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38results about How to "Strengthen the bridging effect" patented technology

Plugging material and plugging slurry for protecting reservoir stratum with low fracturing fracture ability

The invention discloses a plugging material and plugging slurry for protecting a reservoir stratum with the low fracturing fracture ability. The plugging material is prepared from, by weight, 5-6 parts of walnut shell powder, 2-3 parts of a composite plugging agent, 1.5-2 parts of an agent for plugging while drilling, 4-5 parts of an acid soluble plugging agent, 4-5 parts of a high-dehydration-rate plugging agent and 0.2-0.3 part of calcium oxide. The natural plant inertia material, the fiber plugging agent and the acid soluble plugging agent are mixed according to the certain matching ratio to form the acid soluble plugging material in granule and fiber shapes. The material has the advantages that the bridging effect of a bridging material is good and the plugging success rate is high, and also has the advantages that the density is low, stratum pressure is effectively balanced, the stratum damage is small, the plugging property is strong and acid solubility is achieved. The plugging slurry prepared from the plugging material and water has the advantages of being low in density, high in pressure bearing capability, good in malignant leakage plugging effect, high in acid solubility and the like; the on-site preparation process is simple, construction is safe and reliable, and the purposes of reducing well leakage loss and protecting the reservoir stratum can be achieved.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method for destabilization coagulating treatment of well drilling waste liquid

The invention relates to a method for destabilization coagulating treatment of well drilling waste liquid for carrying out innocent treatment on the well drilling waste liquid in oil-gas field well drilling. The method can be used for carrying out innocent treatment on the well drilling waste liquid and increasing a treatment effect. In a technical scheme, the method comprises the following stepsof: firstly, adding a destabilizing agent into a reaction tank filled with well drilling waste liquid, wherein the destabilizing agent is prepared by preparing a mixture of 85 percent of CaCl2 and 15percent of MgCl2 into a solution with the concentration of 20 percent; stirring and mixing for 10-15 minutes to make destabilize the well drilling waste liquid; adding a coagulating agent into the tank, wherein the coagulating agent is prepared by preparing a mixture of 95 percent of polyAlCl3 and 5 percent of polyacrylamide into a solution with the concentration of 20 percent; stirring and mixing for 15-20 minutes; and finally, inputting the mixture into a solid-liquid separating device, wherein after the mixture is separated, a liquid phase reaches an emission standard and a curing agent isadded into a solid phase for carrying out curing treatment. Treatment agents used in the invention have good destabilizing and coagulating effects on the well drilling waste liquid and are low in dosage and convenient for operation; and the method has the advantages of low cost and economy and is used for innocent treatment of the well drilling waste liquid.
Owner:FD PETROL GRP

Controllably degraded biological full-degradable plastic and preparation method thereof

The invention discloses a controllably degraded biological full-degradable plastic, and relates to the technical field of plastic preparation. The controllably degraded biological full-degradable plastic is prepared from the following raw materials in parts by weight: 15 to 25 parts of straw fiber, 10 to 20 parts of bran, 5 to 15 parts of cyclodextrin, 4 to 12 parts of maltodextrin, 15 to 25 partsof polylactic acid, 15 to 25 parts of poly(butylene succinate), 6 to 16 parts of calcium carbonate, 4 to 10 parts of Pulullan, 3 to 7 parts of chitosan, 1 to 7 parts of benzoic acid, 1 to 5 parts ofacetic acid, 2 to 8 parts of sodium stearate, 1 to 7 parts of ethylene acrylic acid co polymer, 4 to 12 parts of linolenate, 5 to 15 parts of Arabic gum, 2 to 8 parts of mannitol, 2 to 8 parts of oxidized polyethlene wax and 4 to 10 parts of sodium carboxymethyl starch. The preparation method comprises the following steps: pretreatment of bran, modification of straw fiber, mixing, extrusion blow molding and the like. According to the plastic disclosed by the invention, biological full-degradation can be carried out, and the degradation time is controlled by adjusting the proportion of degradable substances, and degradation can be completed fundamentally outdoors for 3 to 9 months, so that the environment cannot be polluted, and the plastic is high in structural strength and mechanical strength at the same time.
Owner:肖宇萍

Lignin-based polyquatemary salt cation water treatment agent and preparation method thereof

The invention relates to the technical field of a sewage treatment material, in particular to a lignin-based polyquatemary salt cation water treatment agent and a preparation method thereof. The method is characterized in that potassium ethyl xanthogenate and 2-bromopropionic acid are used as raw materials for preparing 2-(ethoxythiomethyl) thiodipropionic acid; then, the 2-(ethoxythiomethyl) thiodipropionic acid and alkali lignin or lignin derivatives are synthetized into a lignin-based RAFT chain transfer agent through esterification reaction; finally, under the effects of a radical initiator and the lignin-based RAFT chain transfer agent, methacryloyloxyethyl trimethyl ammonium chloride is polymerized to obtain a star-shaped multi-arm lignin-based polyquatemary salt cation water treatment agent through free radical active polymerization. The method has the characteristics that the conversion rate is high; the molecular weight is great; the molecular weight distribution is narrow; the reaction conditions are mild; the target product structure can be designed, regulated and controlled according to the flocculating performance; the flocculating efficiency is high. The prepared water treatment agent can be widely applied to the removal of suspension solid particles difficult to settle in domestic sewage and industrial sewage.
Owner:GUANGXI UNIV FOR NATITIES

Preparation method of polylactic acid composite material by use of oriented distribution of nano-hydroxyapatite for enhancement

The invention relates to a preparation method of a polylactic acid composite material by use of oriented distribution of nano-hydroxyapatite for enhancement, and the method is as follows: calcium nitrate, ammonium phosphate and gelatin aqueous solution are mixed for preparation of hydroxyapatite suspension by heating, PH adjusting and homoiothermy; polylactic acid is dissolved in an organic solvent and then is added to the suspension for mixing, heating and centrifugal drying to prepare hydroxyapatite-polylactic acid composite powder and granulate; and multi-channel shear extrusion deformation of an injection-molded composite molding material is performed by an equal channel angular pressing die under certain process conditions to obtain the target product. The advantages of the preparation method are that: gelatin is introduced to improve the uniform distribution of the hydroxyapatite in a polylactic acid matrix and increase the interface bonding strength; by multi-channel equal angular pressing, the rod-like hydroxyapatite can be directionally evenly distributed in the polylactic acid matrix, the comprehensive mechanics performance of the composite material can be improved, and the preparation process is simple, low-cost, and more suitable for productization.
Owner:TIANJIN UNIVERSITY OF TECHNOLOGY

Aluminum pigment for 3D printing high polymer material and preparation method of aluminum pigment

The invention discloses an aluminum pigment for a 3D printing high polymer material. The aluminum pigment comprises the following raw materials in percentage by weight: 75-80% of an aluminum pigment,10-15% of a carrier resin, 3-5% of a compatilizer, 1-3 parts of an antioxidant and 2-4 parts of a lubricant. A preparation method of the aluminum pigment comprises the following steps: uniformly mixing the raw materials according to a formula ratio so as to obtain a mixed material; putting the mixed material into a single screw extruder, and performing extrusion through eight temperature zones of130 DEG C, 140 DEG C, 160 DEG C, 160 DEG C, 160 DEG C, 160 DEG C, 150 DEG C and DEG C, thereby obtaining a finished product. The aluminum pigment has the advantages that the formula of a pre-dispersedaluminum pigment is optimized, the 3D printing high polymer material is adopted as the carrier resin and has an excellent coupling dispersion property and a bridging function of a silane coupling agent, the compatibility of the pre-dispersed aluminum pigment and a main body high polymer material is greatly improved, and the VOCs (Volatile Organic Chemicals) emission is reduced; the aluminum pigment is processed by virtue of the thermal plastic principle of plastic, defective products can be reprocessed, the product pass percent is increased, and the production and manufacturing cost is reduced.
Owner:安徽天易金属新材料有限公司

Ammonium salt sewage treatment flocculant

The invention relates to the field of sewage treatment, in particular to an ammonium salt sewage treatment flocculant. The preparation method comprises the following steps: grafting carboxyl anions on cyano groups of chitosan molecules by using chloroacetic acid, then carrying out free radical polymerization by using a quaternary ammonium salt cationic monomer, and grafting a long-chain cationic unit to prepare the chitosan flocculant with an amphoteric structure. According to the invention, the steric hindrance during free radical polymerization of the cationic monomer is reduced, the grafting rate of a long-chain cationic unit is increased, the flocculant fully plays a sufficient charge attraction role, the bridging capability of molecules is improved, and the electrostatic adsorption capability and flocculation effect of the flocculant material are improved; secondly, the reactivity of chitosan molecules is improved, so that the situation that the flocculating agent only swells and loses the flocculation capacity due to self-crosslinking of long-chain cation units is prevented. The chitosan flocculant belongs to a natural polymer material, and has the advantages of high efficiency, environmental protection, low cost and the like.
Owner:成都高云智新材料科技有限公司

Radicalized nanowire growing on surface of C/C-Si composite material and preparation method at room temperature

The invention relates to a radicalized nanowire growing on the surface of a C/C-Si composite material and a preparation method at the room temperature. An embedding method is adopted to prepare a silicon coating on the surface of a carbon/ carbon composite material in a vacuum heating furnace, after the C/C-Si composite material is soaked by adopting a concentrated sulfuric acid and hydrogen peroxide mixed solution, the surface of the C/C-Si composite material is put into a monodisperse polystyrene microsphere solution, and after drying is carried out, metal spraying is carried out in a metalspraying sputtering instrument; then the C/C-Si composite material is put into a mixed solution composed of deionized water, glycerol, hydrogen peroxide and hydrofluoric acid by volume and etched at different time, and a Si nanowire growing radially on the surface of the C/C-Si composite material at the room temperature. The nanowire is the radicalized nanowire growing from the surface of the C/C-Si composite material, the binding force between an internal coating and an external coating can be improved, the thermal expansion mismatch is relieved, the decline of the mechanical performance caused by high-temperature processing for multiple times on the carbon/ carbon composite material can be reduced, so that the carbon/ carbon composite material can be effectively protected.
Owner:无锡博智复合材料有限公司

A plugging material and plugging slurry for protecting low-pressure fractured reservoirs

The invention discloses a plugging material and plugging slurry for protecting a reservoir stratum with the low fracturing fracture ability. The plugging material is prepared from, by weight, 5-6 parts of walnut shell powder, 2-3 parts of a composite plugging agent, 1.5-2 parts of an agent for plugging while drilling, 4-5 parts of an acid soluble plugging agent, 4-5 parts of a high-dehydration-rate plugging agent and 0.2-0.3 part of calcium oxide. The natural plant inertia material, the fiber plugging agent and the acid soluble plugging agent are mixed according to the certain matching ratio to form the acid soluble plugging material in granule and fiber shapes. The material has the advantages that the bridging effect of a bridging material is good and the plugging success rate is high, and also has the advantages that the density is low, stratum pressure is effectively balanced, the stratum damage is small, the plugging property is strong and acid solubility is achieved. The plugging slurry prepared from the plugging material and water has the advantages of being low in density, high in pressure bearing capability, good in malignant leakage plugging effect, high in acid solubility and the like; the on-site preparation process is simple, construction is safe and reliable, and the purposes of reducing well leakage loss and protecting the reservoir stratum can be achieved.
Owner:CHINA PETROLEUM & CHEM CORP +1

Preparation method of polylactic acid composite material reinforced with nano-hydroxyapatite orientation distribution

The invention relates to a preparation method of a polylactic acid composite material by use of oriented distribution of nano-hydroxyapatite for enhancement, and the method is as follows: calcium nitrate, ammonium phosphate and gelatin aqueous solution are mixed for preparation of hydroxyapatite suspension by heating, PH adjusting and homoiothermy; polylactic acid is dissolved in an organic solvent and then is added to the suspension for mixing, heating and centrifugal drying to prepare hydroxyapatite-polylactic acid composite powder and granulate; and multi-channel shear extrusion deformation of an injection-molded composite molding material is performed by an equal channel angular pressing die under certain process conditions to obtain the target product. The advantages of the preparation method are that: gelatin is introduced to improve the uniform distribution of the hydroxyapatite in a polylactic acid matrix and increase the interface bonding strength; by multi-channel equal angular pressing, the rod-like hydroxyapatite can be directionally evenly distributed in the polylactic acid matrix, the comprehensive mechanics performance of the composite material can be improved, and the preparation process is simple, low-cost, and more suitable for productization.
Owner:TIANJIN UNIVERSITY OF TECHNOLOGY
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