54results about How to "Enhanced charge strength" patented technology

The invention discloses an amide quaternary ammonium salt sodium hydroxypropyl sulfonate asphalt emulsifier and a preparation method thereof. The asphalt emulsifier is prepared from coconut oil acyl propyl dimethyl tertiary amine, alcohol solvent, acrylic acid, epoxy chloropropane and sodium hydrogen sulfite according to a molar ratio of 1mol:(4.00-9.00)mol):(1.00-1.10)mol:(1.0-1.15)mol:(1.05-1.25)mol, wherein the alcohol solvent is alcohol, methanol or isopropanol. The asphalt emulsifier is easy-to-obtain in synthesis raw materials, low in production cost, simple in process and needless of high-temperature reaction and can emulsify asphalt different in type, emulsified asphalt prepared by using the asphalt emulsifier is exquisite, uniform and high in storage stability, and cationic emulsified asphalt can be prepared.

The invention discloses a secondary amide di-quaternary ammonium salt type hydroxypropyl sodium sulfonate asphalt emulsifier and a preparation method thereof, wherein the secondary amide di-quaternary ammonium salt type hydroxypropyl sodium sulfonate asphalt emulsifier is prepared from the following raw materials N-hydrogenated tallow-1,3-propylene diamine, an alcohol solvent, N-hydroxymethyl acrylamide, epichlorohydrin and sodium bisulfite according to a molar ratio of 1:(5.00-11.00):(3.00-3.10):(2.00-2.30):(2.10-2.50), and the alcohol solvent is ethanol, methanol or isopropanol. According to the present invention, the preparation method has advantages of easily available raw material, low production cost, simple process and no requirement of high temperature reaction; and the obtained secondary amide di-quaternary ammonium salt type hydroxypropyl sodium sulfonate asphalt emulsifier can emulsify a variety of different types of asphalts, and can be used for preparing cationic emulsified asphalts, and the emulsified asphalt prepared from the secondary amide di-quaternary ammonium salt type hydroxypropyl sodium sulfonate asphalt emulsifier has advantages of fine and uniform property and good storage stability.

The invention discloses a carboxylic acid diquaternary ammonium salt type sodium hydroxypropyl sulfonate asphalt emulsifier, the molecular structure of which is as follows: it is prepared from raw materials with the following molar ratio: N-hydrogenated tallow-1,3- The molar ratio of propylene diamine, alcohol solvent, acrylic acid, epichlorohydrin, sodium bisulfite is 1mol: (5.00‑11.00) mol: (3.00‑3.10) mol: (2.00‑2.30) mol: (2.10‑ 2.50) mol. The production cost of the asphalt emulsifier of the invention is low, the process is simple, and no high-temperature reaction is required.

The invention discloses a preparation method of an ultra-fine packaged cadmium sulfide selenide ceramic pigment. The steps are: 1) dissolving cadmium salt and surfactant in water to obtain solution A, dissolving sodium sulfide and selenium in water to obtain alkaline solution, dropping solution A into the alkaline solution to obtain cadmium sulfide selenide precursor, and then Carry out hydrothermal reaction to obtain dispersed cadmium sulfide selenide; 2) add water glass solution to acid solution, control pH to obtain silicic acid solution; 3) add dispersed cadmium sulfide selenide to zirconium oxychloride dispersion liquid, add silicon Acid solution, adjust the concentration of silicon ions and zirconium ions, adjust pH, and heat to obtain gel; 4) After drying the gel, mix it with a mineralizer, and calcine to obtain an ultra-fine packaged cadmium sulfide selenide ceramic colorant . The particle size D100 of the colorant prepared by the method is less than 1.3 μm, and the controllable and reproducible conditions of the method are very good, which is very suitable for large-scale production.

The invention discloses a dication asphalt emulsifier. The molecular structure of the dication asphalt emulsifier is shown in the description, wherein when x is equal to 1, y is equal to 1 and i is equal to 0; when x is equal to 2, y is equal to 0, z is equal to 1 or 0, and i plus z is equal to 1. The dication asphalt emulsifier is prepared from the following raw material in molar ratio: 1 mol of N-Hydrogenated tallow-1, 3-diaminopropane, 6.00-13.00 mol of alcohols solvent, 1.02-3.05 mol of methyl acrylate, and 2.02-2.10 mol of sodium chloroacetate. The alcohols solvent adopts ethyl alcohol, methyl alcohol or isopropyl alcohol. The synthetic raw material of the dication asphalt emulsifier is easy to get, the production cost is low, the technology is simple, and high-temperature reaction is not required. Different types of asphalt can be emulsified, the prepared asphalt emulsifier is exquisite and uniform, the storage stability is good, dication emulsified asphalt can be prepared, and the dication asphalt emulsifier is applied to spreading of road penetrated oil layers or bonding oil as well as slurry surfacing and micro-surfacing parts, and has the characteristics of a medium breaking asphalt emulsifier and a slow breaking asphalt emulsifier.

The invention discloses a secondary amide polyamine quaternary ammonium salt amphoteric asphalt emulsifier and a preparation method thereof. The asphalt emulsifier is prepared from the following molar ratio raw materials: cocoyl propyl dimethyl tertiary amine, alcohol The molar ratio of solvent-like solvent, water, epichlorohydrin, polyethylene polyamine, and acrylic acid is 1mol: (4.50‑10.00) mol: (14.00‑18.00) mol: (1.00‑1.15) mol: (1.00‑1.20) mol: (1.00‑1.20) mol. The alcoholic solvent is ethanol, methanol or isopropanol. The polyethylene polyamine is diethylenetriamine, triethylenetetramine or tetraethylenepentamine. The synthetic raw materials of the asphalt emulsifier of the invention are easy to obtain, the production cost is low, the process is simple, and no high-temperature reaction is required. It can emulsify various types of asphalt, and the prepared emulsified asphalt is fine and uniform, and has good storage stability.

The invention discloses a quaternary ammonium hydroxypropyl sodium phosphate quick breaking asphalt emulsifier and a preparation method thereof. The asphalt emulsifier is prepared from the following raw materials according to molar ratio: octadeyl dimethyl tertiary amine, an alcohol solvent, epoxy chloropropane and sodium dihydrogen phosphate with the molar ratio of 1mol to (4.00-9.00)mol to (1.00-1.15)mol to (1.50-1.73)mol, or octadeyl dimethyl tertiary amine, an alcohol solvent, epoxy chloropropane, rtiary sodium phosphate and hydrochloric acid with the molar ratio of 1mol to 4.00-9.00)mol to (1.00-1.15)mol to (1.30-1.50)mol to (1.40-1.61)mol. The alcohol solvent adopts ethanol, methanol or isopropanol. The asphalt emulsifier has the advantages that the raw materials are available, the production cost is low, the technology is simple, and high-temperature reaction is not required, various different models of asphalt can be emulsified, formed emulsified asphalt is fine and uniform, the storage stability is good, and cationic emulsified asphalt can be prepared.

The invention discloses a lignin polyamine cation rapid-cracking type asphalt emulsifier and a preparation method thereof. The molecular structure of the emulsifier is as shown in the specification. In the formula, R is methyl (-CH3), ethyl (-C2H5) or ethoxyl (-C2H4OH); LIGNIN represents a lignin molecular chain. The lignin polyamine cation rapid-cracking type asphalt emulsifier is prepared from the following raw materials in parts by weight: lignin, water, sodium hydroxide, diethylenetriamine, crylic acid, formaldehyde (37%), low-carbon-number tertiary amine and industrial hydrochloric acid in a ratio of 100:(159-230):(19-27):(32-40):(23-29):(30-36):(35-82):(42-50):(31-37). The lignin polyamine cation rapid-cracking type asphalt emulsifier disclosed by the invention is high in synthesis raw material availability, low in production cost, simple in process and free of high-temperature reaction. Multiple types of asphalt of different models can be emulsified, the prepared emulsified asphalt is fine and uniform, the storage stability is good, and the rapid-cracking type cation emulsified asphalt can be prepared.

The invention discloses a lignin cyclamine cationic-type asphalt emulsifier and a preparation method and application thereof. The molecular structure general formula of the emulsifier is as shown in the description, wherein R is a methyl group (-CH3) or an ethyl group (-C2H5) or a hydroxyethyl group (-C2H4OH), and LIGNIN represents a lignin molecular chain. The lignin cyclamine cationic-type asphalt emulsifier is prepared from, by mass, 100 parts of lignin, 159-230 parts of water, 19-27 parts of sodium hydroxide, 42-50 parts of N-aminoethylpiperazine, 23-29 parts of acrylic acid, 30-36 parts of formaldehyde (37%), 35-82 parts of tertiary amine with a low carbon number, 42-50 parts of industrial hydrochloric acid (30%) and 31-37 parts of epoxy chloropropane. According to the lignin cyclamine cationic-type asphalt emulsifier, the synthesis raw materials are easy to obtain, the production cost is low, the technology is simple, and high-temperature reacting is not needed; the emulsifier can emulsify different types of asphalt, the prepared emulsified asphalt is fine and uniform, the storage stability is good, and rapid-cracking cationic-type emulsified asphalt can be prepared.