The application discloses a device for preparing electronic-grade
sodium hypophosphite dearsenicated
salt sodium salt, and belongs to the technical field of electronic
chemical preparation. The device realizes the efficient dispersion of
phosphine gas into micron-sized bubbles through a membrane dispersion
reaction system, realizes the full and stable reaction of the
phosphine gas with
sodium hypochlorite solution, guarantees the high efficiency and uniformity of the main synthesis reaction from the source, and provides a composition-stable crude product liquid for subsequent continuous purification. Through a bypass
arsenic removal unit integrated in a buffer adjustment
system, the on-line circulation oxidation-
precipitation-separation of
arsenic impurities is realized without interrupting the main synthesis process, and the problem of the interruption of the synthesis
route caused by the intermittent
arsenic removal in the traditional process is solved. By arranging
yellow phosphorus storage tanks in parallel and alternately working, the continuous and stable supply of the
raw material yellow phosphorus to the
phosphine reaction kettle is realized. The device ensures the long-term continuous and stable operation of the synthesis
route and the high consistency of product batches, and is particularly suitable for the large-scale
continuous production of electronic-grade
sodium hypophosphite.