 31%-53% of lead oxide, 0%-6% of calcium oxide and magnesium oxide, 0%-6.9% of sodium oxide and potassium oxide, 0.5%-6% of bismuth trioxide, 0%-7.2% of tin oxide, 0%-6.5% of antimonous oxide, 0%-13% of ferric oxide, 0%-4.2% of copper oxide, 0%-4% of cobalt oxide, 0%-9% of manganese oxide, 0%-2% of silver oxide and 0%-0.15% of gold oxide. Compared with the traditional enamel painted porcelain, the enamel painted porcelain provided bythe invention has the advantages that the melting point is lower; the colored glaze and an ancient enamel colored pigment layer show a "like-fusion-like" phenomenon at high temperature, can be matchedwith the thermal expansion coefficients of the surface glaze and the pigment layer of the traditional enamel color, has good adhesiveness and good adhesiveness before firing, is easy to disperse, hasmoderate material surface tension in the firing and fusing process, not only meets the fusing property, but also can keep a certain colored drawing three-dimensional shape.
Owner:佛山市天工嘉荟文化科技有限公司 +1

A kind of production method of environment-friendly size polyester for fabric sizing

The invention provides a production method of an environment-friendly polyester slurry. The production method comprises the following steps: (1) putting right amounts of ethylene glycol and terephthalic acid into a slurrying kettle, and stirring into a slurry; (2) carrying out esterification reaction on the slurry in an esterification kettle at 255-265 DEG C, sending the water generated by esterification and volatile ethylene glycol into a fractionating column to perform separation, and controlling the column top temperature by a column top condenser water inlet regulating valve and an external reflux regulating valve, thereby separating out the esterification water; weighing the obtained esterification water, and judging that the esterification reaction is finished when the weighed water is greater than or equal to 95 wt% of the theoretical generated water; (3) polycondensation reaction: carrying out two steps in a vacuum state, and judging the end point of the polycondensation reaction according to the stirring power of the polycondensation reaction kettle; and (4) granulating or slicing. The production method has the advantages of simple technique and stable operation. By adopting the process of judging the end point of the polycondensation reaction according to the stirring power of the polycondensation reaction kettle, the production method is simple, feasible and easy to operate in mass production, and saves the human resources and material resources.
Owner:湖北尚助化学有限公司
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