Dicationic amide type asphalt emulsifier and preparation method therefor
A kind of asphalt emulsifier, dication technology, applied in the field of dication amide type asphalt emulsifier and its preparation, can solve the problems of high temperature reaction, high temperature reaction, high cost, etc., to achieve improved emulsification performance, good storage stability and low production cost low effect
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Embodiment 1
[0031] (1) Preparation of dicationic amide type asphalt emulsifier:
[0032] 1) Add 269.5g octadecylamine, 260g isopropanol in the reactor, heat and stir to dissolve. Then 145.7 g of acrylamide was added dropwise, and the reaction was stirred at 70° C. for 3 h.
[0033] The above synthetic product was separated and purified by recrystallization and then detected by FTIR. The results are as follows: 3371cm -1 and 3205cm -1 The N-H stretching vibration absorption peak at 2916cm -1 and 2850cm -1 The asymmetric and symmetric stretching vibration absorption peaks of methylene respectively, 1666cm -1 It is the amide group C=O stretching vibration absorption peak, 1471cm -1 is the asymmetric bending vibration of methylene, 1417cm -1 is the asymmetric bending vibration of the methyl group, 1263cm -1 and 1128cm -1 C-N stretching vibration absorption peak, 717cm -1 It is the in-plane rocking vibration of methylene, 669cm -1 is the N-H out-of-plane deformation vibration of the ...
Embodiment 2
[0043] (1) Preparation of dicationic amide type asphalt emulsifier:
[0044] 1) Add 269.5g octadecylamine, 260g isopropanol in the reactor, heat and stir to dissolve. Then 145.7 g of acrylamide was added dropwise, and the reaction was stirred at 70° C. for 3 h.
[0045] 2) Add 109.1 g of triethylamine into the reactor, gradually add 131.2 g of 30% industrial hydrochloric acid, then gradually add 97.1 g of epichlorohydrin, stir and react at 35° C. for 2 h, and obtain reaction intermediate B. The prepared reaction intermediate B was added dropwise to the synthesis product in step 1) above, and stirred at 65° C. for 3 h. The dicationic amide type asphalt emulsifier was obtained, which was reserved for the emulsified asphalt test.
[0046] After recrystallization, separation and purification of the prepared dicationic amide type asphalt emulsifier, FTIR detection is carried out, and the results are as follows: 3298cm -1 The stretching vibration absorption peak of O-H is at 3157...
Embodiment 3
[0054] (1) Preparation of dicationic amide type asphalt emulsifier:
[0055] 1) Add 269.5g octadecylamine, 260g isopropanol in the reactor, heat and stir to dissolve. Then 145.7 g of acrylamide was added dropwise, and the reaction was stirred at 65° C. for 4 h.
[0056] 2) Add 189.6g of 85% triethanolamine to the reactor, gradually add 131.2g of 30% industrial hydrochloric acid, then gradually add 97.1g of epichlorohydrin, stir and react at 30-70°C for 2h, and obtain reaction intermediate C. The prepared reaction intermediate C was added dropwise to the synthesis product in step 1) above, and stirred at 70° C. for 2 h. The dicationic amide type asphalt emulsifier was obtained, which was reserved for the emulsified asphalt test.
[0057] After recrystallization, separation and purification of the prepared dicationic amide type asphalt emulsifier, FTIR detection is carried out, and the results are as follows: 3377cm -1 O-H stretching vibration absorption peak at 3159cm -1 Th...
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